Determination of Pesticide Residue Present in Cumin Plant (Nigella orientalis L.) with LC-MS/MS and GC-MS

Nilda Ersoy; Sevinc Sener; Ayse Yalcin Elidemir; Ebru Evcil; Ergun Dogen

doi:10.14233/ajchem.2016.19564

Issue

Vol. 28 No. 5 (2016): Vol 28 Issue 5

Issue Published : January 30, 2016

This work is licensed under a Creative Commons Attribution 4.0 International License.

Determination of Pesticide Residue Present in Cumin Plant (Nigella orientalis L.) with LC-MS/MS and GC-MS

https://doi.org/10.14233/ajchem.2016.19564

Nilda Ersoy

Organic Culture Program, Vocational School of Technical Sciences, Akdeniz University, Antalya 07058, Turkey

Sevinc Sener

Organic Culture Program, Vocational School of Technical Sciences, Akdeniz University, Antalya 07058, Turkey

Ayse Yalcin Elidemir

Vocational Schools of Finike, Akdeniz University, Antalya 07058, Turkey

Ebru Evcil

Izmir Food Control Laboratory Directorate, Turkey

Ergun Dogen

Izmir Food Control Laboratory Directorate, Turkey

Corresponding Author(s) : Nilda Ersoy

nildaersoy@akdeniz.edu.tr

Asian Journal of Chemistry, Vol. 28 No. 5 (2016): Vol 28 Issue 5
Article Published : January 30, 2016

Abstract

In this study, pesticide residues were investigated in black cumin (Nigella orientalis L.) seeds which grown in Turkey. GC-MS and LC-MS/MS analytical instruments are used in high precision, when determining residue limits. A total of 100 pesticide active ingredients in LC-MS/MS devices have been performed in Nigella orientalis L. seeds samples. In this plant, 103 pesticide active ingredients were analyzed in GC-MS. This study conducted in 2012 and 2013. Samples residues were not found in detectable levels for 2 years.

Keywords

Pesticide Residue Black cumin

Ersoy, N., Sener, S., Elidemir, A. Y., Evcil, E., & Dogen, E. (2016). Determination of Pesticide Residue Present in Cumin Plant (Nigella orientalis L.) with LC-MS/MS and GC-MS. Asian Journal of Chemistry, 28(5), 1011–1014. https://doi.org/10.14233/ajchem.2016.19564

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References

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References

M. Zohary, Plant Systematics and Evolution, 142, 71 (1983); doi:10.1007/BF00989605.

B.H. Ali and G. Blunden, Phytother. Res., 17, 299 (2003); doi:10.1002/ptr.1309.

E. Agradi, G. Fico, F. Cillo, C. Francisci and F. Tome, Planta Med., 67, 553 (2001); doi:10.1055/s-2001-16485.

Anonymous (2007); http://bitkilerinyararlari/com/ 2007/07/rek-otu-nigellasativa.html.

P.H. Davis, Flora of Turkey, 1, 98 (1965).

Anonymous (2007); http://www.ihya.org/forum/ mc.php?t2 =metin&mln=2&an=5519.

L. Kokoska, J. Havlik, I. Valterova, A. Nepovim, V. Rada and T. Vanek, Flav. Fragr. J., 20, 419 (2005); doi:10.1002/ffj.1449.

M. Gun, Lokman Hekim J., 2, 43 (2012).

H. Wagner and N.R. Fransworth, Economic and Medicinal Plant Research, Plants and Traditional Medicine, Academic Press, vol. 4 (1990).

C. Nergiz and S. Otles, Food Chem., 48, 259 (1993); doi:10.1016/0308-8146(93)90137-5.

M.A. Farag, H.A. Gad, A.G. Heiss and L.A. Wessjohann, Food Chem., 151, 333 (2014); doi:10.1016/j.foodchem.2013.11.032.

K. Baser, B. Demirci, A. Donmez and Z. Ugurlu, Planta Med., 76, 1231 (2010); doi:10.1055/s-0030-1264451.

A. Meziti, H. Meziti, K. Boudiaf, B. Mustapha and H. Bouriche, World Academy of Science, Eng. Technol., 6, 24 (2012).

A. Wajs and D. Kalemba, J. Essential Oil Res., 22, 232 (2010); doi:10.1080/10412905.2010.9700311.

M. Sirma and I. Kadioglu, Ziraat Fakültesi Dergisi, 27, 27 (2010).

E. Tulukcu and O. Sagdic, Erciyes Üniv. Fen Bilimleri Enstitüsü Dergisi, 27, 304 (2011).

J. Kim, S. Seo, S. Lee, S. Shin and I. Park, J. Agric. Food Chem., 56, 7316 (2008); doi:10.1021/jf800780f.

N. Ersoy, O. Tatli, S. Ozcan, E. Evcil, L.S. Coskun, E. Erdogan and G. Keskin, Selçuk Tarim Gida Bilimleri Dergisi, 25, 70 (2011).

S.J. Lehotay, J. AOAC Int., 90, 485 (2007).

A.M. Mohamadin, B. Sheikh, A.A. Abd El-Aal, A.A. Elberry and F.A. Al-Abbasi, Pestic. Biochem. Physiol., 98, 128 (2010); doi:10.1016/j.pestbp.2010.05.011.

M. Negahban, S. Moharramipour and F. Sefidkon, J. Stored Prod. Res., 43, 123 (2007); doi:10.1016/j.jspr.2006.02.002.

S. Rajendran and V. Sriranjini, J. Stored Prod. Res., 44, 126 (2008); doi:10.1016/j.jspr.2007.08.003.

H.F.C. Su, J. Entomol. Sci., 25, 16 (1990).

S.N. Mukherjee and M. Joseph, J. Med. Arom. Plant Sci., 22-23, 154 (2000).

M.K. Chaubey, African J. Agric. Res., 2, 596 (2007).

E. Shaaya, U. Ravid, N. Paster, B. Juven, U. Zisman and V. Pissarev, J. Chem. Ecol., 17, 499 (1991); doi:10.1007/BF00982120.

T.L.S. Ngamo, A. Goudoum, M.B. Ngassoum, G.M. Lognay, F. Malaisse and T. Hance, African J. Agric. Res., 2, 164 (2007).

I. Tunc, B.M. Berger, F. Erler and F. Dagli, J. Stored Prod. Res., 36, 161 (2000); doi:10.1016/S0022-474X(99)00036-3.

E. Shaaya, M. Kostjukovski, J. Eilberg and C. Sukprakarn, J. Stored Prod. Res., 33, 7 (1997); doi:10.1016/S0022-474X(96)00032-X.

A.A.K. Abou-Arab, Food Chem., 65, 509 (1999); doi:10.1016/S0308-8146(98)00231-3.

Issue

Vol. 28 No. 5 (2016): Vol 28 Issue 5

Determination of Pesticide Residue Present in Cumin Plant (Nigella orientalis L.) with LC-MS/MS and GC-MS

Corresponding Author(s) : Nilda Ersoy

Abstract

Keywords

Full Article

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References

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