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Vol. 31 No. 2 (2019): Vol. 31 No. 2

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A Robust Modification of SiO2 Nanoparticles by Poly(2-hydroxyethylmethacrylate) via Surface-Initiated Atom Transfer Radical Polymerization

https://doi.org/10.14233/ajchem.2019.21608
Duy Trinh Nguyen
Nguyen Tat Thanh University, 300A Nguyen Tat Thanh, District 4, Ho Chi Minh City, Vietnam
Thuong Nhan Phu Nguyen
Nguyen Tat Thanh University, 300A Nguyen Tat Thanh, District 4, Ho Chi Minh City, Vietnam
Duy Chinh Nguyen
Nguyen Tat Thanh University, 300A Nguyen Tat Thanh, District 4, Ho Chi Minh City, Vietnam
Van Thi Thanh Ho
Hochiminh University of Natural Resources and Environment, 236B Le Van Sy, Ward 1, Tan Binh District, Ho Chi Minh City, Vietnam
Md. Rafiqul Islam
Pukyong National University, Busan 608-737, Republic of Korea
Kwon Taek Lim
Pukyong National University, Busan 608-737, Republic of Korea
Long Giang Bach
Nguyen Tat Thanh University, 300A Nguyen Tat Thanh, District 4, Ho Chi Minh City, Vietnam

Corresponding Author(s) : Long Giang Bach

blgiangntt@gmail.com

Asian Journal of Chemistry, Vol. 31 No. 2 (2019): Vol. 31 No. 2

Abstract

An effortless and efficient method for the alteration of SiO2 nanoparticles by poly(2-hydroxyethylmethacrylate) (PHEMA) has been developed. Initially, a strategic atom transfer radical polymerization (ATRP) initiator was anchored to SiO2 nanoparticles surface via coupling reaction followed by surface-initiated atom transfer radical polymerization of HEMA successfully afforded chemically grafted PHEMA to SiO2 nanoparticles (PHEMA-g-SiO2). We used XPS, FT-IR and EDS analyses for confirming the covalent immobilization of PHEMA onto SiO2 nanoparticles. TGA/DSC and zeta potentials measurements were used for determining the thermal and surface charge features of the nanocomposites, respectively.

Keywords

Surface functionalization SiO2 Nanoparticles Polymer chains Poly(2-hydroxyethylmethacrylate)
Nguyen, D. T., Phu Nguyen, T. N., Nguyen, D. C., Thanh Ho, V. T., Islam, M. R., Lim, K. T., & Bach, L. G. (2018). A Robust Modification of SiO2 Nanoparticles by Poly(2-hydroxyethylmethacrylate) via Surface-Initiated Atom Transfer Radical Polymerization. Asian Journal of Chemistry, 31(2), 337–342. https://doi.org/10.14233/ajchem.2019.21608
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