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Vol. 28 No. 9 (2016): Vol 28 Issue 9

Copyright (c) 2016 AJC

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Etched Stainless Steel Wire as Solid-Phase Microextraction Fiber for Determination of Polychlorinated Biphenyls in Water Sample

https://doi.org/10.14233/ajchem.2016.19855
Rui Chang
Huajin Campus of Anhui Normal University, Wuhu 241000, P.R. China
Jing Li
Huajin Campus of Anhui Normal University, Wuhu 241000, P.R. China
Fengqin Wang
Huajin Campus of Anhui Normal University, Wuhu 241000, P.R. China
Guang-Chao Zhao
Huajin Campus of Anhui Normal University, Wuhu 241000, P.R. China; College of Environmental Science and Engineering, Anhui Normal University, Wuhu 241000, P.R. China

Corresponding Author(s) : Guang-Chao Zhao

gczhao@mail.ahnu.edu.cn

Asian Journal of Chemistry, Vol. 28 No. 9 (2016): Vol 28 Issue 9

Abstract

Etched stainless steel wire was simply fabricated and used as a solid-phase microextraction fiber to determinate polychlorinated biphenyls in water sample. The morphology and structure of the proposed fiber was characterized and elucidated by scanning electron microscope. Experimental parameters, including the extraction mode, extraction temperature, extraction time, desorption time were examined and optimized. Under the optimized conditions, a good analytical performance was achieved and the etched stainless steel fiber displayed a better extraction capability than commercial fiber. Furthermore, the spiked recoveries at 80 ng L-1 for real river water were in the range of 88.9-98.9 %, which confirmed the feasibility of the developed method.

Keywords

Solid-phase microextraction Etched stainless steel wire Polychlorinated biphenyls Gas chromatography
Chang, R., Li, J., Wang, F., & Zhao, G.-C. (2016). Etched Stainless Steel Wire as Solid-Phase Microextraction Fiber for Determination of Polychlorinated Biphenyls in Water Sample. Asian Journal of Chemistry, 28(9), 1967–1971. https://doi.org/10.14233/ajchem.2016.19855
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