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Vol. 24 No. 8 (2012): Vol 24 Issue 8

Solid-State Metathetic Synthesis and Photoluminescence of Calcium Tungstate Particles Assisted by Cyclic Microwave Irradiation

Won-Chun Oh
Department of Advanced Materials Science & Engineering, Hanseo University, Seosan 356- 706, South Korea
Chong Yeon Park
Department of Advanced Materials Science & Engineering, Hanseo University, Seosan 356- 706, South Korea
Jeong Won Jeon
Department of Advanced Materials Science & Engineering, Hanseo University, Seosan 356- 706, South Korea
Chang Sung Lim
Department of Advanced Materials Science & Engineering, Hanseo University, Seosan 356- 706, South Korea

Corresponding Author(s) : Chang Sung Lim

cslim@hanseo.ac.kr

Asian Journal of Chemistry, Vol. 24 No. 8 (2012): Vol 24 Issue 8

Abstract

A solid-state metathetic (SSM) route assisted by cyclic microwave irradiation was used to synthesize calcium tungstate (CaWO4) particles. Well crystallized CaWO4 particles were formed at 600 ºC for 3 h, showing a fine and homogeneous morphology with sizes of 1-2 μm. The characteristics of the solid-state metathetic reaction of the CaWO4 particles were examined in detail based on the exothermic reaction. The obtained CaWO4 particles were characterized by X-ray diffraction, Fourier transform infrared spectroscopy and scanning electron microscopy. The optical properties were examined by photoluminescence emission and Raman spectroscopy.

Keywords

Calcium tungstate Solid-state metathetic reaction Cyclic microwave irradiation Photoluminescence Raman spectroscopy
Oh, W.-C., Yeon Park, C., Won Jeon, J., & Sung Lim, C. (2012). Solid-State Metathetic Synthesis and Photoluminescence of Calcium Tungstate Particles Assisted by Cyclic Microwave Irradiation. Asian Journal of Chemistry, 24(8), 3319–3322. Retrieved from https://asianpubs.org/index.php/ajchem/article/view/9364
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