Copyright (c) 2016 AJC
This work is licensed under a Creative Commons Attribution 4.0 International License.
Synthesis, Characterization of Si/Fe2O3 Nanoparticles and their Antibacterial Activity against Staphylococcus aureus and Escherichia coli
Corresponding Author(s) : Muhammad Akhyar Farrukh
Asian Journal of Chemistry,
Vol. 28 No. 7 (2016): Vol 28 Issue 7
Abstract
Silicon doped iron oxide (Si/Fe2O3) nanoparticles were successfully synthesized by co-precipitation method at 60 °C with 2-propanol as solvent. The particle size of Si/Fe2O3 nanoparticles measured with transmission electron microscope and dynamic light scattering techniques are nearly same (36.65 nm). The properties of Si/Fe2O3 nanoparticles are different than core shell SiO2/Fe2O3 nanoparticles as they show aggregation and antibacterial properties. Its antibacterial effect was studied against Staphylococcus aureus and Escherichia coli which showed the significant results. The other structural characteristics of the Si/Fe2O3 nanoparticles were analyzed by scanning electron microscope, X-ray diffraction, thermal gravimetric analysis and Fourier transform infrared spectroscopy.
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- A. Elaissari and V. Bourrel, J. Magn. Magn. Mater., 225, 151 (2001); doi:10.1016/S0304-8853(00)01244-0.
- M. Koneracka, P. Kopcansky, M. Antalik, M. Timko, C. Ramchand, D. Lobo, R. Mehta and R. Upadhyay, J. Magn. Magn. Mater., 201, 427 (1999); doi:10.1016/S0304-8853(99)00005-0.
- H. Gries, W. Mutzel, C. Zurth and H.J. Weinmanm, Magnetic Particles for Diagnostic Purposes, US Patent 5746999 (1998).
- D.K. Kim, Y. Zhang, W. Voit, K.V. Rao and M. Muhammed, J. Magn. Magn. Mater., 225, 30 (2001); doi:10.1016/S0304-8853(00)01224-5.
- Y.H. Choa, J.K. Yang, W.J. Yang and K.H. Auh, J. Magn. Magn. Mater., 266, 20 (2003); doi:10.1016/S0304-8853(03)00451-7.
- E.T. Fung, V. Thulasiraman, S.R. Weinberger and E.A. Dalmasso, Curr. Opin. Biotechnol., 12, 65 (2001); doi:10.1016/S0958-1669(00)00167-1.
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- A.S. Piers and C.H. Rochester, J. Colloid Interf. Sci., 174, 97 (1995); doi:10.1006/jcis.1995.1369.
- H. Okabayashi, I. Shimizu, E. Nishio and C.J.O. Connor, Colloid Polym. Sci., 275, 744 (1997); doi:10.1007/s003960050143.
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- O.K. Park, Y.S. Kang and B.G. Jo, J. Ind. Eng. Chem., 10, 733 (2004).
- S.A. Chulovskaya, K.N. Zheleznov and O.V. Zemtsova, Colloid J., 65, 786 (2003); doi:10.1023/B:COLL.0000009127.73109.cd.
- Y.S. Kang, S. Risbud, J.F. Rabolt and P. Stroeve, Chem. Mater., 8, 2209 (1996); doi:10.1021/cm960157j.
- S. Tao, X. Liu, X. Chu and Y. Shen, Sens. Actuators B, 61, 33 (1999); doi:10.1016/S0925-4005(99)00276-2.
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- W. Stöber, A. Fink and E. Bohn, J. Colloid Interf. Sci., 26, 62 (1968);doi:10.1016/0021-9797(68)90272-5.
- M. Ohmori and E. Matijević, J. Colloid Interf. Sci., 150, 594 (1992); doi:10.1016/0021-9797(92)90229-F.
- T. Naseem and M.A. Farrukh, J. Chem., 2015, 1 (2015); doi:10.1155/2015/912342.
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References
A. Elaissari and V. Bourrel, J. Magn. Magn. Mater., 225, 151 (2001); doi:10.1016/S0304-8853(00)01244-0.
M. Koneracka, P. Kopcansky, M. Antalik, M. Timko, C. Ramchand, D. Lobo, R. Mehta and R. Upadhyay, J. Magn. Magn. Mater., 201, 427 (1999); doi:10.1016/S0304-8853(99)00005-0.
H. Gries, W. Mutzel, C. Zurth and H.J. Weinmanm, Magnetic Particles for Diagnostic Purposes, US Patent 5746999 (1998).
D.K. Kim, Y. Zhang, W. Voit, K.V. Rao and M. Muhammed, J. Magn. Magn. Mater., 225, 30 (2001); doi:10.1016/S0304-8853(00)01224-5.
Y.H. Choa, J.K. Yang, W.J. Yang and K.H. Auh, J. Magn. Magn. Mater., 266, 20 (2003); doi:10.1016/S0304-8853(03)00451-7.
E.T. Fung, V. Thulasiraman, S.R. Weinberger and E.A. Dalmasso, Curr. Opin. Biotechnol., 12, 65 (2001); doi:10.1016/S0958-1669(00)00167-1.
A.K. Singh, A.W. Flounders, J.V. Volponi, C.S. Ashley, K. Wally and J.S. Schoeniger, Biosens. Bioelectron., 14, 703 (1999); doi:10.1016/S0956-5663(99)00044-5.
A.S. Piers and C.H. Rochester, J. Colloid Interf. Sci., 174, 97 (1995); doi:10.1006/jcis.1995.1369.
H. Okabayashi, I. Shimizu, E. Nishio and C.J.O. Connor, Colloid Polym. Sci., 275, 744 (1997); doi:10.1007/s003960050143.
K.C. Vrancken, L. De Coster, P. Van Der Voort, P.J. Grobet and E.F. Vansant, J. Colloid Interf. Sci., 170, 71 (1995); doi:10.1006/jcis.1995.1073.
S.T. Lim, M.S. Cho, H.J. Choi and M.S. Jhon, J. Ind. Eng. Chem., 9, 336 (2003).
M.S. Cho, S.T. Lim, I.B. Jang, H.J. Choi and M.S. Jhon, IEEE Trans. Magn., 40, 3036 (2004); doi:10.1109/TMAG.2004.830413.
I. Muneer, M.A. Farrukh, S. Javaid, M. Shahid and M. Khaleeq-ur-Rahman, Superlattices Microstruct., 77, 256 (2015); doi:10.1016/j.spmi.2014.10.006.
S. Javaid, M.A. Farrukh, I. Muneer, M. Shahid, M. Khaleeq-ur-Rahman and A.A. Umar, Superlattices Microstruct., 82, 234 (2015); doi:10.1016/j.spmi.2015.01.038.
K. Kim and H. Kim, J. Sol-Gel Sci. Technol., 25, 183 (2002); doi:10.1023/A:1020217105290.
O.K. Park, Y.S. Kang and B.G. Jo, J. Ind. Eng. Chem., 10, 733 (2004).
S.A. Chulovskaya, K.N. Zheleznov and O.V. Zemtsova, Colloid J., 65, 786 (2003); doi:10.1023/B:COLL.0000009127.73109.cd.
Y.S. Kang, S. Risbud, J.F. Rabolt and P. Stroeve, Chem. Mater., 8, 2209 (1996); doi:10.1021/cm960157j.
S. Tao, X. Liu, X. Chu and Y. Shen, Sens. Actuators B, 61, 33 (1999); doi:10.1016/S0925-4005(99)00276-2.
X. Liu, Z. Ma, J. Xing and H. Liu, J. Magn. Magn.Mater., 270, 1 (2004); doi:10.1016/j.jmmm.2003.07.006.
W. Stöber, A. Fink and E. Bohn, J. Colloid Interf. Sci., 26, 62 (1968);doi:10.1016/0021-9797(68)90272-5.
M. Ohmori and E. Matijević, J. Colloid Interf. Sci., 150, 594 (1992); doi:10.1016/0021-9797(92)90229-F.
T. Naseem and M.A. Farrukh, J. Chem., 2015, 1 (2015); doi:10.1155/2015/912342.
E. Doelsch, W.E.E. Stone, S. Petit, A. Masion, J. Rose, J.-Y. Bottero and D. Nahon, Langmuir, 17, 1399 (2001); doi:10.1021/la0013188.