Issue

Vol. 25 No. 15 (2013): Vol 25 Issue 15

Copyright (c) 2013 AJC

Creative Commons License

This work is licensed under a Creative Commons Attribution 4.0 International License.

Tetramer Crystal Structure of Thiophene-2-carboxylic Acid

https://doi.org/10.14233/ajchem.2013.15334
Wei Ke
College of Biology and Environmental Engineering, Zhejiang Shuren University, Hangzhou 310015, Zhejiang, P.R. China
Na-Bo Sun
College of Biology and Environmental Engineering, Zhejiang Shuren University, Hangzhou 310015, Zhejiang, P.R. China
Hong-Ke Wu
College of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310014, Zhejiang, P.R. China

Corresponding Author(s) : Hong-Ke Wu

wuhk910@gmail.com

Asian Journal of Chemistry, Vol. 25 No. 15 (2013): Vol 25 Issue 15

Abstract

The structure of thiophene-2-carboxylic acid (m.f. C20H16O8S4) was studied by X-ray diffraction. The crystals are orthorhombic, space group Pna2(1) with a = 10.106(2), b = 14.299(3), c = 16.092(3) Å, a = 90.00, b = 90, g = 90.00º, V = 2325.5(8) Å3, Z = 4, F(000) = 1056, Dc = 1.464 g/cm3, μ = 0.452 cm-1, the final R = 0.0481 and wR = 0.1358. A total of 16217 reflections were collected, of which 3849 were independent (Rint = 0.0429).

Keywords

Tetramer Crystal structure Thiophene-2-carboxylic acid
Ke, W., Sun, N.-B., & Wu, H.-K. (2013). Tetramer Crystal Structure of Thiophene-2-carboxylic Acid. Asian Journal of Chemistry, 25(15), 8715–8717. https://doi.org/10.14233/ajchem.2013.15334
Download Citation
Endnote/Zotero/Mendeley (RIS)
BibTeX
References
  1. (a) X.H. Liu, C.X. Tan and J.Q. Weng, Asian J. Chem., 23, 4064 (2011); (b) X.H. Liu, C.X. Tan and J.Q. Weng, Phosphorus Sulfur Silicon Rel. Elem., 186, 552 (2011); (c) X.H. Liu, J.Q. Weng, C.X. Tan, L. Pan, B.L. Wang and Z.M. Li, Asian J. Chem., 23, 4031 (2011); (d) C.X. Tan, Y.X. Shi, J.Q. Weng, X.H. Liu, B.J. Li and W.G. Zhao, Lett. Drug Des. Discov., 9, 431 (2012); (e) C.X. Tan, Y.X. Shi, J.Q. Weng, X.H. Liu, B.J. Li and W.G. Zhao, J. Heterocycl. Chem., doi: 10.1002/jhet.1656; (f) J.Y. Tong, Y.X. Shi, X.H. Liu, N.B. Sun and B.J. Li, Chin. J. Org. Chem., 32, 2373 (2012); (g) X.H. Liu, W.G. Zhao, B.L. Wang and Z.M. Li, Res. Chem. Intermed., 38, 1999 (2012); (h) N.N. Su, Y. Li, S.J. Yu, X. Zhang, X.H. Liu and W.G. Zhao, Res. Chem. Intermed., 39, 759 (2012); (i) X.H. Liu, L. Pan, Y. Ma, J.Q. Weng, C.X. Tan, Y.H. Li, Y.X. Shi, B.J. Li, Z.M. Li and Y.G. Zhang, Chem. Biol. Drug Des., 78, 689 (2011); (j) X.H. Liu, J.Q. Weng, B.L. Wang, Y.H. Li, C.X. Tan and Z.M. Li, Res. Chem. Intermed., DOI: 10.1007/s11164-013-1113-4 (2013); (k) J.Y. Tong, N.B. Sun and H.K. Wu, J. Chem. Soc. Pakistan, 34, 1300 (2012); (l) N.B. Sun, J.Z. Jin, C. Lei and W. Ke, Asian J. Chem., 25, 4067 (2013).
  2. (a) Y.L. Xue, Y.G. Zhang and X.H. Liu, Asian J. Chem., 24, 3016 (2012); (b) P.Q. Chen, C.X. Tan, J.Q. Weng and X.H. Liu, Asian J. Chem., 24, 2808 (2012); (c) Y.L. Xue, Y.G. Zhang and X.H. Liu, Asian J. Chem., 24, 1571 (2012); (d) Y.L. Xue, Y.G. Zhang and X.H. Liu, Asian J. Chem., 24, 5087 (2012); (e) X.F. Liu and X.H. Liu, Acta Cryst., E67, o202 (2011); (f) X.H. Liu, L. Pan, C.X. Tan, J.Q. Weng, B.L. Wang and Z.M. Li, Pestic. Biochem. Physiol., 101, 143 (2011); (g) X.H. Liu, J.Q. Weng, C.X. Tan and H.J. Liu, Acta Cryst., E68, o493 (2012); (h) H.J. Liu, J.Q. Weng, C.X. Tan and X.H. Liu, Acta Cryst., E67, o1940 (2011); (i) X.H. Liu, C.X. Tan and J.Q. Weng, Phosphorus Sulfur Silicon Rel. Elem., 186, 558 (2011); (j) C.X. Tan, J.Q. Weng, Z.X. Liu, X.H. Liu and W.G. Zhao, Phosphorus Sulfur Silicon Rel. Elem., 187, 990 (2012); (k) J.Q. Weng, L. Wang and X.H. Liu, J. Chem. Soc. Pak., 34, 1248 (2012); (l) X.H. Liu, L. Pan, J.Q. Weng, C.X. Tan, Y.H. Li, B.L. Wang and Z.M. Li, Mol. Divers., 16, 251 (2012); (m) R. Wu, C. Zhu, X.J. Du, L.X. Xiong, S.J. Yu, X.H. Liu, Z.M. Li and W.G. Zhao, Chem. Cent. J., 6, 99 (2012); (n) X.H. Liu, J.Q. Weng and C.X. Tan, J. Chem., Article ID 306361 (2013); (o) X.F. Liu, X.W. Xiao and X.H. Liu, Chin. J. Struct. Chem., 30, 1437 (2011).
  3. M.A.M. Asli, L. Firoozpour, V. Sheibani, D.N. Sarkandi,A. Sakhteman, A. Davood, A. Shafiee and A. Foroumadi, Asian J. Chem., 23, 2487 (2011).
  4. (a) P. Verma and P. Srivastava, Asian J. Chem., 22, 4234 (2010); (b) S.A. Khan and M. Kumar, Asian J. Chem., 23, 1439 (2011).
  5. Z.A. Kaplancikli, G. Turan-Zirouni, A. Ozdemir, M.D. Altintop and Y. Tunali, Asian J. Chem., 22, 6107 (2010).
  6. K. Gangarapu, S. Manda, S. Thota, R. Yerra, S.S. Karki, J. Balzarini, E. De Clercq and H. Tokuda, Lett. Drug Des. Discov., 9, 934 (2012).
  7. J. Varshney, A. Sharma and S.P. Gupta, Lett. Drug Des. Discov., 9, 389 (2012).
  8. R. Romagnoli, P.G. Baraldi, M.D. Carrion, C.L. Cara, A. Casolari, E. Hamel, E. Fabbri and R. Gambari, Lett. Drug Des. Discov., 7, 476 (2010).
  9. M. Nardelli, G. Fava and G. Giraldi, Acta Crystallogr., 15, 737 (1962).
Read More
Author biographies is not available.
Download
PDF
Statistic
Read Counter : 0 Download : 0