A variety of rough tungsten electrodes were created and their surface morphology and apparent electrochemical reactivity were analyzed, in order to explore their feasibility as a highly reactive working electrode in electrochemical cells. For this purpose, tungsten electrodes with different surface irregularities were prepared by a chemical etching process and the self-similar fractal dimensions of their surfaces were determined. Then, the integrated charges for hydrogen evolution on their surfaces were estimated in the potentiostatic condition as a measure of their surface reactivity.
Park, I.-T., Kim, W., Kim, E.-J., Bae, S.-E., Kim, J.-Y., & Shin, H.-C. (2013). Electrochemical Reactivity of Chemically Roughened Tungsten Electrodes. Asian Journal of Chemistry, 25(12), 7037–7040. https://doi.org/10.14233/ajchem.2013.13