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Synthesis and Supramolecular Structure of 1-(4-{[(E)-3,5-Dibromo-2-hydroxybenzylidene]amino}phenyl)ethanone O-benzyloxime
Corresponding Author(s) : Li Zhao
Asian Journal of Chemistry,
Vol. 25 No. 11 (2013): Vol 25 Issue 11
Abstract
The compound, 1-(4-{[(E)-3,5-dibromo-2-hydroxybenzylidene]amino}phenyl)ethanone O-benzyloxime, has been synthesized by ({4-amino}phenyl)ethanone O-benzyloxime and 3,5-dibromosalicylaldehyde in ethanol solution and characterized by X-ray crystallography. There is one fairly strong intramolecular O1-H1···N2 hydrogen bond. In the crystal structure, each compound is linked to two other molecules into an infinite 1D supramolecular chain via Br···O interactions [3.354(4) Å].
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- T. Katsuki, Coord. Chem. Rev., 140, 189 (1995).
- W.K. Dong, Y.X. Sun, C.Y. Zhao, X.Y. Dong and L. Xu, Polyhedron, 29, 2087 (2010).
- W.K. Dong, X.N. He, H.B. Yan, Z.W. Lv, X. Chen, C.Y. Zhao and X.L. Tang, Polyhedron, 28, 1419 (2009).
- J.P. Costes, F. Dahan and A. Dupuis, Inorg. Chem., 39, 165 (2000).
- W.K. Dong, Y.X. Sun, G.H. Liu, L. Li, X.Y. Dong and X.H. Gao, Z. Anorg. Allg. Chem., 638, 1370 (2012).
- M.F. Summers, L.G. Marzilli, P.N. Bresciani and L. Randaccio, J. Am. Chem. Soc., 106, 4478 (1984).
- W.K. Dong, Y.X. Sun, S.J. Xing, Y. Wang and X.H. Gao, Z. Naturforsch., 67b, 197 (2012).
- W.K. Dong, G. Wang, S.S. Gong, J.F. Tong, Y.X. Sun and X.H. Gao, Transition Met. Chem., 37, 271 (2012).
- L. Zhao and S. Weng, Acta Crystal., E66, o2473 (2010).
- W.K. Dong, J.G. Duan, Y.H. Guan, J.Y. Shi and C.Y. Zhao, Inorg. Chim. Acta, 362, 1129 (2009).
- W.K. Dong, Y.X. Sun, Y.P. Zhang, L. Li, X.N. He and X.L, Tang, Inorg. Chim. Acta, 362, 117 (2009).
- H.L. Wu, X.C. Huang, J.K. Yuan, F. Kou, F. Jia, B. Liu and Y. Bai, Z. Naturforsch., 66b, 1049 (2011).
- Y. Fan, W. You, H.-F. Qian, J.-L. Liu and W. Huang, Acta Cryst., E64, o799 (2008).
References
T. Katsuki, Coord. Chem. Rev., 140, 189 (1995).
W.K. Dong, Y.X. Sun, C.Y. Zhao, X.Y. Dong and L. Xu, Polyhedron, 29, 2087 (2010).
W.K. Dong, X.N. He, H.B. Yan, Z.W. Lv, X. Chen, C.Y. Zhao and X.L. Tang, Polyhedron, 28, 1419 (2009).
J.P. Costes, F. Dahan and A. Dupuis, Inorg. Chem., 39, 165 (2000).
W.K. Dong, Y.X. Sun, G.H. Liu, L. Li, X.Y. Dong and X.H. Gao, Z. Anorg. Allg. Chem., 638, 1370 (2012).
M.F. Summers, L.G. Marzilli, P.N. Bresciani and L. Randaccio, J. Am. Chem. Soc., 106, 4478 (1984).
W.K. Dong, Y.X. Sun, S.J. Xing, Y. Wang and X.H. Gao, Z. Naturforsch., 67b, 197 (2012).
W.K. Dong, G. Wang, S.S. Gong, J.F. Tong, Y.X. Sun and X.H. Gao, Transition Met. Chem., 37, 271 (2012).
L. Zhao and S. Weng, Acta Crystal., E66, o2473 (2010).
W.K. Dong, J.G. Duan, Y.H. Guan, J.Y. Shi and C.Y. Zhao, Inorg. Chim. Acta, 362, 1129 (2009).
W.K. Dong, Y.X. Sun, Y.P. Zhang, L. Li, X.N. He and X.L, Tang, Inorg. Chim. Acta, 362, 117 (2009).
H.L. Wu, X.C. Huang, J.K. Yuan, F. Kou, F. Jia, B. Liu and Y. Bai, Z. Naturforsch., 66b, 1049 (2011).
Y. Fan, W. You, H.-F. Qian, J.-L. Liu and W. Huang, Acta Cryst., E64, o799 (2008).