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Characterization of Volatile Constituents of Magnolia denudata Desr Flowers by Gas Chromatography-Mass Spectrometry with Headspace Solid-Phase Microextraction
Corresponding Author(s) : Qing Ye
Asian Journal of Chemistry,
Vol. 25 No. 11 (2013): Vol 25 Issue 11
Abstract
In this study, the volatile constituents of Magnolia denudata Desr flowers, including budding flowers, blooming flowers and withered flowers, were investigated by headspace (HS) solid-phase microextraction(SPME) and gas chromatography-mass spectrometry (GC-MS). Different SPME parameters (extraction temperature and extraction time) and fibres were studied. There are 47 compounds, 32 compounds, 31 compounds detected in budding, blooming and withered flowers, respectively. The result showed that HS-SPME-GC-MS afforded a simple, rapid, solvent-free method suitable for analysis of volatile compounds emitted from Magnolia denudata Desr flowers in different florescence.
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References
J. Adedeji, T.G. Hartman, R.T. Rosen and C. Ho, J. Agric. Food Chem., 139, 1494 (1991).
J. Zhang, P.L. Sun, S.Y. Xu and K. Yang, Fine Chem., 23, 372 (2006).
H.W. Wang, X.E. Lu and Y.X. Peng, Fine Chem., 24, 257 (2007).
A. Macleod and N.M. Pieris, Phytochemistry, 23, 361 (1984).
A.J. Macleod and C.H. Snyder, J. Agric. Food Chem., 33, 380 (1985).
M.F. Kok, F.M. Yong and G. Lim, Agric. Food Chem., 35, 779 (1987).
G.P. Blanch, G. Reglero, M. Herraiz and J. Tabera, J. Chromatogr. Sci., 29, 11 (1991).
A. Miszczak, C. Forney and R.K. Prange, J. Agric. Food Chem., 120, 650 (1995).
T.M.M. Malundo, E.A. Baldwin, M.G. Moshonas, R.A. Baker and R.L. Shewfelt, J. Agric. Food Chem., 45, 2187 (1997).
E. Ibanez, S. Lopez-Sebastifin, E. Ramos, J. Tabera and G. Reglero, Food Chem., 63, 281 (1998).
C. Falqui-Cao, Z. Wang, L. Urruty, J. Pommier and M. Montury, J. Agric. Food Chem., 49, 5092 (2001).
A. Sanusi, V. Guillet and M. Montury, J. Chromatogr. A, 1046, 35 (2004).
H. Li, G. Li and J. Jen, J. Chromatogr. A, 1012, 129 (2003).
M.R. Criado, I.R. Pereiro and R.C. Torrijos, Talanta, 63, 533 (2004).
M.C. Wei and J.F. Jen, J. Chromatogr. A, 1012, 111 (2003).
Y.Y. Shu, S.S. Wang, M. Tardif and Y.P. Huang, J. Chromatogr. A, 1008, 1 (2003).
V. Pino, J.H. Ayala, A.M. Afonso and V. Gonzalez, Anal. Chim. Acta, 477, 81 (2003).
N. Alizadeh,A. Mohammadia and M. Tabrizchi, J. Chromatogr. A, 1183, 21 (2008).
Y. Zhou, Q.W. Jiang, Q. Peng, D.L. Xuan and W.D. Qu, Chemosphere, 70, 256 (2007).
C.H. Deng, S. Lin, T.M. Huang, G.L. Duan and X.M. Zhang, Rapid Commun. Mass Spectrom., 20, 2120 (2006).
G.X. Song, C.H. Deng, D. Wu and Y.M. Hu, Chromatographia, 58, 769 (2003).
Z.G. Li, M.R. Lee and D.L. Shen, Anal. Chim. Acta, 576, 43 (2006).
Q. Wu, C.H. Deng, S. Shen, G.X. Song, Y.M. Hu, D.X. Fu, J.K. Chen and X.M. Zhang, Chromatographia, 59, 763 (2004).
C.H. Deng, Y. Mao, N. Yao and X.M. Zhang, Anal. Chim. Acta, 575, 120 (2006).
C.A. Zini, F. Augusto and E. Christensen, Anal. Chem., 73, 4729 (2001).
D. McCaskill and R. Croteau, TIBTECH, 16, 349 (1998).
J. Gershenzon and R. Croteau, In eds.: G. Rosenthal and M. Berenbaum, In Herbivores: Their Interaction with Secondary Plant Metabolites, Academic Press: San Diego, CA, Vol. 1, p. 165 (1991).
B.B. Lorenzetti, G.E.P. Souza, S.J. Sarti, D.S. Filho and S.H. Ferreira, J. Ethnopharmacol., 34, 43 (1991).
W.A. Russin, J.D. Hoesley, C.E. Elson, M.A. Tanner and M.N. Gould, Carcinogenesis, 10, 2161 (1989).
G. Zheng, P.M. Kenney and L.K.T. Lam, J. Agric. Food Chem., 41, 153 (1993).