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Synthesis and Crystal Structure of 1-(4-{[(E)-4-methoxy-2-hydroxybenzylidene]amino}phenyl)ethanoe Oxime
Corresponding Author(s) : Wen-Kui Dong
Asian Journal of Chemistry,
Vol. 25 No. 11 (2013): Vol 25 Issue 11
Abstract
The compound 1-(4-{[(E)-4-methoxy-2-hydroxybenzylidene]amino}phenyl)ethanoe oxime with the molecular formula C16H16N2O3, has been synthesized and characterized structurally. The two benzene rings in the molecule form a dihedral angle of 3.05(2)º. There is one strong intramolecular O-H···N hydrogen bond between the hydroxyl (O2-H2) groups and the Schiff base nitrogen (N2) atom, with the distance of d(N2-O2) = 2.593(4) Å. In the crystal structure, each molecule links other three molecules into an infinite 2D supramolecular structure by three pairs of intermolecular O1-H1···N1, C1-H1A···O1 and C16-H16B···O3 hydrogen bonds.
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- S. Akine, T. Taniguchi, W.K. Dong and T. Nabeshima, J. Org. Chem., 70, 1704 (2005).
- K. Narasaka and M. Kitamura, Eur. J. Org. Chem., 4505 (2005).
- W.K. Dong, Y.X. Sun, Y.P. Zhang, L. Li, X.N. He and X.L. Tang, Inorg. Chim. Acta, 362, 117 (2009).
- W.K. Dong, Y.X. Sun, X.N. He, J.F. Tong and J.C. Wu, Spectrochim. Acta A, 76, 476 (2010).
- W.K. Dong, X.N. He, H.B. Yan, Z.W. Lv, X. Chen, C.Y. Zhao and X.L. Tang, Polyhedron, 28, 1419 (2009).
- W.K. Dong, J.G. Duan, Y.H. Guan, J.Y. Shi and C.Y. Zhao, Inorg. Chim. Acta, 362, 1129 (2009).
- W.K. Dong, Y.X. Sun, C.Y. Zhao, X.Y. Dong and L. Xu, Polyhedron, 29, 2087 (2010).
- W.K. Dong, L. Li, C.F. Li, L. Xu and J.G. Duan, Spectrochim. Acta A, 71, 650 (2008).
- S. Akine, T. Taniguchi and T. Nabeshima, Angew. Chem. Int. Ed., 41, 4670 (2002).
- S. Akine, T. Taniguchi and T. Nabeshima, Inorg. Chem., 43, 6142 (2004).
- C. Policar, F. Lambert, M. Cesario and I. Morgenstern-badarau, Eur. J. Inorg. Chem., 12, 2201 (1999).
- D.A. Atwood and M.J. Harvey, Chem. Rev., 101, 37 (2001).
- W.K. Dong and J.G. Duan, J. Coord. Chem., 61, 781 (2007).
- H.L. Wu, X.C. Huang, J.K. Yuan, F. Kou, F. Jia, B. Liu and Y. Bai, Z. Naturforsch., 66b, 1049 (2011).
References
S. Akine, T. Taniguchi, W.K. Dong and T. Nabeshima, J. Org. Chem., 70, 1704 (2005).
K. Narasaka and M. Kitamura, Eur. J. Org. Chem., 4505 (2005).
W.K. Dong, Y.X. Sun, Y.P. Zhang, L. Li, X.N. He and X.L. Tang, Inorg. Chim. Acta, 362, 117 (2009).
W.K. Dong, Y.X. Sun, X.N. He, J.F. Tong and J.C. Wu, Spectrochim. Acta A, 76, 476 (2010).
W.K. Dong, X.N. He, H.B. Yan, Z.W. Lv, X. Chen, C.Y. Zhao and X.L. Tang, Polyhedron, 28, 1419 (2009).
W.K. Dong, J.G. Duan, Y.H. Guan, J.Y. Shi and C.Y. Zhao, Inorg. Chim. Acta, 362, 1129 (2009).
W.K. Dong, Y.X. Sun, C.Y. Zhao, X.Y. Dong and L. Xu, Polyhedron, 29, 2087 (2010).
W.K. Dong, L. Li, C.F. Li, L. Xu and J.G. Duan, Spectrochim. Acta A, 71, 650 (2008).
S. Akine, T. Taniguchi and T. Nabeshima, Angew. Chem. Int. Ed., 41, 4670 (2002).
S. Akine, T. Taniguchi and T. Nabeshima, Inorg. Chem., 43, 6142 (2004).
C. Policar, F. Lambert, M. Cesario and I. Morgenstern-badarau, Eur. J. Inorg. Chem., 12, 2201 (1999).
D.A. Atwood and M.J. Harvey, Chem. Rev., 101, 37 (2001).
W.K. Dong and J.G. Duan, J. Coord. Chem., 61, 781 (2007).
H.L. Wu, X.C. Huang, J.K. Yuan, F. Kou, F. Jia, B. Liu and Y. Bai, Z. Naturforsch., 66b, 1049 (2011).