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Vol. 25 No. 7 (2013): Vol 25 Issue 7

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Solid Phase Extraction of Three Organic Acids from Salicornia herbacea L. Using Amino Imidazolium Ionic Liquid-Based Cartridge

https://doi.org/10.14233/ajchem.2013.13732
T. Zhu
Department of Chemical Engineering, Inha University, 253 Yonghyun-Dong, Nam-Ku, Incheon 402-751, South Korea
C.H. Yoon
Department of Chemical Engineering, Inha University, 253 Yonghyun-Dong, Nam-Ku, Incheon 402-751, South Korea
K.H. Row
Department of Chemical Engineering, Inha University, 253 Yonghyun-Dong, Nam-Ku, Incheon 402-751, South Korea

Corresponding Author(s) : K.H. Row

rowkho@inha.ac.k

Asian Journal of Chemistry, Vol. 25 No. 7 (2013): Vol 25 Issue 7

Abstract

An amino imidazolium ionic liquid-based cartridge was prepared and developed for the selective extraction and determination of protocatechuic acid, caffeic acid and ferulic acid from Salicornia herbacea L. The optimum extraction condition was obtained, extraction solvent of methanol, extraction time of 1 h and ultrasonic power of 75 W. High performance liquid chromatography analysis was occurred on a C18 column with ultraviolet detection at 270 nm and the mobile phase was acetonitrile/H2O/CH3COOH (15/85/0.05, v/v/v, pH 5.0) with flow rate of 0.8 mL min-1, which showed good linearity for concentrations from 0.10-100 μg mL-1.

Keywords

Extraction Purification Organic acids Ionic liquids Salicornia herbacea L
Zhu, T., Yoon, C., & Row, K. (2013). Solid Phase Extraction of Three Organic Acids from Salicornia herbacea L. Using Amino Imidazolium Ionic Liquid-Based Cartridge. Asian Journal of Chemistry, 25(7), 3731–3734. https://doi.org/10.14233/ajchem.2013.13732
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