Copyright (c) 2013 AJC
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Rapid Analysis of Indoxacarb Residues in Vegetable by QuEChERS and LC-MS/MS
Corresponding Author(s) : Hua Shao
Asian Journal of Chemistry,
Vol. 25 No. 6 (2013): Vol 25 Issue 6
Abstract
A method for determination of indoxacarb residues in vegetable was established by QuEChERS and LC-MS/MS. The average recovery of this method was in the range from 74.2-106.5 % at the spiked level of 0.2, 0.4 and 0.8 mg/kg into samples and the RSDs were in the range from 1.9-10.2 %. The linearity of method was good from 0.05-2 mg/L and limit of quantification (LOQ) was 0.05 mg/kg. This method is simple, rapid and applicable for rapid analysis of indoxacarb residues in vegetable.
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- Y.B. Liu, M.X. Zhang and R.F. Xue, Chem. Res. Appl., 23, 1269 (2011).
- L.Z. Zhang, J.F. Zhang and D.Q. Sun, Asian J. Chem., 24, 1413 (2012).
- F. Yang, D.M. Xu, S.Y. Lu, Y.H. Lin, Z.C. Liu, K.J. Yu, J.C. Lan and G.N. Chen, J. Food Sci., 29, 520 (2008).
- L.P. Chen, J.H. Guo, E.X. Cai and W.D. Zhang, Chin. J. Pesticide Sci., 10, 443 (2008).
- S.M. Lu, X.C. Wang, J,T. Zhang and Y.E. Ma, Modern Agrochem., 6, 30 (2007).
- P.J. Zhao, Z.M. Li, L.G. Deng, J.S. Mao and S.C. Zhao, Agrochemicals, 45, 758 (2006).
- F.S. Dong, Y.Q. Zheng, X.N. Sha, S. Li and J.R. Rao, J. Agro-Environ. Sci., 24, 1027 (2005).
- J.Y. Park, J.H. Choi, A.M. Abd El-Aty, B.M. Kim, J.H. Oh, J.A. Do, K.S. Kwon, K.H.S him, O.J. Choi, S.C. Shin and J.H. Shim, Food Chem., 128, 241 (2011).
- J. Wang, D. Leung and W.J. Chow, Agric. Food Chem., 58, 5904 (2011).
- S.C. Cunha, J.O. Fernandes, A. Alves and M.B.P.P. Oliveira, J. Chromatogr. A, 1216, 119 (2009).
- M.J. Ramalhosa, P. Paíga, S. Morais, C. Delerue-Matos and M.B.P.P. Oliveira, J. Sep. Sci., 32, 3529 (2009).
- G. Stubbings and T. Bigwood, Anal. Chim. Acta, 637, 68 (2009).
- U. Koesukwiwata, K. Sanguankaewa and N. Leepipatpiboona, Anal. Chim. Acta, 626, 10 (2008).
- S.J. Lehotay, J. AOAC Int., 90, 485 (2007).
- E.J. Llorent-Martínez, J.F. García-Reyes, P. Ortega-Barrales and A. Molina-Díaz, Food Chem., 102, 676 (2007).
- S.C. Cunha, S.J. Lehotay, K. Mastovska, J.O. Fernandes, M. Beatriz and P.P. Oliveira, J. Sep. Sci., 30, 620 (2007)
References
Y.B. Liu, M.X. Zhang and R.F. Xue, Chem. Res. Appl., 23, 1269 (2011).
L.Z. Zhang, J.F. Zhang and D.Q. Sun, Asian J. Chem., 24, 1413 (2012).
F. Yang, D.M. Xu, S.Y. Lu, Y.H. Lin, Z.C. Liu, K.J. Yu, J.C. Lan and G.N. Chen, J. Food Sci., 29, 520 (2008).
L.P. Chen, J.H. Guo, E.X. Cai and W.D. Zhang, Chin. J. Pesticide Sci., 10, 443 (2008).
S.M. Lu, X.C. Wang, J,T. Zhang and Y.E. Ma, Modern Agrochem., 6, 30 (2007).
P.J. Zhao, Z.M. Li, L.G. Deng, J.S. Mao and S.C. Zhao, Agrochemicals, 45, 758 (2006).
F.S. Dong, Y.Q. Zheng, X.N. Sha, S. Li and J.R. Rao, J. Agro-Environ. Sci., 24, 1027 (2005).
J.Y. Park, J.H. Choi, A.M. Abd El-Aty, B.M. Kim, J.H. Oh, J.A. Do, K.S. Kwon, K.H.S him, O.J. Choi, S.C. Shin and J.H. Shim, Food Chem., 128, 241 (2011).
J. Wang, D. Leung and W.J. Chow, Agric. Food Chem., 58, 5904 (2011).
S.C. Cunha, J.O. Fernandes, A. Alves and M.B.P.P. Oliveira, J. Chromatogr. A, 1216, 119 (2009).
M.J. Ramalhosa, P. Paíga, S. Morais, C. Delerue-Matos and M.B.P.P. Oliveira, J. Sep. Sci., 32, 3529 (2009).
G. Stubbings and T. Bigwood, Anal. Chim. Acta, 637, 68 (2009).
U. Koesukwiwata, K. Sanguankaewa and N. Leepipatpiboona, Anal. Chim. Acta, 626, 10 (2008).
S.J. Lehotay, J. AOAC Int., 90, 485 (2007).
E.J. Llorent-Martínez, J.F. García-Reyes, P. Ortega-Barrales and A. Molina-Díaz, Food Chem., 102, 676 (2007).
S.C. Cunha, S.J. Lehotay, K. Mastovska, J.O. Fernandes, M. Beatriz and P.P. Oliveira, J. Sep. Sci., 30, 620 (2007)