Issue

Vol. 25 No. 6 (2013): Vol 25 Issue 6

Copyright (c) 2013 AJC

Creative Commons License

This work is licensed under a Creative Commons Attribution 4.0 International License.

A Facile Solvothermal Process to Synthesize MSnO3 (M = Sr, Mg) Nanoparticles Assisted by Microwave Irradiation

https://doi.org/10.14233/ajchem.2013.13594A
Chang Sung Lim
Department of Advanced Materials Science and Engineering, Hanseo University, Seosan 356-706, South Korea

Corresponding Author(s) : Chang Sung Lim

cslim@hanseo.ac.kr

Asian Journal of Chemistry, Vol. 25 No. 6 (2013): Vol 25 Issue 6

Abstract

MSnO3 (M = Sr, Mg) nanoparticles were synthesized successfully using a facile microwave solvothermal route followed by further heat-treatment. Well-crystallized SrSnO3 and MgSnO3 nanoparticles were formed after heat-treatment at 800 ºC for 3 h showing a fine and homogeneous morphology with particle sizes of 20-40 nm for SrSnO3 and 50-200 nm for MgSnO3. The synthesized SrSnO3 and MgSnO3 nanoparticles were characterized by X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscopy and transmission electron microscopy.

Keywords

SrSnO3 MgSnO3 Nanoparticles Microwave irradiation Solvothermal process
Sung Lim, C. (2013). A Facile Solvothermal Process to Synthesize MSnO3 (M = Sr, Mg) Nanoparticles Assisted by Microwave Irradiation. Asian Journal of Chemistry, 25(6), 3211–3214. https://doi.org/10.14233/ajchem.2013.13594A
Download Citation
Endnote/Zotero/Mendeley (RIS)
BibTeX
References
  1. A. Kumar, R.N.P. Choudhary, B.P. Singh and A.K. Thakur, Ceram. Int., 32, 73 (2006).
  2. A. Aydi, H. Khemakhem, A. Simon, D. Michau and R. von der Muehll, J. Alloys Comp., 484, 356 (2009).
  3. W. Yude, S. Xiaodan, L. Yanfeng, Z. Zhenlai and W. Xinghui, Solid State Electron., 44, 2009 (2000).
  4. A. Kumar, B.P. Singh, R.N.P. Choudhary and A.K. Thakur, J. Alloys Comp., 394, 292 (2005).
  5. A.M. Azad, L.J. Min and M.A. Alim, Ceram. Int., 27, 335 (2001).
  6. S. Upadhyay, O. Parkash and D. Kurmar, J. Mater. Sci. Lett., 16, 1330 (1997).
  7. M.M. Rashad and H. El-Shall, Powder Technol., 183, 161 (2008).
  8. A.M. Azad, M. Hashim, S. Baptist, A. Badri and A.U. Haq, J. Mater. Sci., 35, 5475 (2000).
  9. A.S. Deepa, S. Vidya, P.C. Manu, S. Solomon, A. John and J.K. Thomas, J. Alloys Comp., 509, 1830 (2010).
  10. C. Fan, X. Song, H. Yu, Z. Yin, H. Xu, G. Cao, D. Zheng and S. Sun, Mater. Lett., 61, 1591 (2007).
  11. R. Koeferstein, L. Jaeger, M. Zenker and S.G. Ebbinghaus, J. Eur. Ceram. Soc., 29, 2324 (2009).
  12. J. Bohnemann, R. Libanori, M.L. Moreira and E. Longo, Chem. Eng. J., 155, 905 (2009).
  13. C.P. Udawatte, M. Kakihana and M. Yoshimura, Solid State Ionics, 128, 217 (2000).
  14. B. Ramdas and R. Vijayaraghavan, Bull. Mater. Sci., 33, 75 (2010).
  15. M.C.F. Alves, S. Boursicot, S. Ollivier, V. Bouquet, S. Deputier, A. Perrin, I.T. Weber, A.G. Souza, I.M.G. Santos and M. Guilloux-Viry, Thin Solid Films, 519, 614 (2010).
  16. A.M. Azad, L.L.W. Shyan, T.Y. Pang and C.H. Nee, Ceramic Int., 26, 685 (2000).
  17. A.M. Azad, L.L.W. Shyan and P.T. Yen, J. Alloys Comp., 282, 109 (1999).
  18. S. Das, A.K. Mukhopadhyay, S. Datta and D. Basu, Bull. Mater. Sci., 32, 1 (2009).
  19. K.P.F. Siqueira, R.L. Moreira, M. Valadares and A. Dias, J. Mater. Sci., 45, 6083 (2010).
  20. J.C. Sczancoski, L.S. Cavalcante, M.R. Joya, J.A. Varela, P.S. Pizani and E. Longo, Chem. Eng. J., 140, 632 (2008).
  21. J. Bi, L. Wu, Z. Li, Z. Ding, X. Wang and X. Fu, J. Alloys Comp., 480, 684 (2009).
  22. T. Thongtem, A. Phuruangrant and S. Thongtom, Curr. Appl. Phy., 8, 189 (2008).
Read More
Author biographies is not available.
Download
PDF
Statistic
Read Counter : 1 Download : 1