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Vol. 25 No. 5 (2013): Vol 25 Issue 5

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Synthesis and Characterization of Uniform ZnS Sphere Crystalline by Using a Zinc Coordination Complex as Precursor

https://doi.org/10.14233/ajchem.2013.13486
Weihua Chen
College of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou 450001, Henan Province, P.R. China
Qi Ding
College of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou 450001, Henan Province, P.R. China ; Institute of Surface Micro and Nano Materials, Xuchang University, Xuchang 461000, Henan Province, P.R. China
Shanshan Guo
Institute of Surface Micro and Nano Materials, Xuchang University, Xuchang 461000, Henan Province, P.R. China
Yuanfang Chen
College of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou 450001, Henan Province, P.R. China ; Institute of Surface Micro and Nano Materials, Xuchang University, Xuchang 461000, Henan Province, P.R. China
Zhen Li
College of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou 450001, Henan Province, P.R. China ; Institute of Surface Micro and Nano Materials, Xuchang University, Xuchang 461000, Henan Province, P.R. China
Liwei Mi
Institute of Surface Micro and Nano Materials, Xuchang University, Xuchang 461000, Henan Province, P.R. China
Zhi Zheng
Institute of Surface Micro and Nano Materials, Xuchang University, Xuchang 461000, Henan Province, P.R. China

Corresponding Author(s) : Qi Ding

Asian Journal of Chemistry, Vol. 25 No. 5 (2013): Vol 25 Issue 5

Abstract

Without using any surfactant or chemical assistant, we just use [Zn(phen)2(H2O)2]2L·6H2O complex as precursor to react with sulfourea as sulphur source under moderate conditions. Uniform ZnS sphere crystalline has been successfully synthesized via a convenient solvothermal method, in which ethanediol and ethanediamine were utilized as mixed solvent. The composition and morphology of as-prepared samples were, respectively characterized by X-ray diffraction and scanning electron microscope. Also the photoluminescence property of the as-synthesized ZnS materials was studied in this work.

Keywords

ZnS Crystalline sphere Photoluminescence
Chen, W., Ding, Q., Guo, S., Chen, Y., Li, Z., Mi, L., & Zheng, Z. (2012). Synthesis and Characterization of Uniform ZnS Sphere Crystalline by Using a Zinc Coordination Complex as Precursor. Asian Journal of Chemistry, 25(5), 2583–2585. https://doi.org/10.14233/ajchem.2013.13486
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