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Vol. 25 No. 5 (2013): Vol 25 Issue 5

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A Solvothermal Process to Synthesize Barium Metastannate Nanoparticles Assisted by Microwave Irradiation

https://doi.org/10.14233/ajchem.2013.1CSLim
Chang Sung Lim
Department of Advanced Materials Science & Engineering, Hanseo University, Seosan 356-706, South Korea

Corresponding Author(s) : Chang Sung Lim

cslim@hanseo.ac.kr

Asian Journal of Chemistry, Vol. 25 No. 5 (2013): Vol 25 Issue 5

Abstract

Barium metatstannate (BaSnO3) nanoparticles were synthesized successfully using a facile microwave solvothermal route followed by further heat-treatment. Well-crystallized BaSnO3 nanoparticles were formed after heat-treatment at 800 ºC for 3 h showing a fine and homogeneous morphology with particle sizes of 60-80 nm. The synthesized BaSnO3 nanoparticles were characterized by X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscopy and transmission electron microscopy.

Keywords

Barium metatstannate Microwave irradiation Solvothermal process Nanoparticles
Sung Lim, C. (2012). A Solvothermal Process to Synthesize Barium Metastannate Nanoparticles Assisted by Microwave Irradiation. Asian Journal of Chemistry, 25(5), 2363–2365. https://doi.org/10.14233/ajchem.2013.1CSLim
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References
  1. A. Kumar, R.N.P. Choudhary, B.P. Singh and A.K. Thakur, Ceram. Int., 32, 73 (2006).
  2. A. Aydi, H. Khemakhem, A. Simon, D. Michau and R. von der Muehll, J. Alloys Comp., 484, 356 (2009).
  3. W. Yude, S. Xiaodan, L. Yanfeng, Z. Zhenlai and W. Xinghui, Solid State Elect., 44, 2009 (2000).
  4. A. Kumar, B.P. Singh, R.N.P. Choudhary and A.K. Thakur, J. Alloys Comp., 394, 292 (2005).
  5. A.M. Azad, L.J. Min and M.A. Alim, Ceram. Int., 27, 335 (2001).
  6. S. Upadhyay, O. Parkash and D. Kurmar, J. Mater. Sci. Lett., 16, 1330 (1997).
  7. M.M. Rashad and H. El-Shall, Powder Technol., 183, 161 (2008).
  8. A. M. Azad, M. Hashim, S. Baptist, A. Badri and A.U. Haq, J. Mater. Sci., 35, 5475 (2000).
  9. A.S. Deepa, S. Vidya, P.C. Manu, S. Solomon,A. John and J.K. Thomas, J. Alloys Comp., 509, 1830 (2010).
  10. C. Fan, X. Song, H. Yu, Z. Yin, H. Xu, G. Cao, D. Zheng and S. Sun, Mater. Lett., 61, 1591 (2007).
  11. R. Koeferstein, L. Jaeger, M. Zenker and S.G. Ebbinghaus, J. Eur. Ceram. Soc., 29, 2324 (2009).
  12. J. Bohnemann, R. Libanori, M.L. Moreira and E. Longo, Chem. Eng. J., 155, 905 (2009).
  13. C.P. Udawatte, M. Kakihana and M. Yoshimura, Solid State Ionics, 128, 217 (2000).
  14. B. Ramdas and R. Vijayaraghavan, Bull. Mater. Sci., 33, 75 (2010).
  15. M.C.F. Alves, S. Boursicot, S. Ollivier, V. Bouquet, S. Deputier, A. Perrin, I.T. Weber, A.G. Souza, I.M.G. Santos and M. Guilloux-Viry, Thin Solid Films, 519, 614 (2010).
  16. A.M. Azad, L.L.W.Shyan, T.Y. Pang and C.H. Nee, Ceram. Int., 26, 685 (2000).
  17. A.M. Azad, L.L.W.Shyan and P.T. Yen, J. Alloys Comp., 282, 109 (1999).
  18. S. Das, A.K. Mukhopadhyay, S. Datta and D. Basu, Bull. Mater. Sci., 32, 1 (2009).
  19. K.P.F. Siqueira, R.L. Moreira, M. Valadares and A. Dias, J. Mater. Sci., 45, 6083 (2010).
  20. J.C. Sczancoski, L.S. Cavalcante, M.R. Joya, J.a. Varela, P.S. Pizani and E. Longo, Chem. Eng. J., 140, 632 (2008).
  21. J. Bi, L. Wu, Z. Li, Z. Ding, X. Wang and X. Fu, J. Alloys Comp., 480, 684 (2009).
  22. T. Thongtem, A. Phuruangrant and S. Thongtom, Curr. Appl. Phys., 8, 189 (2008).
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