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Preparation of Aminolignin from Paper Mill Sludge and Its Discolouring Flocculant Performance
Corresponding Author(s) : Xiaofeng Li
Asian Journal of Chemistry,
Vol. 25 No. 3 (2013): Vol 25 Issue 3
Abstract
Lignin was extracted from paper mill sludge by the process of alkali dissolving and acid precipitating. Then a new kind of aminolignin discolouring flocculant was prepared with the lignin and dimethylamine epoxypropylamine (named as epoxy amimes monomer) as the raw materials and NaOH as the catalyst. The influencing factors such as the ratio of reactants, activation time, reaction temperature and reaction time on the preparation of aminolignin were investigated so as to optimize the reaction conditions. The products were characterized by using Fourier transform infrared spectroscopy. The possibility of aminolignin as a flocculant was examined by using simulated waste water of several dyes and the results show that it has a satisfactory decolourizing ability, which can afford a new method of effectively utilizing lignin and tackling paper mill sludge.
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- NCASI Technical Bulletin, Solid Waste Management Practices in the U.S. Paper Industry 1995, NCASI Technical Bulletin No. 793 (1999).
- NCASI Technical Bulletin, Progress in Reducing Water Use and Waste Water Loads in the US Paper Industry, NCASI Technical Bulletin No. 603 (1991).
- L. Beyer, R. Frund and K. Mueller, Sci. Total. Environ., 197, 127 (1997).
- A. Battaglia, N. Calace and E. Nardi, Microchem. J., 75, 97 (2003).
- R. Baziramakenga and R.R. Simard, Compost. Sci. Util., 9, 115 (2001).
- S.Y. Lin and C.W. Dence, Methods in Lignin Chemistry, Springer, Berlin (1992).
- V.G. Verkhanovsky, A.F. Nikiforov and V.V. Pushkarev, Khim. Tekhnol. Vody., 4, 29 (1982).
- M.G. Morekhin, Khim. Drev., 4, 68 (1978).
- B.Y. Wu and G. Yu, Environ. Prot. Chem. Ind., 17, 268 (1997).
- G.Z. Fang, C.L. Wu and Z.Q. Song, China Pulp Paper, 22, 24 (2003).
- M. Yousuf, A. Mollah and P. Palta, Cement Concrete. Res., 25, 671 (1995).
- H.L. Hergert, J. Org. Chem., 25, 405 (1960).
References
NCASI Technical Bulletin, Solid Waste Management Practices in the U.S. Paper Industry 1995, NCASI Technical Bulletin No. 793 (1999).
NCASI Technical Bulletin, Progress in Reducing Water Use and Waste Water Loads in the US Paper Industry, NCASI Technical Bulletin No. 603 (1991).
L. Beyer, R. Frund and K. Mueller, Sci. Total. Environ., 197, 127 (1997).
A. Battaglia, N. Calace and E. Nardi, Microchem. J., 75, 97 (2003).
R. Baziramakenga and R.R. Simard, Compost. Sci. Util., 9, 115 (2001).
S.Y. Lin and C.W. Dence, Methods in Lignin Chemistry, Springer, Berlin (1992).
V.G. Verkhanovsky, A.F. Nikiforov and V.V. Pushkarev, Khim. Tekhnol. Vody., 4, 29 (1982).
M.G. Morekhin, Khim. Drev., 4, 68 (1978).
B.Y. Wu and G. Yu, Environ. Prot. Chem. Ind., 17, 268 (1997).
G.Z. Fang, C.L. Wu and Z.Q. Song, China Pulp Paper, 22, 24 (2003).
M. Yousuf, A. Mollah and P. Palta, Cement Concrete. Res., 25, 671 (1995).
H.L. Hergert, J. Org. Chem., 25, 405 (1960).