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Separation of Three Monosaccharides Using Amino Ionic Liquid-Based Silica
Corresponding Author(s) : Kyung Ho Row
Asian Journal of Chemistry,
Vol. 27 No. 7 (2015): Vol 27 Issue 7, 2015
Abstract
An amino-imidazolium ionic liquid was coated on commercial silica and the resulting ionic liquid-based particles were used as special sorbents of solid-phase. The mobile phase of acetonitrile/water from 90:10 to 70:30 (v/v) could separate the monosaccharides. Good linearity was obtained from 1 to 10 mg/mL with a RSD < 3.4 %. The sorbent produced reproducible results and performed stably, highlighting its potential as a separation material.
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- G. Karlsson, S. Winge and H. Sandberg, J. Chromatogr. A, 1092, 246 (2005); doi:10.1016/j.chroma.2005.08.025.
- M. Taverna, A. Baillet, R. Werner and D. Bailocq-Ferrie, J. Chromatogr. A, 558, 105 (1991); doi:10.1016/0021-9673(91)80115-W.
- M.T. Sancho, S. Muniategui, J. López, J. Simal and J.F. Huidobro, Anal. Bromatology, 42, 71 (1999).
- K. Mopper, C.A. Schultz, L. Chevolot, C. Germain, R. Revuelta and R. Dawson, Environ. Sci. Technol., 26, 133 (1992); doi:10.1021/es00025a014.
- Z. Bubnik, V. Pour, A. Gruberova, H. Starhova, A. Hinkova and P. Kadlec, J. Food Eng., 61, 509 (2004); doi:10.1016/S0260-8774(03)00221-8.
- K.N. Lee, Korean J. Chem. Eng., 20, 532 (2003); doi:10.1007/BF02705561.
- K. Pyrzyñska and M. Trojanowicz, Crit. Rev. Anal. Chem., 29, 313 (1999); doi:10.1080/10408349891199329.
- Y.Q. Cai, G.B. Jiang, J.F. Liu and Q.X. Zhou, Anal. Chem., 75, 2517 (2003); doi:10.1021/ac0263566.
- S. Pandey, Anal. Chim. Acta, 556, 38 (2006); doi:10.1016/j.aca.2005.06.038.
- M.J. Kim, M.Y. Choi, J.K. Lee and Y. Ahn, J. Mol. Catal. B, 26, 115 (2003); doi:10.1016/j.molcatb.2003.04.001.
- W. Bi, M. Tian and K.H. Row, J. Sep. Sci., 33, 1739 (2010); doi:10.1002/jssc.200900835.
- M. Tian, H. Yan and K.H. Row, J. Chromatogr. B Analyt. Technol. Biomed. Life Sci., 877, 738 (2009); doi:10.1016/j.jchromb.2009.02.012.
References
G. Karlsson, S. Winge and H. Sandberg, J. Chromatogr. A, 1092, 246 (2005); doi:10.1016/j.chroma.2005.08.025.
M. Taverna, A. Baillet, R. Werner and D. Bailocq-Ferrie, J. Chromatogr. A, 558, 105 (1991); doi:10.1016/0021-9673(91)80115-W.
M.T. Sancho, S. Muniategui, J. López, J. Simal and J.F. Huidobro, Anal. Bromatology, 42, 71 (1999).
K. Mopper, C.A. Schultz, L. Chevolot, C. Germain, R. Revuelta and R. Dawson, Environ. Sci. Technol., 26, 133 (1992); doi:10.1021/es00025a014.
Z. Bubnik, V. Pour, A. Gruberova, H. Starhova, A. Hinkova and P. Kadlec, J. Food Eng., 61, 509 (2004); doi:10.1016/S0260-8774(03)00221-8.
K.N. Lee, Korean J. Chem. Eng., 20, 532 (2003); doi:10.1007/BF02705561.
K. Pyrzyñska and M. Trojanowicz, Crit. Rev. Anal. Chem., 29, 313 (1999); doi:10.1080/10408349891199329.
Y.Q. Cai, G.B. Jiang, J.F. Liu and Q.X. Zhou, Anal. Chem., 75, 2517 (2003); doi:10.1021/ac0263566.
S. Pandey, Anal. Chim. Acta, 556, 38 (2006); doi:10.1016/j.aca.2005.06.038.
M.J. Kim, M.Y. Choi, J.K. Lee and Y. Ahn, J. Mol. Catal. B, 26, 115 (2003); doi:10.1016/j.molcatb.2003.04.001.
W. Bi, M. Tian and K.H. Row, J. Sep. Sci., 33, 1739 (2010); doi:10.1002/jssc.200900835.
M. Tian, H. Yan and K.H. Row, J. Chromatogr. B Analyt. Technol. Biomed. Life Sci., 877, 738 (2009); doi:10.1016/j.jchromb.2009.02.012.