Analysis of Ferulic Acid, Rosemarinic Acid and Caffeic Acid in Rosmarnus officinalis L. by Capillary Zone Electrophoresis

Y. Zhang; C. Kong; Y. Liu

doi:10.14233/ajchem.2015.17894

Issue

Vol. 27 No. 6 (2015): Vol 27 Issue 6

Issue Published : March 17, 2015

This work is licensed under a Creative Commons Attribution 4.0 International License.

Analysis of Ferulic Acid, Rosemarinic Acid and Caffeic Acid in Rosmarnus officinalis L. by Capillary Zone Electrophoresis

https://doi.org/10.14233/ajchem.2015.17894

Y. Zhang

Jinan Infectious Disease Hospital, Jingshi Road 22029, Jinan 250021, Shandong Province, P.R. China

C. Kong

Analysis and Testing Centre, Dezhou University, University West Road 566, Dezhou 253023, P.R. China

Y. Liu

Department of Pharmaceutics, Shandong Cancer Hospital and Institute, Shandong Academy of Medical Sciences, Jiyan Road 440, Jinan 250117, Shandong Province, P.R. China

Corresponding Author(s) : Y. Liu

yuguoliu140426@163.com

Asian Journal of Chemistry, Vol. 27 No. 6 (2015): Vol 27 Issue 6
Article Published : March 18, 2015

Abstract

A capillary zone electrophoretic method has been developed to determine ferulic acid, rosemarinic acid and caffeic acid in Rosmarnus officinalis L. The effects of buffer pH and concentration and applied voltage on separation were investigated. The optimum electrophoretic conditions are as follows: 40 mmol L^-1 Borax-40 mmol L^-1 NaH₂PO₄ (pH 8.0) as the running buffer and applied voltage of 25 kV. Under the optimized conditions, a good linearity between the peak area and the concentration was found in the ranges of 10-200, 20-400 and 20-400 mg mL^-1 for rosemarinic acid, ferulic acid and caffeic acid, respetively. The relative standard deviation in migration time and peak area was 0.68 and 1.37 % for ferulic acid, 0.51 and 1.98 % for rosemarinic acid, 0.76 and 1.86 % for caffeic acid. The detection limits of the three analytes ranged from 3.1 to 5.6 mg mL^-1. The recoveries of three analytes ranged between 92.5 and 102.5 %.

Keywords

Capillary zone electrophoresis Ferulic acid Rosemarinic acid Caffeic acid

Zhang, Y., Kong, C., & Liu, Y. (2015). Analysis of Ferulic Acid, Rosemarinic Acid and Caffeic Acid in Rosmarnus officinalis L. by Capillary Zone Electrophoresis. Asian Journal of Chemistry, 27(6), 2154–2156. https://doi.org/10.14233/ajchem.2015.17894

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References

S. Zou and X. Sun, China Food Additives, 25, 223 (2010).

P. Zou, X. Lu and C. Hu, Ion Exchange Adsorption, 27, 304 (2011).

H. Wang and Z.Q. Zhang, Chinese J. Exp. Trad. Medical Formulae, 17, 116 (2013).

X. Dai and R.G. Compton, J. Anal. Sci., 22, 567 (2006); doi:10.2116/analsci.22.567.

S. Cao, Y.G. Zu and L. Zhang, Chinese J. Food Sci., 33, 196 (2012).

Z. Chen, Z. Lin, L. Zhang, Y. Cai and L. Zhang, Analyst, 137, 1723 (2012); doi:10.1039/c2an16313f.

L. Han, Q.X. Chen, X.H. Liu, Y.Z. Zhou, J.S. Li and B.C. Cai, Chinese J. Pharm. Anal., 33, 1525 (2013).

T.N. Wu, C.Z. Yu, R. Li, X.M. Sun and J. Li, Chin. Tradit. Herbal Drugs, 44, 2404 (2013).

H. Xu, X.H. Liu, X.S. Fu, L. Chen, J.S. Li, B.C. Cai and Y.Z. Zhou, Chinese Pharm. J., 47, 1661 (2012).

X. Guo, Q. Wang and W. Liu, China J. Chinese Med., 28, 69 (2013).

S.Y. Gao, L. Wang, T. Fan and H. Li, Chem. Anal., 48, 392 (2012).

Y. Lu, D. Wang and Q. Yao, Pak. J. Pharm. Sci., 27, 487 (2014).

R.J. Jing, X.Y. Jiang, S.R. Hou, X.J. Li and Z.B. Yuan, Chinese J. Anal. Chem., 35, 1187 (2007).

S. Zhang, S. Dong, L. Chi, P. He, Q. Wang and Y. Fang, Talanta, 76, 780 (2008); doi:10.1016/j.talanta.2008.04.025.

Y. Lu, C. Jia, Q. Yao, H. Zhong and M.C. Breadmore, J. Chromatogr. A, 1319, 160 (2013); doi:10.1016/j.chroma.2013.10.014.

Z.Y. Ren, Y. Zhang and Y.P. Shi, Talanta, 78, 959 (2009); doi:10.1016/j.talanta.2009.01.006.

H. Zhong, Q. Yao, M.C. Breadmore, Y. Li and Y. Lu, Analyst, 136, 4486 (2011); doi:10.1039/c1an15277g.

Q. Shi, L. Sui and Y. Lu, Pak. J. Pharm. Sci., 26, 1131 (2013).

J. Zhu, K. Yu, X. Chen and Z. Hu, J. Chromatogr. A, 1166, 191 (2007); doi:10.1016/j.chroma.2007.08.018.

J. Li, X. Liu, B. Cai, Y. Zhang, X. Fu and D. Yin, Chinese J. Chromatogr., 28, 402 (2012); doi:10.3724/SP.J.1123.2010.00402.

Y. Deng and J. He, High Performance Capillary Electrophoresis, Academic Press, Beijing, p. 26 (1995).

Issue

Vol. 27 No. 6 (2015): Vol 27 Issue 6

Analysis of Ferulic Acid, Rosemarinic Acid and Caffeic Acid in Rosmarnus officinalis L. by Capillary Zone Electrophoresis

Corresponding Author(s) : Y. Liu

Abstract

Keywords

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