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Vol. 27 No. 3 (2015): Vol 27 Issue 3

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Analysis of Alkali Chemical Constituents from Holotrichia diomphalia Bates by GC-MS

https://doi.org/10.14233/ajchem.2015.17139
Yuan-Yuan Liu
Department of Natural Medicine, School of Pharmacy, Fourth Military Medical University, Xi'an 710032, P.R. China
Ya Zhang
Department of Natural Medicine, School of Pharmacy, Fourth Military Medical University, Xi'an 710032, P.R. China
Wei Cao
Department of Natural Medicine, School of Pharmacy, Fourth Military Medical University, Xi'an 710032, P.R. China
Si-Wang Wang
Department of Natural Medicine, School of Pharmacy, Fourth Military Medical University, Xi'an 710032, P.R. China

Corresponding Author(s) : Wei Cao

caowei@fmmu.edu.cn

Asian Journal of Chemistry, Vol. 27 No. 3 (2015): Vol 27 Issue 3

Abstract

The alkali chemical constituents were obtained after 95 % alcohol extraction, condensation, acidification and extraction with chloroform from Holotrichia diomphalia bates. The chemical constituents were analysis by GC-MS and their relative contents were calculated by area normalization method. Seventy nine components were identified and 14 nitrogen-containing compounds were found by analysis with GC-MS. The main of nitrogen-containing compounds including 2-piperidinone, 4-methyl-5-thiazoleethanol, 2-[4-(2-hydroxy-phenyl)-thiazol-2-yl]-5-phenyl-penta-2,4-dienenitrile, 4,4'-bis(dimethylamino)benzhydrol, 5a-pregnane-3,20a-dio,14a,18a-[4-methyl-3-oxo-(1-oxa-4-azabutane-1,4-diyl)]-diacetate, 5,10-diethoxy-2,3,7,8-tetrahydro-1H,6H-dipyrrolo[1,2-a:1',2'-d]pyrazine; 9H-pyrido[3,4-b]indole, 5-aminovaleric acid, Ile-ser, 4,4-dimethylazetidin-2-one and 1-methyl-2-piperidinone. The novel findings of the present study provide a scientific basis for the further development and utilization of Holotrichia diomphalia bates.

Keywords

Holotrichia diomphalia bates Chemical constituents Alkaloids GC-MS
Liu, Y.-Y., Zhang, Y., Cao, W., & Wang, S.-W. (2015). Analysis of Alkali Chemical Constituents from Holotrichia diomphalia Bates by GC-MS. Asian Journal of Chemistry, 27(3), 849–859. https://doi.org/10.14233/ajchem.2015.17139
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