Copyright (c) 2014 AJC
This work is licensed under a Creative Commons Attribution 4.0 International License.
Online Detection for Notoginseng Ingredients in Macroporous Resin Purification Process Using Near Infrared Technology in Combination with Partial Least Squares
Corresponding Author(s) : C.J. Wu
Asian Journal of Chemistry,
Vol. 26 No. 3 (2014): Vol 26 Issue 3
Abstract
In this work, we have developed new prediction models for online detection of notoginseng ingredients (Ginsenoside Rg1, Ginsenoside Re and Notoginsenoside R1) during the macroporous resin purification process by near infrared technology in combination with partial least squares. In the experiments, calibration models were generated based on min max normalization (MMN) for Ginsenoside Rg1, Ginsenoside Re and First derivative + vector normalization for notoginsenoside R1. Finally, the root mean square errors of cross-validation (RMSECV) of Rg1 Re and R1 were 0.952, 0.106, 0.214 mg/mL, respectively; the root mean square errors of prediction (RMSEP) were 1.132, 0.121 and 0.381 mg/mL, respectively; the correlation coefficients (R2) of cross-validation were 0.9858, 0.9787 and 0.9793, respectively; the correlation coefficients (R2) of prediction were 0.9884, 0.9898 and 0.9709, respectively. In conclusion, this research indicated that NIR technology can be used for rapid analysis and online quality control of traditional Chinese medicine (TCM) in production process..png)
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- Y. Jiang, B. David, P.F. Tu and Y. Barbin, Anal. Chim. Acta, 657, 9 (2010); doi:10.1016/j.aca.2009.10.024.
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- J.A. Cayuela, Postharvest Biol. Technol., 47, 75 (2008); doi:10.1016/j.postharvbio.2007.06.005.
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- Q.S. Chen, J.W. Zhao, S. Chaitep and Z.M. Guo, Food Chem., 113, 1272 (2009); doi:10.1016/j.foodchem.2008.08.042.
- M. Blanco, R.G. Bañó and E. Bertran, Talanta, 56, 203 (2002); doi:10.1016/S0039-9140(01)00559-8.
- Y. Chen, M.Y. Xie, Y. Yan, S.B. Zhu, S.P. Nie, C. Li, Y.X. Wang and X.F. Gong, Anal. Chim. Acta, 618, 121 (2008); doi:10.1016/j.aca.2008.04.055.
- D. Wu, J.Y. Chen, B.Y. Lu, L.N. Xiong, Y. He and Y. Zhang, Food Chem., 135, 2147 (2012); doi:10.1016/j.foodchem.2012.07.011.
- G. Reich, Adv. Drug Deliv. Rev., 57, 1109 (2005); doi:10.1016/j.addr.2005.01.020.
- J. Luypaert, D.L. Massart and Y. Vander Heyden, Talanta, 72, 865 (2007); doi:10.1016/j.talanta.2006.12.023.
- W.L. Li, L.H. Xing, Y. Cai and H.B. Qu, Vib. Spectrosc., 55, 58 (2011); doi:10.1016/j.vibspec.2010.07.004.
- H. Winning, N. Viereck, T. Salomonsen, J. Larsen and S.B. Engelsen, Carbohydr. Res., 344, 1833 (2009); doi:10.1016/j.carres.2008.10.015.
- Y. Roggo, P. Chalus, L. Maurer, C. Lema-Martinez, A. Edmond and N. Jent, J. Pharm. Biomed. Anal., 44, 683 (2007); doi:10.1016/j.jpba.2007.03.023.
References
Y. Jiang, B. David, P.F. Tu and Y. Barbin, Anal. Chim. Acta, 657, 9 (2010); doi:10.1016/j.aca.2009.10.024.
J. Xue, C. Wu, L. Wang, S. Jiang, G. Huang, J. Zhang, S. Wen and L. Ye, Food Chem., 126, 725 (2011); doi:10.1016/j.foodchem.2010.11.036.
Q.F. Xu, X.L. Fang and D.F. Chen, J. Ethnopharmacol., 84, 187 (2003); doi:10.1016/S0378-8741(02)00317-3.
C.C. Bai, S.Y. Han, X.Y. Chai, Y. Jiang, P. Li and P.F. Tu, J. Liq. Chromatogr. Rel. Technol., 32, 242 (2008); doi:10.1080/10826070802603187.
W. Luo, J. Wu, X.K. Wang, X. Lin and H. Li, Anal. Methods, 5, 1337 (2013); doi:10.1039/c2ay26260f.
J.A. Cayuela, Postharvest Biol. Technol., 47, 75 (2008); doi:10.1016/j.postharvbio.2007.06.005.
J.W. Zhao, Q.S. Chen, X.Y. Huang and C.H. Fang, J. Pharm. Biomed. Anal., 41, 1198 (2006); doi:10.1016/j.jpba.2006.02.053.
Q.S. Chen, J.W. Zhao, S. Chaitep and Z.M. Guo, Food Chem., 113, 1272 (2009); doi:10.1016/j.foodchem.2008.08.042.
M. Blanco, R.G. Bañó and E. Bertran, Talanta, 56, 203 (2002); doi:10.1016/S0039-9140(01)00559-8.
Y. Chen, M.Y. Xie, Y. Yan, S.B. Zhu, S.P. Nie, C. Li, Y.X. Wang and X.F. Gong, Anal. Chim. Acta, 618, 121 (2008); doi:10.1016/j.aca.2008.04.055.
D. Wu, J.Y. Chen, B.Y. Lu, L.N. Xiong, Y. He and Y. Zhang, Food Chem., 135, 2147 (2012); doi:10.1016/j.foodchem.2012.07.011.
G. Reich, Adv. Drug Deliv. Rev., 57, 1109 (2005); doi:10.1016/j.addr.2005.01.020.
J. Luypaert, D.L. Massart and Y. Vander Heyden, Talanta, 72, 865 (2007); doi:10.1016/j.talanta.2006.12.023.
W.L. Li, L.H. Xing, Y. Cai and H.B. Qu, Vib. Spectrosc., 55, 58 (2011); doi:10.1016/j.vibspec.2010.07.004.
H. Winning, N. Viereck, T. Salomonsen, J. Larsen and S.B. Engelsen, Carbohydr. Res., 344, 1833 (2009); doi:10.1016/j.carres.2008.10.015.
Y. Roggo, P. Chalus, L. Maurer, C. Lema-Martinez, A. Edmond and N. Jent, J. Pharm. Biomed. Anal., 44, 683 (2007); doi:10.1016/j.jpba.2007.03.023.
