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Vol. 26 No. 6 (2014): Vol 26 Issue 6

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Preparation, Micromorphology and Optical Properties of SPION/BaWO4:Er3+, Yb3+ Composites via Cyclic Microwave-Assisted Metathetic Route

https://doi.org/10.14233/ajchem.2014.16405
Chang Sung Lim
Department of Advanced Materials Science & Engineering, Hanseo University, Seosan 356-706, Republic of Korea

Corresponding Author(s) : Chang Sung Lim

cslim@hanseo.ac.kr

Asian Journal of Chemistry, Vol. 26 No. 6 (2014): Vol 26 Issue 6

Abstract

Superparamagnetic iron oxide nanoparticles (SPIONs) incorporated Er3+/Yb3+ co-doped BaWO4 (SPION/BaWO4:Er3+/Yb3+) composites were successfully prepared via cyclic microwave-assisted metathetic route. The micromorphology exhibited a well-defined and homogeneous morphology with sizes of 1-2 μm for the BaWO4:Er3+/Yb3+ particles and 0.1-0.5 μm for the Fe3O4 particles, respectively. The Fe3O4 particles were self-preferentially crystallized and immobilized on the surface of BaWO4:Er3+/Yb3+ particles. The synthesized SPION/BaWO4:Er3+/Yb3+ composites were characterized by X-ray diffraction, scanning electron microscopy and energy-dispersive X-ray spectroscopy. Other optical properties were also examined by using photoluminescence emission data and Raman spectroscopy.

Keywords

Micromorphology Optical properties SPIONs BaMoO4:Er3 /Yb3 Cyclic microwave-assisted metathetic route
Sung Lim, C. (2014). Preparation, Micromorphology and Optical Properties of SPION/BaWO4:Er3+, Yb3+ Composites via Cyclic Microwave-Assisted Metathetic Route. Asian Journal of Chemistry, 26(6), 1857–1860. https://doi.org/10.14233/ajchem.2014.16405
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