Facile Synthesis of Mesoporous Silica for Separation of Coalbed Methane

Lusheng Yang; Zhenghe Liu; Wenxiang Zheng

doi:10.14233/ajchem.2014.16124

Issue

Vol. 26 No. 12 (2014): Vol 26 Issue 12

Issue Published : June 5, 2014

This work is licensed under a Creative Commons Attribution 4.0 International License.

Facile Synthesis of Mesoporous Silica for Separation of Coalbed Methane

https://doi.org/10.14233/ajchem.2014.16124

Lusheng Yang

Institute of Mining Technology, Taiyuan University of Technology, Taiyuan 030024, Shanxi, P.R. China ;College of Arts and Science, Shanxi Agricultural University, Taigu 030801, Shanxi, P.R. China

Zhenghe Liu

Institute of Mining Technology, Taiyuan University of Technology, Taiyuan 030024, Shanxi, P.R. China

Wenxiang Zheng

Institute of Mining Technology, Taiyuan University of Technology, Taiyuan 030024, Shanxi, P.R. China; Inner Mongolia University of Science and Technology, School of Coal Science and Engineering, Baotou 014047, Neimeng, P.R. China

Corresponding Author(s) : Zhenghe Liu

lzhyls2013@126.com

Asian Journal of Chemistry, Vol. 26 No. 12 (2014): Vol 26 Issue 12
Article Published : June 5, 2014

Abstract

Mesoporous silica as potential adsorbent for separation of coalbed methane was prepared by using one anionic surfactant containing poly(ethylene oxide) group as template in a facile method. Small angle XRD, TEM and N₂ adsorption-desorption isotherms were carried out to confirm the final product. From the results of characterizations, the diameters of the spherical particles have a narrow range of 100-130 nm and the mesoporous sizes are in 2-4 nm. In addition, the average pore size is 2.98 nm, the BET surface area is 572 m²/g and the pore volume is 0.4150 cm³/g.

Keywords

Mesoporous silica Separation Coalbed methane

Yang, L., Liu, Z., & Zheng, W. (2014). Facile Synthesis of Mesoporous Silica for Separation of Coalbed Methane. Asian Journal of Chemistry, 26(12), 3504–3506. https://doi.org/10.14233/ajchem.2014.16124

Download Citation

References

J.S. Beck, J.C. Vartuli, W.J. Roth, M.E. Leonowicz, C.T. Kresge, K.D. Schmitt, C.T.W. Chu, D.H. Olson and E.W. Sheppard, J. Am. Chem. Soc., 114, 10834 (1992); doi:10.1021/ja00053a020.
T.-L. Chew, A.L. Ahmad and S. Bhatia, Adv. Colloid Interface Sci., 153, 43 (2010); doi:10.1016/j.cis.2009.12.001.
J.H. Clark, D.J. Macquarrie and S.J. Tavener, Dalton Trans., 4297 (2006); doi:10.1039/b607831a.
I.I. Slowing, J.L. Vivero-Escoto, C.-W. Wu and V.S.-Y. Lin, Adv. Drug Deliv. Rev., 60, 1278 (2008); doi:10.1016/j.addr.2008.03.012.
J.L. Vivero-Escoto, I.I. Slowing, B.G. Trewyn and V.S.-Y. Lin, Small, 6, 1952 (2010); doi:10.1002/smll.200901789.
G. Garnweitner and M. Niederberger, J. Mater. Chem., 18, 1171 (2008); doi:10.1039/b713775c.
Z. Chen, T.L. Greaves, R.A. Caruso and C.J. Drummond, J. Mater. Chem., 22, 10069 (2012); doi:10.1039/c2jm30708a.
Y. Wan and D. Zhao, Chem. Rev., 107, 2821 (2007); doi:10.1021/cr068020s.
D. Zhao, J. Feng, Q. Huo, N. Melosh, G.H. Fredrickson, B.F. Chmelka and G.D. Stucky, Science, 279, 548 (1998); doi:10.1126/science.279.5350.548.
G.S. Armatas and M.G. Kanatzidis, Nature, 441, 1122 (2006); doi:10.1038/nature04833.
D. Sun, A.E. Riley, A.J. Cadby, E.K. Richman, S.D. Korlann and S.H. Tolbert, Nature, 441, 1126 (2006); doi:10.1038/nature04891.
V. Luca, J.N. Watson, M. Ruschena and R.B. Knott, Chem. Mater., 18, 1156 (2006); doi:10.1021/cm051255k.
G. Chen, L. Jiang, L. Wang and J. Zhang, Micropor. Mesopor. Mater., 134, 189 (2010); doi:10.1016/j.micromeso.2010.05.025.
M.J. Stébé, M. Emo, A. Forny-Le Follotec, L. Metlas-Komunjer, I. Pezron and J.L. Blin, Langmuir, 29, 1618 (2013); doi:10.1021/la304315v.
L. Han, J. Ruan, Y. Li, O. Terasaki and S. Che, Chem. Mater., 19, 2860 (2007); doi:10.1021/cm0705845.
K.S.W. Sing, D.H. Everett, R.A.W. Haul, L. Moscou, R.A. Pierotti, J. Rouquerol and T. Siemieniewska, Pure Appl. Chem., 57, 603 (1985); doi:10.1351/pac198557040603.

References

J.S. Beck, J.C. Vartuli, W.J. Roth, M.E. Leonowicz, C.T. Kresge, K.D. Schmitt, C.T.W. Chu, D.H. Olson and E.W. Sheppard, J. Am. Chem. Soc., 114, 10834 (1992); doi:10.1021/ja00053a020.

T.-L. Chew, A.L. Ahmad and S. Bhatia, Adv. Colloid Interface Sci., 153, 43 (2010); doi:10.1016/j.cis.2009.12.001.

J.H. Clark, D.J. Macquarrie and S.J. Tavener, Dalton Trans., 4297 (2006); doi:10.1039/b607831a.

I.I. Slowing, J.L. Vivero-Escoto, C.-W. Wu and V.S.-Y. Lin, Adv. Drug Deliv. Rev., 60, 1278 (2008); doi:10.1016/j.addr.2008.03.012.

J.L. Vivero-Escoto, I.I. Slowing, B.G. Trewyn and V.S.-Y. Lin, Small, 6, 1952 (2010); doi:10.1002/smll.200901789.

G. Garnweitner and M. Niederberger, J. Mater. Chem., 18, 1171 (2008); doi:10.1039/b713775c.

Z. Chen, T.L. Greaves, R.A. Caruso and C.J. Drummond, J. Mater. Chem., 22, 10069 (2012); doi:10.1039/c2jm30708a.

Y. Wan and D. Zhao, Chem. Rev., 107, 2821 (2007); doi:10.1021/cr068020s.

D. Zhao, J. Feng, Q. Huo, N. Melosh, G.H. Fredrickson, B.F. Chmelka and G.D. Stucky, Science, 279, 548 (1998); doi:10.1126/science.279.5350.548.

G.S. Armatas and M.G. Kanatzidis, Nature, 441, 1122 (2006); doi:10.1038/nature04833.

D. Sun, A.E. Riley, A.J. Cadby, E.K. Richman, S.D. Korlann and S.H. Tolbert, Nature, 441, 1126 (2006); doi:10.1038/nature04891.

V. Luca, J.N. Watson, M. Ruschena and R.B. Knott, Chem. Mater., 18, 1156 (2006); doi:10.1021/cm051255k.

G. Chen, L. Jiang, L. Wang and J. Zhang, Micropor. Mesopor. Mater., 134, 189 (2010); doi:10.1016/j.micromeso.2010.05.025.

M.J. Stébé, M. Emo, A. Forny-Le Follotec, L. Metlas-Komunjer, I. Pezron and J.L. Blin, Langmuir, 29, 1618 (2013); doi:10.1021/la304315v.

L. Han, J. Ruan, Y. Li, O. Terasaki and S. Che, Chem. Mater., 19, 2860 (2007); doi:10.1021/cm0705845.

K.S.W. Sing, D.H. Everett, R.A.W. Haul, L. Moscou, R.A. Pierotti, J. Rouquerol and T. Siemieniewska, Pure Appl. Chem., 57, 603 (1985); doi:10.1351/pac198557040603.

Issue

Vol. 26 No. 12 (2014): Vol 26 Issue 12

Facile Synthesis of Mesoporous Silica for Separation of Coalbed Methane

Corresponding Author(s) : Zhenghe Liu

Abstract

Keywords

Full Article

Download Citation

References

Table Of Contents