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Vol. 26 No. 16 (2014): Vol 26 Issue 16

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Bismuth as Internal Standard for Reliable Detection of Trace Lead at Screen-Printed Electrode

https://doi.org/10.14233/ajchem.2014.16740
Haiyun Zhang
Key Laboratory of Coastal Environmental Processes and Ecological Remediation, Yantai Institute of Coastal Zone Research (YIC), Chinese Academy of Sciences (CAS); Shandong Provincial Key Laboratory of Coastal Environmental Processes, YICCAS, Yantai 264003, Shandong Province, P.R. China ; University of Chinese Academy of Sciences, Beijing 100049, P.R. China
Mingyue Lin
Key Laboratory of Coastal Environmental Processes and Ecological Remediation, Yantai Institute of Coastal Zone Research (YIC), Chinese Academy of Sciences (CAS); Shandong Provincial Key Laboratory of Coastal Environmental Processes, YICCAS, Yantai 264003, Shandong Province, P.R. China ; University of Chinese Academy of Sciences, Beijing 100049, P.R. China
Qing Zhang
The Key Lab in Molecular and Nano-Materials Probes of the Ministry of Education of China, College of Chemistry, Chemical Engineering and Materials Science, Shandong Normal University, Jinan 250014, Shandong Province, P.R. China
Haitao Han
School of Chemistry and Chemistry Engineering, Yantai University, Yantai 264005, Shandong Province, P.R. China
Dawei Pan
Key Laboratory of Coastal Environmental Processes and Ecological Remediation, Yantai Institute of Coastal Zone Research (YIC), Chinese Academy of Sciences (CAS); Shandong Provincial Key Laboratory of Coastal Environmental Processes, YICCAS, Yantai 264003, Shandong Province, P.R. China

Corresponding Author(s) : Dawei Pan

dwpan@yic.ac.cn

Asian Journal of Chemistry, Vol. 26 No. 16 (2014): Vol 26 Issue 16

Abstract

In this paper, bismuth served as an internal standard used for reliable anodic stripping voltammetric determination of trace lead at screen-printed carbon electrodes. Besides its negligible concentration in water samples, bismuth can form alloy with lead and their anodic stripping peaks can be separated obviously. The influence of three electrode pretreatment methods and various experimental parameters upon the stripping signal was investigated. Under optimized conditions, the response ratio IPb/IBi against the concentration of lead was linear in the 2-200 μg L-1 concentration range with a correlation coefficient of 0.998 after 2 min deposition. The practical application of this method was carried out for the determination of lead in river water samples and the results were consistent with the values obtained by ICP-MS. The attractive behaviors of the low cost carbon strip electrodes coupled with the reliable quantitative strategy facilitates the development of portable electrochemical sensing platform.

Keywords

Bismuth Internal standard Screen-printed electrodes Anodic stripping voltammetry Lead
Zhang, H., Lin, M., Zhang, Q., Han, H., & Pan, D. (2014). Bismuth as Internal Standard for Reliable Detection of Trace Lead at Screen-Printed Electrode. Asian Journal of Chemistry, 26(16), 5217–5222. https://doi.org/10.14233/ajchem.2014.16740
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