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Vol. 26 No. 19 (2014): Vol 26 Issue 19

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Simple Preparation of Components from Gardenia Jasminoides Ellis by Targeted Partition in Liquid Two-Phase Extraction

https://doi.org/10.14233/ajchem.2014.16381
Sheng Liu
Department of Chemistry, Guangxi University, Nanning 530004, Guangxi Province, P.R. China
Wanxing Wei
Department of Chemistry, Guangxi University, Nanning 530004, Guangxi Province, P.R. China
Min Zhou
Department of Chemistry, Guangxi University, Nanning 530004, Guangxi Province, P.R. China
Zhiping Liu
Department of Chemistry, Guangxi University, Nanning 530004, Guangxi Province, P.R. China
Xiurong Ling
Department of Environment, Guangxi University, Nanning 530004, Guangxi Province, P.R. China

Corresponding Author(s) : Wanxing Wei

wxwei@gxu.edu.cn

Asian Journal of Chemistry, Vol. 26 No. 19 (2014): Vol 26 Issue 19

Abstract

Compounds were prepared from Gardenia jasminoides Ellis by targeted partition in two-liquid phase system without any chromatography columns. After Gardenia yellow and target guide reagent (polyethylene glycol, PEG) are dissolved in water, they would be partitioned with organic solvents in gradient to selectively give high-richened target component fractions. These fractions were crystallized, respectively to provide three components. Two of them were crocetin [b-D-glucopyranosyl-(1-6)-b-D-glucopyranosyl] ester (1) and crocin (2). Effects of partition on targeted compounds were investigated. The results not only shows that the component which is more oleophilic was most difficult to be extracted from the organic phase in these targeted partition systems, but also shows that using the target indicator PEG-2000, which is the lowest molecular weight in these systems, can facilitate selective separation of components.

Keywords

Gardenia yellow Targeted partition Crocetin ester Polyethylene glycol Preparation
Liu, S., Wei, W., Zhou, M., Liu, Z., & Ling, X. (2014). Simple Preparation of Components from Gardenia Jasminoides Ellis by Targeted Partition in Liquid Two-Phase Extraction. Asian Journal of Chemistry, 26(19), 6379–6382. https://doi.org/10.14233/ajchem.2014.16381
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References
  1. A. Ozaki, M. Kitano, N. Furusawa, H. Yamaguchi, K. Kuroda and G. Endo, Food Chem. Toxicol., 40, 1603 (2002); doi:10.1016/S0278-6915(02)00118-7.
  2. R.A.A. Lelono, S. Tachibana and K. Itoh, Pak. J. Biol. Sci., 12, 949 (2009); doi:10.3923/pjbs.2009.949.956.
  3. B. Yang, X. Liu and Y.X. Gao, Nnov. Food Sci. Emerg., 10, 610 (2009); doi:10.1016/j.ifset.2009.03.003.
  4. M. Carmona, A. Zalacain, A.M. Sanchez, J.L. Novella and G.L. Alonso, J. Agric. Food Chem., 54, 973 (2006); doi:10.1021/jf052297w.
  5. Y.Q. Zheng, J.X. Liu, J.N. Wang and L. Xu, Brain Res., 1138, 86 (2007); doi:10.1016/j.brainres.2006.12.064.
  6. K.N. Nam, Y.M. Park, H.J. Jung, J.Y. Lee, B.D. Min, S.-U. Park, W.-S. Jung, K.-H. Cho, J.-H. Park, I. Kang, J.-W. Hong and E.H. Lee, Eur. J. Pharmacol., 648, 110 (2010); doi:10.1016/j.ejphar.2010.09.003.
  7. Y. Chen, H. Zhang, X. Tian, C. Zhao, L. Cai, Y. Liu, L. Jia, H.-X. Yin and C. Chen, Food Chem., 109, 484 (2008); doi:10.1016/j.foodchem.2007.09.080.
  8. T.Q. Pham, F. Cormier, E. Farnworth, V.H. Tong and M.-R. Van Calsteren, J. Agric. Food Chem., 48, 1455 (2000); doi:10.1021/jf991263j.
  9. B. Ghadrdoost, A.A. Vafaei, A. Rashidy-Pour, R. Hajisoltani, A.R. Bandegi, F. Motamedi, S. Haghighi, H.R. Sameni and S. Pahlvan, Eur. J. Pharmacol., 667, 222 (2011); doi:10.1016/j.ejphar.2011.05.012.
  10. T. Debnath, P.-J. Park, N.C. Deb Nath, N.B. Samad, H.W. Park and B.O. Lim, Food Chem., 128, 697 (2011); doi:10.1016/j.foodchem.2011.03.090.
  11. L. Sheng, Z.Y. Qian, S.G. Zheng and L. Xi, Eur. J. Pharmacol., 543, 116 (2006); doi:10.1016/j.ejphar.2006.05.038.
  12. S.S. Maysam, B.S. Zahra and H. Heydarzadel, Clin. Biochem., 44, S27 (2011); doi:10.1016/j.clinbiochem.2011.08.080.
  13. S. Soeda, T. Ochiai, L. Paopong, H. Tanaka, Y. Shoyama and H. Shimeno, Life Sci., 69, 2887 (2001); doi:10.1016/S0024-3205(01)01357-1.
  14. M.M. Xu, Q. Sun, J. Su, J.F. Wang, C. Xu, T. Zhang and Q.L. Sun, Enzyme Microb. Technol., 42, 440 (2008); doi:10.1016/j.enzmictec.2008.01.003.
  15. M. Scordino, A. Di Mauro, A. Passerini and E. Maccarone, J. Agric. Food Chem., 52, 1965 (2004); doi:10.1021/jf035220l.
  16. C.P. Wang, J.B. Ji, L.H. Wang and T.H. Pao, Chem. Ind. Eng. Prog., 22, 622 (2003).
  17. Y.Y. Li and Y.X. Gao, J. Food Sci., 27, 113 (2006).
  18. J.F. Chen, G.M. Fu, Y. Wan, C.M. Liu, J.X. Chai, H.G. Li, J.T. Wang, M. Hu and L.N. Zhang, J. Chromatogr. B, 893-894, 43 (2012); doi:10.1016/j.jchromb.2012.02.032.
  19. W.D. Conway, in ed.: R.J. Petroski, Modern Countercurrent Chromatography, ACS Symposium Series, American Chemical Society: Washington, DC, p. 92 (1995).
  20. S.A. Mohajeri, H. Hosseinzadeh, F. Keyhanfar and J. Aghamohammadian, J. Sep. Sci., 33, 2302 (2010); doi:10.1002/jssc.201000183.
  21. M.R.V. Calsteren and M.C. Biseannetle, J. Agric. Food Chem., 45, 1055 (1997); doi:10.1021/jf9603487.
  22. A. Ozaki, M. Kitano, N. Furusawa, H. Yamaguchi, K. Kuroda and G. Endo, Food Chem. Toxicol., 40, 1603 (2002); doi:10.1016/S0278-6915(02)00118-7.
  23. Y. Yu, X.L. Feng, H. Gao, Z.L. Xie, Y. Dai, X.J. Huang, H. Kurihara, W.C. Ye, Y. Zhong and X.S. Yao, Fitoterapia, 83, 563 (2012); doi:10.1016/j.fitote.2011.12.027.
  24. H.J. Choi, Y.S. Park, M.G. Kim, T.K. Kim, N.S. Yoon and Y.J. Lim, Dyes Pigments, 49, 15 (2001); doi:10.1016/S0143-7208(01)00007-9.
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