Derivatizing Condition of Trace Dicyandiamide with Dansyl Chloride and Application of Spectrum Analysis Method

Huidong Qiu; Dongdi Sun; Todd Mlsna

doi:10.14233/ajchem.2014.16752

Issue

Vol. 26 No. 19 (2014): Vol 26 Issue 19

Issue Published : September 16, 2014

This work is licensed under a Creative Commons Attribution 4.0 International License.

Derivatizing Condition of Trace Dicyandiamide with Dansyl Chloride and Application of Spectrum Analysis Method

https://doi.org/10.14233/ajchem.2014.16752

Huidong Qiu

Department of Chemistry and Chemical engineering, Chong Qing University of Science and Technology, Chongqing, 401331, P.R. China; Department of Chemistry, Mississippi State University, Mississippi State, MS 39762, USA

Dongdi Sun

Department of Chemistry, Mississippi State University, Mississippi State, MS 39762, USA

Todd Mlsna

Department of Chemistry, Mississippi State University, Mississippi State, MS 39762, USA

Corresponding Author(s) : Huidong Qiu

qhd324@163.com

Asian Journal of Chemistry, Vol. 26 No. 19 (2014): Vol 26 Issue 19
Article Published : September 19, 2014

Abstract

A dicyandiamide dansylation procedure compatible with UV spectum was presented. The method provides quickly derivatization while the ratio of dansyl chloride to dicyandiamide over a 10000-fold range, buffer pH of 9.5, ambient temperature of 40 °C and reaction time of 10 min. The method is convenient only using a simple UV spectrometers and successfully achieved method limit of quantification 30 ng/L in water sample.

Keywords

Dansyl chloride Dicyandiamide Derivation Spectrum analysis

Qiu, H., Sun, D., & Mlsna, T. (2014). Derivatizing Condition of Trace Dicyandiamide with Dansyl Chloride and Application of Spectrum Analysis Method. Asian Journal of Chemistry, 26(19), 6605–6608. https://doi.org/10.14233/ajchem.2014.16752

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References

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References

K.L. McGeough, R.J. Laughlin, C.J. Watson, C. Muller, M. Ernfors, E. Cahalan and K.G. Richards, Biogeosciences, 9, 4909 (2012); doi:10.5194/bg-9-4909-2012.

H.J. Di and K.C. Cameron, J. Soils Sediments, 11, 1032 (2011); doi:10.1007/s11368-011-0372-1.

L.L. Zhang, Z.J. Wu, L.J. Chen, H.J. Zhang, Y.L. Zhang and Z.H. Chen, Ecol. Environ. Sci., 18, 1508 (2009).

K. Joji, T. Watanabe and T. Noboru, J. Chem. Soc. Jpn. Chem. Ind. Chem., 1, 37 (1997).

G.N. Lucas, Sri Lanka J. Child. Health, 42, 63 (2013).

L. Schep, W. Temple and M. Beasley, Clin. Toxicol., 47, 58 (2009); doi:10.1080/15563650802459254.

J.E. Milks and R.H. Janes, Anal. Chem., 28, 846 (1956); doi:10.1021/ac60113a019.

C.M. Zhou, J.P. Zhou, J. Wu and X.J. Li, Jiangsu J. Prev. Med., 20, 63 (2009).

L. Wu, B.J. Shi and Y. Wang, Chinese J. Biochem. Pharm., 30, 110 (2009).

C. Schwarzer and K. Haselwandter, J. Chromatogr. A, 732, 390 (1996); doi:10.1016/0021-9673(95)01283-4.

J.B. Nair, J. Chromatogr. A, 671, 367 (1994); doi:10.1016/0021-9673(94)80262-9.

S. Macmahon, T.H. Begley, G.W. Diachenko and S.A. Stromgren, J. Chromatogr. A, 1220, 101 (2012); doi:10.1016/j.chroma.2011.11.066.

M. Turowski and B. Deshmukh, Anal. Lett., 37, 1981 (2004); doi:10.1081/AL-120039440.

Z.X. Wang, J. Jiang, L. Sun, H.B. Zhou and Y.X. Zhao, J. Instrum. Anal., 31, 593 (2012).

J.J. Xu, J.X. Zhang, B.F. Huang and Y.P. Ren, J. Food Safety and Quality, 4, 415 (2013).

L. Wu, B.J. Shi and Y. Wang, Chin. Pharm. J., 10, 780 (2010).

S. Hiradate, T. Kamo, E. Nakajima, K. Kato and Y. Fujii, J. Chromatogr. A, 1098, 138 (2005); doi:10.1016/j.chroma.2005.08.035.

X.Z. Chen, W.Q. Chen, J. Wang, L.Y. Huang and D.L. Zhang, Chinese J. Chromatogr., 31, 875 (2013).

Y. Tapuhi, D.E. Schmidt, W. Lindner and B.L. Karger, Anal. Biochem., 115, 123 (1981); doi:10.1016/0003-2697(81)90534-0.

H.L. Cai, R.H. Zhu, H.D. Li, J. Zhang and L.F. Li, J. Chromatogr. B, 879, 1993 (2011); doi:10.1016/j.jchromb.2011.05.006.

X.M. Cai, H. Zhao, M. Wu, X.Q. Hu, H.M. He, C.P. Zhang, C.R. Zhang and Z. Li, Chromatographia, 75, 1069 (2012); doi:10.1007/s10337-012-2276-7.

W.F. Dong, X.Z. Li and W.X. Lin, J. Dalian Institute of Light Ind., 2, 115 (2005).

S. Chen, A.P. Ocampo and P.J. Kucera, J. Chromatogr. A, 558, 141 (1991); doi:10.1016/0021-9673(91)80119-2.

A. Negro, S. Garbisa, L. Gotte and M. Spina, Anal. Biochem., 160, 39 (1987); doi:10.1016/0003-2697(87)90611-7.

R. Bartzatt, Anal. Chim. Acta, 488, 203 (2003); doi:10.1016/S0003-2670(03)00704-9.

R. Nirogi, P. Komarneni, V. Kandikere, R. Boggavarapu, G. Bhyrapuneni, V. Benade and S. Gorentla, J. Chromatogr. B, 913-914, 41 (2013); doi:10.1016/j.jchromb.2012.09.034.

H.X. Wang, Y. Zhou and Q.W. Jiang, Food Addit. Contam. Part A, 30, 166 (2013); doi:10.1080/19440049.2012.720036.

T.Y. Kim and H.J. Kim, J. Chromatogr. A, 933, 99 (2001); doi:10.1016/S0021-9673(01)01240-7.

H. Yamada, A. Yamahara, S. Yasuda, M. Abe, K. Oguri, S. Fukushima and S. Ikeda-Wada, J. Anal. Toxicol., 26, 17 (2002); doi:10.1093/jat/26.1.17.

M.E. AbdEl-Ghaffar, D.R. El-Wasseef, D.T. El-Sherbiny and S.M. El-Ashry, J. Anal. Chem., 66, 476 (2011); doi:10.1134/S1061934811050029.

Issue

Vol. 26 No. 19 (2014): Vol 26 Issue 19

Derivatizing Condition of Trace Dicyandiamide with Dansyl Chloride and Application of Spectrum Analysis Method

Corresponding Author(s) : Huidong Qiu

Abstract

Keywords

Full Article

Download Citation

References

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