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Vol. 26 No. 21 (2014): Vol 26 Issue 21

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Purification of Flavone C-Glycosides from Bamboo Leaves by Macroporous Adsorption Resin

https://doi.org/10.14233/ajchem.2014.16570
Hui Guo
College of Pharmaceutical Science, Zhejiang University of Technology, Hangzhou 310014, P.R China
Kang-Mei Fan
College of Pharmaceutical Science, Zhejiang University of Technology, Hangzhou 310014, P.R China
Jun-Qing Qian
College of Pharmaceutical Science, Zhejiang University of Technology, Hangzhou 310014, P.R China

Corresponding Author(s) : Jun-Qing Qian

qianguozjut@163.com

Asian Journal of Chemistry, Vol. 26 No. 21 (2014): Vol 26 Issue 21

Abstract

A simple and efficient process for purification flavone C-glycosides from bamboo leaves was developed in this paper. The adsorptive properties of flavone C-glycosides on the resins were evaluated. Among the ten macroporous resin adsorbents tested, the non-polar resin H103 has the best adsorption and desorption performance. Besides, the static equilibrium adsorption data fitted well with the Langmuir equation. The gradient elution program was as follows: 2 BV (bed volume) of deionized water, 2 BV of 20 % ethanol, 5 BV of 80 % ethanol at a flow rate of 1 mL/min. After the H103 resin treatment, the contents of the total 6 flavone C-glycosides were increased from 2.49 to 50.40 %, the recovery rate of which was 69.73 %. Therefore, the method can be applied to the separation of flavone C-glycosides from bamboo leaves.

Keywords

Bamboo leaves DesorptBn Flavone C-glycosides Macroporous resin
Guo, H., Fan, K.-M., & Qian, J.-Q. (2014). Purification of Flavone C-Glycosides from Bamboo Leaves by Macroporous Adsorption Resin. Asian Journal of Chemistry, 26(21), 7221–7225. https://doi.org/10.14233/ajchem.2014.16570
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