Shaped-Controlled Synthesis of Nanosized Cuprous Oxides by Hydrothermal Oxidation Method

Nguyen Tien Thao; Mai Quang Tuong

doi:10.14233/ajchem.2014.17414

Issue

Vol. 26 No. 22 (2014): Vol 26 Issue 22

Issue Published : November 6, 2014

This work is licensed under a Creative Commons Attribution 4.0 International License.

Shaped-Controlled Synthesis of Nanosized Cuprous Oxides by Hydrothermal Oxidation Method

https://doi.org/10.14233/ajchem.2014.17414

Nguyen Tien Thao

Faculty of Chemistry, VNU University of Science, Vietnam National University, Hanoi 10999, Vietnam ; VNU University of Science, 19-Le Thanh Tong ST, Hanoi 10999, Vietnam

Mai Quang Tuong

VNU University of Science, 19-Le Thanh Tong ST, Hanoi 10999, Vietnam

Corresponding Author(s) : Nguyen Tien Thao

ntthao@vnu.edu.vn

Asian Journal of Chemistry, Vol. 26 No. 22 (2014): Vol 26 Issue 22
Article Published : November 6, 2014

Abstract

Nanoscaled cuprous oxides were synthesized using the reaction between metallic copper and aqueous hydrogen peroxide solution in isothermal conditions. The resultant solids are characterized by XRD, SEM, TEM, BET techniques. The obtained products are mainly cuprous oxides with different morphologies. The size, shape and aspect ratio of products can be readily controlled by aging time and additive amounts. The present controlled synthesis method yield some kinds of highly crystalline metal oxide nanocrystals. An introduction of HCOOH additive into reaction mixture would significantly affect the controllable size, shape and yield of Cu₂O.

Keywords

Controlled synthesis Cu2O Nanoparticles Nanostructured oxide

Tien Thao, N., & Quang Tuong, M. (2014). Shaped-Controlled Synthesis of Nanosized Cuprous Oxides by Hydrothermal Oxidation Method. Asian Journal of Chemistry, 26(22), 7635–7637. https://doi.org/10.14233/ajchem.2014.17414

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References

H. Xu, W. Wang and W. Zhu, J. Phys. Chem. B, 110, 13829 (2006); doi:10.1021/jp061934y.

Y. Chang, J.J. Teo and H.C. Zeng, Langmuir, 21, 1074 (2005); doi:10.1021/la047671l.

H. Zhang, D. Zhou, L. Zhang, D.-F. Zhang, L. Guo, L. He and C.-P. Chen, J. Nanosci. Nanotechnol., 9, 1321 (2009); doi:10.1166/jnn.2009.C147.

M.A. Shoeib, O.E. Abdelsalam, M.G. Khafagi and R.E. Hammam, Adv. Powder Technol., 23, 298 (2012); doi:10.1016/j.apt.2011.04.001.

J. Zhang, J. Liu, Q. Peng, X. Wang and Y. Li, Chem. Mater., 18, 867 (2006); doi:10.1021/cm052256f.

H.Y. Zhao, Y.F. Wang and J.H. Zeng, Cryst. Growth Des., 8, 3731 (2008); doi:10.1021/cg8003678.

N.T. Thao, VN J. Chem., 51(3B), 500 (2013).

X. Zhang, J. Song, J. Jiao and X. Mei, Solid State Sci., 12, 1215 (2010); doi:10.1016/j.solidstatesciences.2010.03.009.

G. Li, L. Jiang, S. Pang, H. Peng and Z. Zhang, J. Phys. Chem. B, 110, 24472 (2006); doi:10.1021/jp064855v.

M. Fernandez-Garcıa, A. Martínez-Arias, J.C. Hanson and J.A. Rodriguez, Chem. Rev., 104, 4063 (2004); doi:10.1021/cr030032f.

S. Yin, S. Akita, M. Shinozaki, R. Li and T. Sato, J. Mater. Sci., 43, 2234 (2008); doi:10.1007/s10853-007-2070-3.

Y. Dong, Y. Li, C. Wang, A. Cui and Z. Deng, J. Colloid Interf. Sci., 243, 85 (2001); doi:10.1006/jcis.2001.7857.

X. Zhang, G. Wang, H. Wu, D. Zhang, X. Zhang, P. Li and H. Wu, Mater. Lett., 62, 4363 (2008); doi:10.1016/j.matlet.2008.07.028.

Z.C. Orel, A. Anzlovar, G. Drazic and M. Zigon, Cryst. Growth Des., 7, 453 (2007); doi:10.1021/cg060615t.

X. Xu, S. Sithambaram, Y. Zhang, C.-H. Chen, L. Jin, R. Joesten and S.L. Suib, Chem. Mater., 21, 1253 (2009); doi:10.1021/cm802915m.

Issue

Vol. 26 No. 22 (2014): Vol 26 Issue 22

Shaped-Controlled Synthesis of Nanosized Cuprous Oxides by Hydrothermal Oxidation Method

Corresponding Author(s) : Nguyen Tien Thao

Abstract

Keywords

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