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Simultaneous Determination of Organochlorine Pesticides, Polycyclic Aromatic Hydrocarbons and Polychlorinated Biphenyls in Water by Solid Phase Disk Extraction-Ultrasonic Desorption and GCMS
Corresponding Author(s) : Y.T. Zhang
Asian Journal of Chemistry,
Vol. 27 No. 2 (2015): Vol 27 Issue 2
Abstract
A method was developed for the simultaneous determination of organochlorine pesticides, polycyclic aromatic hydrocarbons and polychlorinated biphenyls in water by solid-phase disk extraction-ultrasonic desorption and gas chromatography-mass (GC-MS).The samples were extracted by C18 solid-phase disk extraction, and ultrasonic wave to promote the extraction of object from the solid phase membranes, which realize the simultaneous purification of 17 types organochlorine pesticides, 16 kinds of polycyclic aromatic hydrocarbons and 2 kinds of aroclors. The recoveries of the compounds of this method were 70-130 %, with relative standard deviation below 10 and the detection limit between 0.2 and 1.1 ng/L, which would satisfy the demand of daily water quality analysis.
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- X.L. He, T.T. Xu, Y.Y. Zhang, J.T. Wang and N. Xia, Rock Miner. Anal., 6, 57 (2012).
- W.W. Dong, Y.J. Hao, D. Wang and Y. Xu, Hubei Agric. Sci. Sci., 8, 1693 (2011).
- T.F. Bidleman, M.D. Walla, R. Roura, E. Carr and S. Schmidt, Mar. Pollut. Bull., 26, 258 (1993); doi:10.1016/0025-326X(93)90064-Q.
- B.G. Loganathan and K. Kannan, Ambio, 3, 187 (1994).
- S. Tanabe, H. Hidaka and R. Tatsukawa, Chemosphere, 12, 277 (1983); doi:10.1016/0045-6535(83)90171-6.
- Y. Wang, X.X. Zhi and L.J. Zhang, J. Instrumental Anal., 5, 493 (2008).
- J. Fang and K.X. Wang, Chin. J. Anal. Chem., 11, 1607 (2007).
- Z.W. Xie, P. Yang, Ch. Liao, Ch.H. Ren, Ch.H. Guo, X.Q. Wu and J. Liao, Environ. Moint. China, 5, 20 (2008).
- Environmental Protection Agency (EPA), Standard Methods for the Determination of Polychlorinated Biphenyls (PCBs) by Gas Chromatography, Washington DC (1996).
References
A. Aguilar and A. Borrell, in eds.: M.C. Fossi and C. Leonzio, Assessment of Organochlorine Pollutants in Cetaceans by Averages of Skin and Hypodermic Biopsies, In: Non-Destructive Biomarkers in Vertebrates, Boca Raton, FL. Lewis Publishers, pp. 245-268 (1994).
K. Haraguchi, T. Endo, M. Sakata, Y. Masuda and M. Simmonds, Shokuhin Eiseigaku Zasshi, 41, 287 (2000); doi:10.3358/shokueishi.41.287.
D. Viale, Int. J. Environ., 45, 183 (1994); doi:10.1080/00207239408710893.
X.L. He, T.T. Xu, Y.Y. Zhang, J.T. Wang and N. Xia, Rock Miner. Anal., 6, 57 (2012).
W.W. Dong, Y.J. Hao, D. Wang and Y. Xu, Hubei Agric. Sci. Sci., 8, 1693 (2011).
T.F. Bidleman, M.D. Walla, R. Roura, E. Carr and S. Schmidt, Mar. Pollut. Bull., 26, 258 (1993); doi:10.1016/0025-326X(93)90064-Q.
B.G. Loganathan and K. Kannan, Ambio, 3, 187 (1994).
S. Tanabe, H. Hidaka and R. Tatsukawa, Chemosphere, 12, 277 (1983); doi:10.1016/0045-6535(83)90171-6.
Y. Wang, X.X. Zhi and L.J. Zhang, J. Instrumental Anal., 5, 493 (2008).
J. Fang and K.X. Wang, Chin. J. Anal. Chem., 11, 1607 (2007).
Z.W. Xie, P. Yang, Ch. Liao, Ch.H. Ren, Ch.H. Guo, X.Q. Wu and J. Liao, Environ. Moint. China, 5, 20 (2008).
Environmental Protection Agency (EPA), Standard Methods for the Determination of Polychlorinated Biphenyls (PCBs) by Gas Chromatography, Washington DC (1996).