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Vol. 37 No. 8 (2025): Vol 37 Issue 8, 2025

Copyright (c) 2025 SITI KHATIJAH DERAMAN

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Physicochemical Studies of Ni/Al Layered Double Hydroxide at Ambient Temperature

https://doi.org/10.14233/ajchem.2025.34005
Siti Nurul 'Afini Mohd Johari
School of Chemistry and Environment, Faculty of Applied Sciences, Universiti Teknologi MARA (UiTM), 40450 Shah Alam, Selangor, Malaysia
https://orcid.org/0009-0005-3007-454X
Siti Khatijah Deraman
Centre of Foundation Studies, Universiti Teknologi MARA, Cawangan Selangor, Kampus Dengkil 43800 Dengkil, Selangor, Malaysia
https://orcid.org/0000-0002-2724-1838
Hussein Hanibah
Centre of Foundation Studies, Universiti Teknologi MARA, Cawangan Selangor, Kampus Dengkil 43800 Dengkil, Selangor, Malaysia
https://orcid.org/0000-0002-5882-1018
Nazrizawati Ahmad Tajuddin
School of Chemistry and Environment, Faculty of Applied Sciences, Universiti Teknologi MARA (UiTM), 40450 Shah Alam, Selangor, Malaysia
https://orcid.org/0000-0002-1980-782X

Corresponding Author(s) : Siti Khatijah Deraman

drsitikhatijah@uitm.edu.my

Asian Journal of Chemistry, Vol. 37 No. 8 (2025): Vol 37 Issue 8, 2025

Abstract

The Ni/Al layered double hydroxide (Ni/Al LDH) was synthesized via alkali free co-precipitation method with ratio of 4:1. The product of co-precipitation was undergone aging process for 24 h. Then, it was placed in oven at 100 ºC overnight and finally was calcined at 450 ºC for 13 h. The correlation of crystallinity; morphology and particle size of Ni/Al LDH before and after calcination were examined and compared. Thermogravimetric analysis (TGA) was used to evaluate the interlayer anion and carbonate content of Ni/Al LDH. Powder X-ray diffraction (PXRD) was used to study the textural and structural characteristics of the samples. Particle size, morphology and particle properties were characterized by Brunauer-Emmett-Teller (BET) and field emission scanning electron (FESEM). The bonding and structural of Ni/Al LDH was studied by Fourier transform infrared (FTIR).

Keywords

Layered double hydroxide Hydrotalcites Nanocomposite Co-precipitation
(1)
Mohd Johari, S. N. 'Afini; Deraman, S. K.; Hanibah, H.; Tajuddin, N. A. Physicochemical Studies of Ni Al Layered Double Hydroxide at Ambient Temperature. ajc 2025, 37, 1898-1902.
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