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Vol. 33 No. 1 (2021): Vol 33 Issue 1

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Synthesis of PEG-Fe3O4/ZnO Magnetic Nanocomposites by Ultrasound Assisted Co-Precipitation Process and their Antibacterial Activity

https://doi.org/10.14233/ajchem.2021.22990
Nguyen Thi Huong
Institute of Chemistry and Materials, 17 Hoang Sam, Cau Giay, Hanoi, Vietnam
Dao The Nam
Institute of Chemistry and Materials, 17 Hoang Sam, Cau Giay, Hanoi, Vietnam
Nguyen Thi Nhan
Institute of Chemistry and Materials, 17 Hoang Sam, Cau Giay, Hanoi, Vietnam
Nguyen Ngoc Son
Institute of Chemistry and Materials, 17 Hoang Sam, Cau Giay, Hanoi, Vietnam
Le Minh Tri
Institute for Military Science and Technology, 17 Hoang Sam, Cau Giay, Hanoi, Vietnam
Vu Minh Thanh
Institute of Chemistry and Materials, 17 Hoang Sam, Cau Giay, Hanoi, Vietnam

Corresponding Author(s) : Nguyen Thi Huong

nguyenhuong0916@gmail.com

Asian Journal of Chemistry, Vol. 33 No. 1 (2021): Vol 33 Issue 1

Abstract

In this study, PEG-Fe3O4/ZnO magetic nanocomposties were synthesized by a ultrasound assisted co-precipitation method. The magnetic nanocomposites were characterized by XRD, FT-IR, FESEM and VSM techniques. The effect of Fe3O4:ZnO ratio on the crystallite size and the lattice parameter of the nanoparticles was also studied using XRD. Magetic nanoparticles of PEG-Fe3O4/ZnO nanocomposites exhibit the particles size in the range of 20-30 nm. The VSM measurements at room temperature showed that PEG-Fe3O4/ZnO nanocomposites had superparamagnetic properties. These results indicated that ultrasonication time and ration (Fe3O4/ZnO) greatly affect the characteristics of the nanoparticles. The antibacterial efficiency of PEG-Fe3O4/ZnO nanoparticles was tested against Sacharomyces cerevisiae, Bacillus subtilis and E. coli bacteria using disc diffusion method.

Keywords

PEG-Fe3O4/ZnO Ultrasonication Crystallite Lattice parameter Antibacterial activity
Thi Huong, N., The Nam, D., Thi Nhan, N., Ngoc Son, N., Minh Tri, L., & Minh Thanh, V. (2020). Synthesis of PEG-Fe3O4/ZnO Magnetic Nanocomposites by Ultrasound Assisted Co-Precipitation Process and their Antibacterial Activity. Asian Journal of Chemistry, 33(1), 215–219. https://doi.org/10.14233/ajchem.2021.22990
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References
  1. D. Frascione, C. Diwoky, G. Almer, P. Opriessnig, C. Vonach, K.Gradauer, G. Leitinger, H. Mangge, R. Stollberger and R. Prassl, Int.J. Nanomed., 7, 2349 (2012); https://doi.org/10.2147/IJN.S30617
  2. Ü. Özgür, Y.I. Alivov, C. Liu, A. Teke, M. Reshchikov, S. Dogan, V. Avrutin, S.-J. Cho and H. Morkoç, J. Appl. Phys., 98, 041301 (2005); https://doi.org/10.1063/1.1992666
  3. M. Roselli, A. Finamore, I. Garaguso, M.S. Britti and E. Mengheri, J.Nutr., 133, 4077 (2003); https://doi.org/10.1093/jn/133.12.4077
  4. L.-E. Shi, Z.-H. Li, W. Zheng, Y.-F. Zhao, Y.-F. Jin and Z.-X. Tang, Food Addit. Contam. Part A, 31, 173 (2014);https://doi.org/10.1080/19440049.2013.865147
  5. J. Sawai, S. Shoji, H. Igarashi, A. Hashimoto, T. Kokugan, M. Shimizu and H. Kojima, J. Ferment. Bioeng., 86, 521 (1998); https://doi.org/10.1016/S0922-338X(98)80165-7
  6. M. Liu, X. Sun, Z. Liao, Y. Li, X. Qi, Y. Qian, H. Fenniri, P. Zhao and J. Shen, Drug Deliv., 26, 732 (2019); https://doi.org/10.1080/10717544.2019.1642419
  7. G. Bisht, S. Rayamajhi, B. Kc, S.N. Paudel, D. Karna and B.G. Shrestha, Nanoscale Res. Lett., 11, 537 (2016);https://doi.org/10.1186/s11671-016-1734-9
  8. S. Bagheri and N.M. Julkapli, J. Magn. Magn. Mater., 416, 117 (2016);https://doi.org/10.1016j.jmmm.2016.05.042
  9. V.M. Thanh, D.T. Nam, P.T. Phuong, P.T. Anh, C.T. Dung, N.N. Son and N.T. Huong, J. Chem., 57, 365 (2019) (in Vietnamese).
  10. J. Sawai, J. Microbiol. Methods, 54, 177 (2003); https://doi.org/10.1016/S0167-7012(03)00037-X
  11. T.J. Daou, G. Pourroy, S. Bégin-Colin, J.M. Grenèche, C. UlhaqBouillet, P. Legaré, P. Bernhardt, C. Leuvrey and G. Rogez, Chem. Mater., 18, 4399 (2006); https://doi.org/10.1021/cm060805r
  12. M. Roeinfard and A. Bahari, J. Supercond. Nov. Magn., 30, 3541 (2017);https://doi.org/10.1007/s10948-017-4154-x
  13. H. Qiu, B. Cui, G. Li, J. Yang, H. Peng, Y. Wang, N. Li, R. Gao, Z. Chang and Y. Wang, J. Phys. Chem. C, 118, 14929 (2014);https://doi.org/10.1021/jp502820r
  14. J. Gajendiran and V. Rajendran, Mater. Lett., 116, 311 (2014); https://doi.org/10.1016/j.matlet.2013.11.063
  15. S. Jafarirad, M. Mehrabi, B. Divband and M. Kosari-Nasab, Mater. Sci. Eng. C, 59, 296 (2016); https://doi.org/10.1016/j.msec.2015.09.089
  16. K. Ali, S. Dwivedi, A. Azam, Q. Saquib, M.S. Al-Said, A.A. Alkhedhairy and J. Musarrat, J. Colloid Interface Sci., 472, 145 (2016); https://doi.org/10.1016/j.jcis.2016.03.021
  17. P.E. Ochieng, E. Iwuoha, I. Michira, M. Masikini, J. Ondiek, P. Githira and G.N. Kamau, Int. J. BioChem. Phys., 23, 53 (2015).
  18. R. Yuvakkumar, J. Suresh, A.J. Nathanael, M. Sundrarajan and S.I. Hong, Mater. Sci. Eng. C, 41, 17 (2014);https://doi.org/10.1016/j.msec.2014.04.025
  19. N.T. Huong, L.N.T. Trang, C.T. Dung, N.N. Son, N.D. Anh, D.T. Nam and V.M. Thanh, J. Chem., 57, 340 (2019) (in Vietnamese).
  20. A.W. Bauer, W.M. Kirby, J.C. Sherris and M. Turck, Am. J. Clin. Pathol., 45, 493 (1966).
  21. Z. Li, L. Wei, M.Y. Gao and H. Lei, Adv. Mater., 17, 1001 (2005); https://doi.org/10.1002/adma.200401545
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