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Solvent Evaporation Method and Crystal Structure of Thiophene-2,3-dicarboxylate
Corresponding Author(s) : Y.X. He
Asian Journal of Chemistry,
Vol. 27 No. 2 (2015): Vol 27 Issue 2
Abstract
One new thiophene compound i.e., thiophene-2,3-dicarboxylate with 2,3-dibromo thiophene, butyllithium and anhydrous ether has been successfully synthesized. The compound has been characterized by X-ray single-crystal diffraction. The new synthesized compound shows a one-dimensional framework. The 3D supramolecular structure is formed via hydrogen bonding connection.
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- J. Roncali, J. Mater. Chem., 9, 1875 (1999); doi:10.1039/a902747e.
- 2 N. C. Tice, S. M. Peak and S. Parkin, Heterocycles, 81, 1631 (2010); doi:10.3987/COM-10-11940.
- Y.H. Wen, J.K. Cheng, Y.L. Feng, J. Zhang, Z.L. Li and Y.G. Yao, Inorg. Chim. Acta, 358, 3347 (2005); doi:10.1016/j.ica.2005.05.004.
- G.M. Sheldrick, SHELXTL97, Program for the Refinement of Crystal Structure, University of Gottingen, Germany (1997).
References
J. Roncali, J. Mater. Chem., 9, 1875 (1999); doi:10.1039/a902747e.
2 N. C. Tice, S. M. Peak and S. Parkin, Heterocycles, 81, 1631 (2010); doi:10.3987/COM-10-11940.
Y.H. Wen, J.K. Cheng, Y.L. Feng, J. Zhang, Z.L. Li and Y.G. Yao, Inorg. Chim. Acta, 358, 3347 (2005); doi:10.1016/j.ica.2005.05.004.
G.M. Sheldrick, SHELXTL97, Program for the Refinement of Crystal Structure, University of Gottingen, Germany (1997).