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Vol. 27 No. 2 (2015): Vol 27 Issue 2

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Synthesis and Structural Characterization of Bromo-Substituted Salamo-Type Bisoximes Based on Bis(aminooxy)alkane and 3,5-Dibromosalicylaldehyde

https://doi.org/10.14233/ajchem.2015.17470
G.-X. An
School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, P.R. China
Y. Zhang
School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, P.R. China
L. Wang
School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, P.R. China
Y.-X. Sun
School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, P.R. China
X.-Y. Dong
School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, P.R. China
W.-K. Dong
School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, P.R. China

Corresponding Author(s) : W.-K. Dong

dongwk@126.com

Asian Journal of Chemistry, Vol. 27 No. 2 (2015): Vol 27 Issue 2

Abstract

A series of bromo-substituted Salamo-type bisoximes H2L1-H2L3 have been synthesized through condensation reactions of 3,5-dibromosalicylaldehyde with 1,2-bis(aminooxy)ethane, 1,3-bis(aminooxy)propane and 1,4-bis(aminooxy)butane in ethanol medium, respectively and characterized by elemental analyses, IR and 1H NMR spectra. In the crystal structure of Salamo-type bisoximes H2L1, an infinite 1D supramolecular double chain-like structure is formed by intramolecular hydrogen bonds, p···p stacking interactions and intermolecular Br···Br halogen bondings.

Keywords

Synthesis Salamo-type bisoxime Characterization Crystal structure
An, G.-X., Zhang, Y., Wang, L., Sun, Y.-X., Dong, X.-Y., & Dong, W.-K. (2015). Synthesis and Structural Characterization of Bromo-Substituted Salamo-Type Bisoximes Based on Bis(aminooxy)alkane and 3,5-Dibromosalicylaldehyde. Asian Journal of Chemistry, 27(2), 663–666. https://doi.org/10.14233/ajchem.2015.17470
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