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Vol. 32 No. 10 (2020): Vol 32 Issue 10

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Extraction Process and Analysis of Components in Essential Oils of Piper longum Linn. Harvested in Dak Lak Province, Vietnam

https://doi.org/10.14233/ajchem.2020.22564
Thien Hien Tran
Center of Excellence for Biochemistry and Natural Products, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam ; NTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam
Van Chi Khang
Center of Excellence for Biochemistry and Natural Products, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam ; NTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam
Hoang Duy Ngo
Faculty of Environmental and Food Engineering, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam
Xuan Tien Le
Department of Chemical Engineering, Ho Chi Minh City University of Technology (HCMUT), 268 Ly Thuong Kiet Street, District 10, Ho Chi Minh City 700000, Vietnam ; Vietnam National University Ho Chi Minh City, Linh Trung Ward, Thu Duc District, Ho Chi Minh City 700000, Vietnam

Corresponding Author(s) : Xuan Tien Le

tien.le@hcmut.edu.vn

Asian Journal of Chemistry, Vol. 32 No. 10 (2020): Vol 32 Issue 10

Abstract

Nowadays, plants containing biological activities are increasingly interested for their antioxidant and antibacterial properties. In particular, Pepper longum Linn. was known as one of the popular types of pepper family in Vietnam with many different uses in food and medicine. In this study, Pepper longum fruits were studied for extraction to essential oil by hydrodistillation through two survey methods such as single factor investigation method and optimization by response surface methodology (RSM). The analysis results by design expert software program version 11 shown that at the condition that the ratio of water to raw material 6:1 (mL/g), during 225 min extraction at 130 ºC, the essential oil yield was obtained 0.8%. The model predicts this result for F-value, P-values and Lack of Fit are mathematically significant and values for reliability R2 = 0.9963, C.V. % =1.99. Essential oil obtained was evaluated by gas chromatography-mass spectrometry (GC-MS) technique, which accounted that β-caryophyllene contains the highest amount among the other 43 components present.

Keywords

Piper longum Linn. Essential oil Gas chromatography Mass spectrometry Response surface methodology
Hien Tran, T., Chi Khang, V., Duy Ngo, H., & Tien Le, X. (2020). Extraction Process and Analysis of Components in Essential Oils of Piper longum Linn. Harvested in Dak Lak Province, Vietnam. Asian Journal of Chemistry, 32(10), 2639–2646. https://doi.org/10.14233/ajchem.2020.22564
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