Copyright (c) 2019 AJC
This work is licensed under a Creative Commons Attribution 4.0 International License.
Nanoemulsion of Sesame Seeds Oil: Preparation, Evaluation and Stability
Corresponding Author(s) : W.A. Al-Saban
Asian Journal of Chemistry,
Vol. 31 No. 12 (2019): Vol 31 Issue 12
Abstract
This work aims to study the effect of using nanoemulsion particles on the stability of sesame seed oil emulsion. During the roasting process of sesame seeds (Sohage-1), some physico-chemical properties of sesame seeds and its oil were determined. The moisture, protein and fiber contents were decreased whereas oil, ash and carbohydrates contents were increased. Sesame oil was extracted from roasted sesame seeds using mechanical pressing; some physico-chemical properties for extracted oil were determined. Results indicated that colour, acid value, free fatty acids (%), peroxide and hydrolysis values were increased, while saponification value was decreased in sesame oil. Also traditional and nanoemulsions form of sesame oil were prepared.Characterization of these emulsions particles was conducted using zeta potential and transmission electron microscope (TEM). The results also indicated that small droplet size of nanoemulsion particles being 26.28 nm in emulsion which prepared by using nano-technique as compared with those of 638.8 nm in traditional emulsion type and low polydispersity index (PDI) was nanoemulsion particles 0.266. This lead to more uniformity in droplet size thus could improve the stability of emulsion system. The TEM results of nanoemulsion particles of sesame oil showed that spherical droplets and nearly similarity in shape in nanoemulsion in compared with semi-spherical and varied particles size in traditional one. Creaming index, centrifugation test, conductivity and freeze-thaw cycles were used to evaluate all type of prepared emulsion stability. The nanoemulsion particles of sesame oil were found to be more stable than those of traditional one. These results indicated that the nanoemulsion process could increase the stability of prepared emulsion. Thus, using of nanoemulsion technique could be used as commercial way to enhance the stability of prepared emulsion.
Keywords
Download Citation
Endnote/Zotero/Mendeley (RIS)BibTeX
- N. Nayar, Sesame, ed.: N.W. Simmonds, In: Evolution of Crop Plants, Longman: London, pp: 231-233 (1984). .
- H. Zebib, G. Bultosa and S. Abera, Agric. Sci., 6, 238 (2015); https://doi.org/10.4236/as.2015.62024.
- M.N. Nagendra Prasad, K.R. Sanjay, D.S. Prasad, N. Vijay, R. Kothari and S. Nanjunda Swamy, J. Nutr. Food Sci., 2, 127 (2012); https://doi.org/10.4172/2155-9600.1000127.
- A. Asghar, M.N. Majeed and M.N. Akhtar, Am. J. Food Nutr., 4, 21 (2014); https://doi.org/10.5251/ajfn.2014.4.1.21.34.
- N. Pathak, A.K. Rai, R. Kumari and K.V. Bhat, Pharmacogn. Rev., 8, 147 (2014); https://doi.org/10.4103/0973-7847.134249.
- S. Kale and S. Deore, Syst. Rev. Pharm., 8, 39 (2016); https://doi.org/10.5530/srp.2017.1.8.
- D. McClements, Food Emulsions: Principles, Practice and Techniques, CRC Press: Washington, USA (2004).
- H. Mirhosseini, C. Tan, N. Hamid and S. Yusof, Food Hydrocol., 22, 1212 (2008); https://doi.org/10.1016/j.foodhyd.2007.06.011.
- K. Silva, M. Rocha-Leão and M. Coelho, J. Food Eng., 97, 335 (2010); https://doi.org/10.1016/j.jfoodeng.2009.10.026.
- T. Mason, J. Wilking, K. Meleson, C. Chang and S. Graves, J. Phys. Condens. Matter, 18, 635 (2006); https://doi.org/10.1088/0953-8984/18/41/R01.
- V. Ghosh, A. Mukherjee and N. Chandrasekaran, J. Pure Appl. Ultrason., 37, 53 (2015).
- M. Hassan, World J. Dairy Food Sci., 7, 195 (2012).
- AOAC, Association of Official Analytical Chemists: Official Methods of Analysis, edn 17, Washington DC. USA (2005).
- P. Pellet and S. Sossy, Food Composition Tables for Use in the Middle East, American University of Beirut, Beirut- Lebanon (1970).
- S. Eknayake, E.R. Jansz and B.M. Nair, Food Chem., 66, 115 (1999); https://doi.org/10.1016/S0308-8146(99)00041-2.
- S. O’Keefe and O. Pike, ed.: S.S. Nielsen, Fat Characterization, In: Food Analysis, Purdue University, West Lafayette, IN, USA, edn 4, pp. 239-259 (2010).
- I.C. Omar, N. Nishio and S. Nagai, Agric. Biol. Chem., 51, 2152 (1987); https://doi.org/10.1271/bbb1961.51.2145.
- P. Rocha-Filho, M. Camargo, M. Ferrari and M. Maruno, J. Nanomed. Nanotechnol., 5, 198 (2014); https://doi.org/10.4172/2157-7439.1000198.
- S. Sarojini, K. Sundar, C.H. Anjali and A. Ravindran, Biotechnol. Indian J., 9, 171 (2014).
- M. Ali, M. Alam, N. Alam and M. Siddiqui, Iran. J. Pharm. Res., 13, 1125 (2014).
- N. Sanjeewani and M. Sakeena, Int. J. Sci. Res. Publ., 3, 1 (2013).
- K. Silva, I. Gouveia, I. Farias, R. Santiago and E. Egito, Designing Sesame Oil Emulsions for Sunscreen Activities, In: XVIIth International Conference on Bioencapsulation, Groningen, Netherlands, vol. 70, pp. 1-4 (2009).
- K. Gomez and A. Gomez, Statistical Procedures for Agricultural Research, John Wiley & Sons Inc.: New York vol. 2 (1984).
- T.Y. Tunde-Akintunde, M.O. Oke and B.O. Akintunde, ed.: G.A. Uduak, Sesame Seed, In: Oilseeds, InTech, pp. 81-98 (2012).
- M. El Khier, K. Ishag and A. Yagoub, Res. J. Agric. Biol. Sci., 4, 761 (2008).
- R. Ghotbi, M. Khatibzadeh and S. Kordbacheh, (2014) Preparation of neem seed oil nanoemulsion, In Proceedings of the 5th International Conference on Nanotechnology: Fundamentals and Applications, Prague, Czech Republic, 150: 11-13.
- V. Ghosh, S. Saranya, A. Mukherjee and N. Chandrasekaran, J. Nanosci. Nanotechnol., 13, 114 (2013); https://doi.org/10.1166/jnn.2013.6701.
- D. Bernardi, T. Pereira, N. Maciel, J. Bortoloto, G. Viera, G. Oliveira and P. Rocha-Filho, J. Nanobiotechnol., 9, 44 (2011); https://doi.org/10.1186/1477-3155-9-44.
- N.U. Okur, S. Apaydin, N.U. Karabay-Yavasoglu, A. Yavasoglu and H.Y. Karasulu, Int. J. Pharm., 416, 136 (2011); https://doi.org/10.1016/j.ijpharm.2011.06.026.
- K. Gurpreet and S.K. Singh, Indian J. Pharm. Sci., 80, 781 (2018); https://doi.org/10.4172/pharmaceutical-sciences.1000422.
References
N. Nayar, Sesame, ed.: N.W. Simmonds, In: Evolution of Crop Plants, Longman: London, pp: 231-233 (1984). .
H. Zebib, G. Bultosa and S. Abera, Agric. Sci., 6, 238 (2015); https://doi.org/10.4236/as.2015.62024.
M.N. Nagendra Prasad, K.R. Sanjay, D.S. Prasad, N. Vijay, R. Kothari and S. Nanjunda Swamy, J. Nutr. Food Sci., 2, 127 (2012); https://doi.org/10.4172/2155-9600.1000127.
A. Asghar, M.N. Majeed and M.N. Akhtar, Am. J. Food Nutr., 4, 21 (2014); https://doi.org/10.5251/ajfn.2014.4.1.21.34.
N. Pathak, A.K. Rai, R. Kumari and K.V. Bhat, Pharmacogn. Rev., 8, 147 (2014); https://doi.org/10.4103/0973-7847.134249.
S. Kale and S. Deore, Syst. Rev. Pharm., 8, 39 (2016); https://doi.org/10.5530/srp.2017.1.8.
D. McClements, Food Emulsions: Principles, Practice and Techniques, CRC Press: Washington, USA (2004).
H. Mirhosseini, C. Tan, N. Hamid and S. Yusof, Food Hydrocol., 22, 1212 (2008); https://doi.org/10.1016/j.foodhyd.2007.06.011.
K. Silva, M. Rocha-Leão and M. Coelho, J. Food Eng., 97, 335 (2010); https://doi.org/10.1016/j.jfoodeng.2009.10.026.
T. Mason, J. Wilking, K. Meleson, C. Chang and S. Graves, J. Phys. Condens. Matter, 18, 635 (2006); https://doi.org/10.1088/0953-8984/18/41/R01.
V. Ghosh, A. Mukherjee and N. Chandrasekaran, J. Pure Appl. Ultrason., 37, 53 (2015).
M. Hassan, World J. Dairy Food Sci., 7, 195 (2012).
AOAC, Association of Official Analytical Chemists: Official Methods of Analysis, edn 17, Washington DC. USA (2005).
P. Pellet and S. Sossy, Food Composition Tables for Use in the Middle East, American University of Beirut, Beirut- Lebanon (1970).
S. Eknayake, E.R. Jansz and B.M. Nair, Food Chem., 66, 115 (1999); https://doi.org/10.1016/S0308-8146(99)00041-2.
S. O’Keefe and O. Pike, ed.: S.S. Nielsen, Fat Characterization, In: Food Analysis, Purdue University, West Lafayette, IN, USA, edn 4, pp. 239-259 (2010).
I.C. Omar, N. Nishio and S. Nagai, Agric. Biol. Chem., 51, 2152 (1987); https://doi.org/10.1271/bbb1961.51.2145.
P. Rocha-Filho, M. Camargo, M. Ferrari and M. Maruno, J. Nanomed. Nanotechnol., 5, 198 (2014); https://doi.org/10.4172/2157-7439.1000198.
S. Sarojini, K. Sundar, C.H. Anjali and A. Ravindran, Biotechnol. Indian J., 9, 171 (2014).
M. Ali, M. Alam, N. Alam and M. Siddiqui, Iran. J. Pharm. Res., 13, 1125 (2014).
N. Sanjeewani and M. Sakeena, Int. J. Sci. Res. Publ., 3, 1 (2013).
K. Silva, I. Gouveia, I. Farias, R. Santiago and E. Egito, Designing Sesame Oil Emulsions for Sunscreen Activities, In: XVIIth International Conference on Bioencapsulation, Groningen, Netherlands, vol. 70, pp. 1-4 (2009).
K. Gomez and A. Gomez, Statistical Procedures for Agricultural Research, John Wiley & Sons Inc.: New York vol. 2 (1984).
T.Y. Tunde-Akintunde, M.O. Oke and B.O. Akintunde, ed.: G.A. Uduak, Sesame Seed, In: Oilseeds, InTech, pp. 81-98 (2012).
M. El Khier, K. Ishag and A. Yagoub, Res. J. Agric. Biol. Sci., 4, 761 (2008).
R. Ghotbi, M. Khatibzadeh and S. Kordbacheh, (2014) Preparation of neem seed oil nanoemulsion, In Proceedings of the 5th International Conference on Nanotechnology: Fundamentals and Applications, Prague, Czech Republic, 150: 11-13.
V. Ghosh, S. Saranya, A. Mukherjee and N. Chandrasekaran, J. Nanosci. Nanotechnol., 13, 114 (2013); https://doi.org/10.1166/jnn.2013.6701.
D. Bernardi, T. Pereira, N. Maciel, J. Bortoloto, G. Viera, G. Oliveira and P. Rocha-Filho, J. Nanobiotechnol., 9, 44 (2011); https://doi.org/10.1186/1477-3155-9-44.
N.U. Okur, S. Apaydin, N.U. Karabay-Yavasoglu, A. Yavasoglu and H.Y. Karasulu, Int. J. Pharm., 416, 136 (2011); https://doi.org/10.1016/j.ijpharm.2011.06.026.
K. Gurpreet and S.K. Singh, Indian J. Pharm. Sci., 80, 781 (2018); https://doi.org/10.4172/pharmaceutical-sciences.1000422.