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Vol. 31 No. 12 (2019): Vol 31 Issue 12

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Extraction of Essential Oils from Vietnam’s Orange (Citrus sinensis) Peels by Hydrodistillation: Modeling and Process Optimization

https://doi.org/10.14233/ajchem.2019.22178
Tan Phat Dao
Center of Excellence for Biochemistry and Natural Products, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam & NTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam
Thien Hien Tran
Center of Excellence for Biochemistry and Natural Products, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam & NTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam
Thi Cam Quyen Ngo
Center of Excellence for Biochemistry and Natural Products, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam & NTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam
Huynh Thi Kieu Linh
BKU Institute of Advanced Applied Science and Technology, Ho Chi Minh City, Vietnam
Le Nguyen Yen Trung
BKU Institute of Advanced Applied Science and Technology, Ho Chi Minh City, Vietnam
Vo Thanh Danh
BKU Institute of Advanced Applied Science and Technology, Ho Chi Minh City, Vietnam
Thuy Trang Le Ngoc
Institute of Applied Materials Science, Vietnam Academy of Science and Technology, Ho Chi Minh City, Vietnam
Nguyen Dong Yen Pham
Institute of Applied Materials Science, Vietnam Academy of Science and Technology, Ho Chi Minh City, Vietnam
Pham Minh Quan
Institute of Natural Products Chemistry, Vietnam Academy of Science and Technology, Hanoi City, Vietnam & Graduate University of Science and Technology, Vietnam Academy of Science and Technology, Hanoi City, Vietnam
Tran Quoc Toan
Institute of Natural Products Chemistry, Vietnam Academy of Science and Technology, Hanoi City, Vietnam & Graduate University of Science and Technology, Vietnam Academy of Science and Technology, Hanoi City, Vietnam

Corresponding Author(s) : Tran Quoc Toan

tranquoctoan2010@gmail.com

Asian Journal of Chemistry, Vol. 31 No. 12 (2019): Vol 31 Issue 12

Abstract

In this study, extraction of essential oil from orange peels was investigated by hydrodistillation method and combine technology software to optimize the process. By using the response surface methodology (RSM) based on Box-Behnken surface statistical design, the effect of parameters such as water-to-material ratio (2-4 mL/g), extraction time (45-75 min), and temperature (120-140 ºC) on the extraction of essential oil process from orange (Citrus sinensis) peels was examined. All factors were significantly affected to the extraction yield of essential orange peel oil. Optimum conditions for extraction oil yield including the ratio of water to material, temperature, extraction time achieved 3.19 mL/g, 130.08 ºC, 74.31 min, respectively. Below the optimal extraction condition, the maximum yield of orange oil of 3.21 % was obtained. Using gas chromatography/mass spectrometry (GC/MS), the results revealed that the essential orange peels oil is extremely rich in limonene (98.343 %).

Keywords

Orange peel Citrus sinensis Hydrodistillation Response surface methodology Central composite design GC-MS
Dao, T. P., Tran, T. H., Quyen Ngo, T. C., Kieu Linh, H. T., Yen Trung, L. N., Danh, V. T., … Toan, T. Q. (2019). Extraction of Essential Oils from Vietnam’s Orange (Citrus sinensis) Peels by Hydrodistillation: Modeling and Process Optimization. Asian Journal of Chemistry, 31(12), 2827–2833. https://doi.org/10.14233/ajchem.2019.22178
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