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This work is licensed under a Creative Commons Attribution 4.0 International License.
Essential Oil Hydrodistillation Process from Vietnamese Calamondin (Citrus microcarpa) Peels and GC/MS Analysis of Essential Oils Components
Corresponding Author(s) : Le Thi Hong Nhan
Asian Journal of Chemistry,
Vol. 31 No. 11 (2019): Vol 31 Issue 11
Abstract
The essential oil of Citrus microcarpa peels was applied in many fields, and the methods to improve the efficiency of citrus exploitation were increasingly concerned. In this study, citrus essential oil was extracted from calamondin by hydrodistillation. This study was carried out to investigate the factors affecting the distillation of essential oils. The highest performance of the distillation process was 2.45 % with optimal conditions (material-water ratio of 1:3 g/mL, time of 2 h, the temperature of 120 ºC). Moreover, calamondin (Citrus microcarpa) peels oil extract was analyzed by gas chromatography-mass spectrometry (GC-MS). The primary compound of calamondin essential oil include limonene 96.925 %, β-myrcene 1.424 %, 1R-α-pinene 0.561 %, cyclohexene 0.343 %, 1R-α-pinene 0.561 % and β-cubebene 0.598 %.
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- E. Christaki, E. Bonos, I. Giannenas and P. Florou-Paneri, Agriculture, 2, 228 (2012); https://doi.org/10.3390/agriculture2030228.
- Q.T. Tran, T.T.T. Le, M.Q. Pham, T.L. Do, M.H. Vu, D.C. Nguyen, L.G. Bach, L.M. Bui and Q.L. Pham, Molecules, 24, 895 (2019); https://doi.org/10.3390/molecules24050895.
- F. Bakkali, S. Averbeck, D. Averbeck and M. Idaomar, Food Chem. Toxicol., 46, 446 (2008); https://doi.org/10.1016/j.fct.2007.09.106.
- C. Benchaar, S. Calsamiglia, A.V. Chaves, G.R. Fraser, D. Colombatto, T.A. McAllister and K.A. Beauchemin, Anim. Feed Sci. Technol., 145, 209 (2008); https://doi.org/10.1016/j.anifeedsci.2007.04.014.
- M.G. Miguel, Flavour Fragr. J., 25, 291 (2010); https://doi.org/10.1002/ffj.1961.
- H. Zhai, H. Liu, S. Wang, J. Wu and A.M. Kluenter, An. Nutr., 4, 179 (2018); https://doi.org/10.1016/j.aninu.2018.01.005.
- R.A.Khan, Saudi Pharm. J., 26, 739 (2018); https://doi.org/10.1016/j.jsps.2018.02.015.
- T.H. Tran, H.H.H. Nguyen, D.C. Nguyen, T.Q. Nguyen, H. Tan, L.T.H. Nhan, D.H. Nguyen, L.D. Tran, S.T. Do and T.D. Nguyen, Processes, 6, 206 (2018); https://doi.org/10.3390/pr6110206.
- T.H. Tran, P.T.N. Nguyen, T.N. Pham, D.C. Nguyen, T.P. Dao, D.T. Nguyen, N.D. Hai, D.V.N. Vo, X.T. Le, N.T.H. Le and L.G. Bach, IOP Conf. Series Mater. Sci. Eng., 479, 012002 (2019); https://doi.org/10.1088/1757-899X/479/1/012002.
- L. Wang, V. Ravichandran, Y. Yin, J. Yin and Y. Zhang, Trends Biotechnol., 37, 492 (2019); https://doi.org/10.1016/j.tibtech.2018.10.003.
- Y. Fu, J. Luo, J. Qin and M. Yang, J. Pharm. Biomed. Anal., 168, 189 (2019); https://doi.org/10.1016/j.jpba.2019.02.027.
- S. Hu, X. Chen, R. Wang, L. Yang and X. Bai, TrAC Trends Anal. Chem., 113, 340 (2019); https://doi.org/10.1016/j.trac.2018.11.006.
- S. Dutta, S. Mahalanobish, S. Saha, S. Ghosh and P.C. Sil, Food Chem. Toxicol., 128, 240 (2019); https://doi.org/10.1016/j.fct.2019.04.012.
- M. Muchtaridi, C.S. Bing, A.S. Abdurrahim and H.A. Wahab, Asian J. Chem., 26, S59 (2014); https://doi.org/10.14233/ajchem.2014.19013.
- H.Y. Yen and Y.C. Lin, Ind. Crops Prod., 108, 716 (2017); https://doi.org/10.1016/j.indcrop.2017.07.039.
- G. Mitropoulou, E. Fitsiou, K. Spyridopoulou, A. Tiptiri-Kourpeti, H. Bardouki and M. Vamvakias, LWT-Food Technol., 84, 344 (2017); https://doi.org/10.1016/j.lwt.2017.05.036.
- F. Wu, Y. Jin, X. Xu and N. Yang, J. Clean. Prod., 159, 85 (2017); https://doi.org/10.1016/j.jclepro.2017.05.010.
- A.K. Maurya, S. Mohanty, A. Pal, C.S. Chanotiya and D.U. Bawankule, J. Ethnopharmacol., 212, 86 (2018); https://doi.org/10.1016/j.jep.2017.10.018.
- S.K. Fagodia, H.P. Singh, D.R. Batish and R.K. Kohli, Ind. Crops Prod., 108, 708 (2017); https://doi.org/10.1016/j.indcrop.2017.07.005.
- S.A.H. Rizvi, S. Ling, F. Tian, F. Xie and X. Zeng, Ind. Crops Prod., 121, 468 (2018); https://doi.org/10.1016/j.indcrop.2018.05.031.
- E. Baba, Ü. Acar, C. Öntas, O.S. Kesbic and S. Yilma, Aquaculture, 465, 13 (2016); https://doi.org/10.1016/j.aquaculture.2016.08.023.
- D. Gonçalves, C.C. Koshima, F.R.M. Batista and C.E.C. Rodrigues, Chem. Eng. Res. Des., 137, 566 (2018); https://doi.org/10.1016/j.cherd.2018.08.008.
- M.W. Cheong, Z.S. Chong, S.Q. Liu, W. Zhou, P. Curran and B. Yu, Food Chem., 134, 686 (2012); https://doi.org/10.1016/j.foodchem.2012.02.162.
- M.W. Cheong, D. Zhu, J. Sng, S.Q. Liu, W. Zhou, P. Curran and B. Yu, Food Chem., 134, 696 (2012); https://doi.org/10.1016/j.foodchem.2012.02.139.
- Q. Li, P. Ning, L. Zheng, J. Huang, G. Li and T. Hsiang, Postharvest Biol. Technol., 58, 157 (2010); https://doi.org/10.1016/j.postharvbio.2010.06.003.
- T.H. Tran, L.K. Ha, D.C. Nguyen, T.P. Dao, L.T.H. Nhan, D.H. Nguyen, T.D. Nguyen, D.V.N. Vo, Q.T. Tran and L.G. Bach, Processes, 7, 56 (2019); https://doi.org/10.3390/pr7020056.
- R. Manouchehri, M.J. Saharkhiz, A. Karami and M. Niakousari, Sustain. Chem. Pharm., 8, 76 (2018); https://doi.org/10.1016/j.scp.2018.03.002.
- H. Cui, H.W. Pan, P.H. Wang, X.D. Yang, W.C. Zhai, Y. Dong and H.L. Zhou, Ind. Crops Prod., 124, 669 (2018); https://doi.org/10.1016/j.indcrop.2018.08.041.
- L.P. Stanojevic, N.S. Radulovic, T.M. Djokic, B.M. Stankovic, D.P. Ilicm, M.D. Cakicm and V.D. Nikolic, Ind. Crops Prod., 65, 429 (2015); https://doi.org/10.1016/j.indcrop.2014.10.067.
- M. Dhobi, V. Mandal and S. Hemalatha, J. Chem. Metrol., 3, 13 (2009).
- M.A. Ferhat, B.Y. Meklati, J. Smadja and F. Chemat, J. Chromatogr. A, 1112, 121 (2006); https://doi.org/10.1016/j.chroma.2005.12.030.
- M.N. Boukhatem, M.A. Ferhat, A. Kameli, F. Saidi and H.T. Kebir, Libyan J. Med., 9, 25431 (2014); https://doi.org/10.3402/ljm.v9.25431.
- L. Cuevas-Glory, E. Sauri-Duch and J.A. Pino, J. Essen. Oil Bearing Plants, 12, 656 (2009); https://doi.org/10.1080/0972060X.2009.10643770.
- H.S. Choi, J. Agric. Food Chem., 53, 1642 (2005); https://doi.org/10.1021/jf040324x.
- G.W. Mcgraw, R.W. Hemingway, L.L. Ingram, C.S. Canady and W.B. Mcgraw, Environ. Sci. Technol., 33, 4029 (1999); https://doi.org/10.1021/es9810641.
References
E. Christaki, E. Bonos, I. Giannenas and P. Florou-Paneri, Agriculture, 2, 228 (2012); https://doi.org/10.3390/agriculture2030228.
Q.T. Tran, T.T.T. Le, M.Q. Pham, T.L. Do, M.H. Vu, D.C. Nguyen, L.G. Bach, L.M. Bui and Q.L. Pham, Molecules, 24, 895 (2019); https://doi.org/10.3390/molecules24050895.
F. Bakkali, S. Averbeck, D. Averbeck and M. Idaomar, Food Chem. Toxicol., 46, 446 (2008); https://doi.org/10.1016/j.fct.2007.09.106.
C. Benchaar, S. Calsamiglia, A.V. Chaves, G.R. Fraser, D. Colombatto, T.A. McAllister and K.A. Beauchemin, Anim. Feed Sci. Technol., 145, 209 (2008); https://doi.org/10.1016/j.anifeedsci.2007.04.014.
M.G. Miguel, Flavour Fragr. J., 25, 291 (2010); https://doi.org/10.1002/ffj.1961.
H. Zhai, H. Liu, S. Wang, J. Wu and A.M. Kluenter, An. Nutr., 4, 179 (2018); https://doi.org/10.1016/j.aninu.2018.01.005.
R.A.Khan, Saudi Pharm. J., 26, 739 (2018); https://doi.org/10.1016/j.jsps.2018.02.015.
T.H. Tran, H.H.H. Nguyen, D.C. Nguyen, T.Q. Nguyen, H. Tan, L.T.H. Nhan, D.H. Nguyen, L.D. Tran, S.T. Do and T.D. Nguyen, Processes, 6, 206 (2018); https://doi.org/10.3390/pr6110206.
T.H. Tran, P.T.N. Nguyen, T.N. Pham, D.C. Nguyen, T.P. Dao, D.T. Nguyen, N.D. Hai, D.V.N. Vo, X.T. Le, N.T.H. Le and L.G. Bach, IOP Conf. Series Mater. Sci. Eng., 479, 012002 (2019); https://doi.org/10.1088/1757-899X/479/1/012002.
L. Wang, V. Ravichandran, Y. Yin, J. Yin and Y. Zhang, Trends Biotechnol., 37, 492 (2019); https://doi.org/10.1016/j.tibtech.2018.10.003.
Y. Fu, J. Luo, J. Qin and M. Yang, J. Pharm. Biomed. Anal., 168, 189 (2019); https://doi.org/10.1016/j.jpba.2019.02.027.
S. Hu, X. Chen, R. Wang, L. Yang and X. Bai, TrAC Trends Anal. Chem., 113, 340 (2019); https://doi.org/10.1016/j.trac.2018.11.006.
S. Dutta, S. Mahalanobish, S. Saha, S. Ghosh and P.C. Sil, Food Chem. Toxicol., 128, 240 (2019); https://doi.org/10.1016/j.fct.2019.04.012.
M. Muchtaridi, C.S. Bing, A.S. Abdurrahim and H.A. Wahab, Asian J. Chem., 26, S59 (2014); https://doi.org/10.14233/ajchem.2014.19013.
H.Y. Yen and Y.C. Lin, Ind. Crops Prod., 108, 716 (2017); https://doi.org/10.1016/j.indcrop.2017.07.039.
G. Mitropoulou, E. Fitsiou, K. Spyridopoulou, A. Tiptiri-Kourpeti, H. Bardouki and M. Vamvakias, LWT-Food Technol., 84, 344 (2017); https://doi.org/10.1016/j.lwt.2017.05.036.
F. Wu, Y. Jin, X. Xu and N. Yang, J. Clean. Prod., 159, 85 (2017); https://doi.org/10.1016/j.jclepro.2017.05.010.
A.K. Maurya, S. Mohanty, A. Pal, C.S. Chanotiya and D.U. Bawankule, J. Ethnopharmacol., 212, 86 (2018); https://doi.org/10.1016/j.jep.2017.10.018.
S.K. Fagodia, H.P. Singh, D.R. Batish and R.K. Kohli, Ind. Crops Prod., 108, 708 (2017); https://doi.org/10.1016/j.indcrop.2017.07.005.
S.A.H. Rizvi, S. Ling, F. Tian, F. Xie and X. Zeng, Ind. Crops Prod., 121, 468 (2018); https://doi.org/10.1016/j.indcrop.2018.05.031.
E. Baba, Ü. Acar, C. Öntas, O.S. Kesbic and S. Yilma, Aquaculture, 465, 13 (2016); https://doi.org/10.1016/j.aquaculture.2016.08.023.
D. Gonçalves, C.C. Koshima, F.R.M. Batista and C.E.C. Rodrigues, Chem. Eng. Res. Des., 137, 566 (2018); https://doi.org/10.1016/j.cherd.2018.08.008.
M.W. Cheong, Z.S. Chong, S.Q. Liu, W. Zhou, P. Curran and B. Yu, Food Chem., 134, 686 (2012); https://doi.org/10.1016/j.foodchem.2012.02.162.
M.W. Cheong, D. Zhu, J. Sng, S.Q. Liu, W. Zhou, P. Curran and B. Yu, Food Chem., 134, 696 (2012); https://doi.org/10.1016/j.foodchem.2012.02.139.
Q. Li, P. Ning, L. Zheng, J. Huang, G. Li and T. Hsiang, Postharvest Biol. Technol., 58, 157 (2010); https://doi.org/10.1016/j.postharvbio.2010.06.003.
T.H. Tran, L.K. Ha, D.C. Nguyen, T.P. Dao, L.T.H. Nhan, D.H. Nguyen, T.D. Nguyen, D.V.N. Vo, Q.T. Tran and L.G. Bach, Processes, 7, 56 (2019); https://doi.org/10.3390/pr7020056.
R. Manouchehri, M.J. Saharkhiz, A. Karami and M. Niakousari, Sustain. Chem. Pharm., 8, 76 (2018); https://doi.org/10.1016/j.scp.2018.03.002.
H. Cui, H.W. Pan, P.H. Wang, X.D. Yang, W.C. Zhai, Y. Dong and H.L. Zhou, Ind. Crops Prod., 124, 669 (2018); https://doi.org/10.1016/j.indcrop.2018.08.041.
L.P. Stanojevic, N.S. Radulovic, T.M. Djokic, B.M. Stankovic, D.P. Ilicm, M.D. Cakicm and V.D. Nikolic, Ind. Crops Prod., 65, 429 (2015); https://doi.org/10.1016/j.indcrop.2014.10.067.
M. Dhobi, V. Mandal and S. Hemalatha, J. Chem. Metrol., 3, 13 (2009).
M.A. Ferhat, B.Y. Meklati, J. Smadja and F. Chemat, J. Chromatogr. A, 1112, 121 (2006); https://doi.org/10.1016/j.chroma.2005.12.030.
M.N. Boukhatem, M.A. Ferhat, A. Kameli, F. Saidi and H.T. Kebir, Libyan J. Med., 9, 25431 (2014); https://doi.org/10.3402/ljm.v9.25431.
L. Cuevas-Glory, E. Sauri-Duch and J.A. Pino, J. Essen. Oil Bearing Plants, 12, 656 (2009); https://doi.org/10.1080/0972060X.2009.10643770.
H.S. Choi, J. Agric. Food Chem., 53, 1642 (2005); https://doi.org/10.1021/jf040324x.
G.W. Mcgraw, R.W. Hemingway, L.L. Ingram, C.S. Canady and W.B. Mcgraw, Environ. Sci. Technol., 33, 4029 (1999); https://doi.org/10.1021/es9810641.