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Vol. 23 No. 2 (2011): Vol 23 Issue 2

Copyright (c) 2010 Wenzheng Xia, Zaifu Pan, Jialin Chen, Qingsong Ye, Weiping Liu

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A Facile Synthesis and Thermal Stability of cis-[Pd(NH3)2(C2O4)]

Wenzheng Xia
State Key Lab of Advanced Technologies for Platinum Metals, Kunming Institute of Precious Metals, Kunming 650106, P.R. China
Zaifu Pan
State Key Lab of Advanced Technologies for Platinum Metals, Kunming Institute of Precious Metals, Kunming 650106, P.R. China
Jialin Chen
State Key Lab of Advanced Technologies for Platinum Metals, Kunming Institute of Precious Metals, Kunming 650106, P.R. China
Qingsong Ye
State Key Lab of Advanced Technologies for Platinum Metals, Kunming Institute of Precious Metals, Kunming 650106, P.R. China
Weiping Liu
State Key Lab of Advanced Technologies for Platinum Metals, Kunming Institute of Precious Metals, Kunming 650106, P.R. China

Corresponding Author(s) : Qingsong Ye

qingsongye@126.com

Asian Journal of Chemistry, Vol. 23 No. 2 (2011): Vol 23 Issue 2

Abstract

A simple and facile method for synthesis of cis-[Pd(NH3)2(C2O4)] has been developed and the thermal decomposition behaviour investigated with TG-DTA under air and nitrogen atmosphere. The complex was prepared by the direct reaction of palladium chloride with ammonium oxalate at mild temperature and the yield was up to 76 %. cis-[Pd(NH3)2(C2O4)] undergoes the thermal decomposition, respectively, at 180 ºC in air and 172 ºC in N2, leading to the formation of Pd powder and CO2 and NH3 as the gas products.

Keywords

Diammineoxalatopalladium Synthesis Characterization Thermal decomposition behaviour
Xia, W., Pan, Z., Chen, J., Ye, Q., & Liu, W. (2010). A Facile Synthesis and Thermal Stability of cis-[Pd(NH3)2(C2O4)]. Asian Journal of Chemistry, 23(2), 785–787. Retrieved from https://asianpubs.org/index.php/ajchem/article/view/31690
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