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Vol. 30 No. 8 (2018): Vol 30 Issue 8

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Determination of Diazinon and Carbofuran Residue Levels in Apples Kept in Cold Storage Depots in Karaman Province, Turkey

https://doi.org/10.14233/ajchem.2018.21237%20
Fevzi Kilicel1
1Department of Chemistry, Faculty of Science, Karamanoglu Mehmetbey University, 70100 Karaman, Turkey 2Department of Chemistry, Institute of Science, Karamanoglu Mehmetbey University, 70100 Karaman, Turkey *Corresponding author: E-mail: fevzi@kmu.edu.tr
Hacer Sibel Karapinar2
1Department of Chemistry, Faculty of Science, Karamanoglu Mehmetbey University, 70100 Karaman, Turkey 2Department of Chemistry, Institute of Science, Karamanoglu Mehmetbey University, 70100 Karaman, Turkey *Corresponding author: E-mail: fevzi@kmu.edu.tr
Ihsan Serin2
1Department of Chemistry, Faculty of Science, Karamanoglu Mehmetbey University, 70100 Karaman, Turkey 2Department of Chemistry, Institute of Science, Karamanoglu Mehmetbey University, 70100 Karaman, Turkey *Corresponding author: E-mail: fevzi@kmu.edu.tr

Asian Journal of Chemistry, Vol. 30 No. 8 (2018): Vol 30 Issue 8

Abstract

In this study, two pesticides viz., diazinon and carbofuran residue levels that is used in agricultural spraying in apple samples that were harvested in 2014 harvest season and kept in cold storage in Karaman province, were examined by gas chromatography-mass spectrometer (GC-MS) and gas chromatography-flame-ionisation detector (GC-FID) method. The samples that were taken from 6 different cold storages in the region at 5 different time zones, were kept in laboratory in refrigerator at + 4 °C. The residue levels of diazinon and carbofuran pesticides in apple samples were determined. In order to identify pesticides residues at least three apple samples that were chosen randomly, were homogenized by homogenizator. In extract of samples QuEChERS method was used since it is fast, easy, low-cost, effective and reliable method. The residues of pesticides were taken from this homogenate with acetonitrile and given to GC-MS equipment in a suitable way. According to the results, carbofuran and diazinon pesticides types that are forbidden in Turkey, were determined in large amount of samples.

Keywords

Apple Pesticides Medicine residue Carbofuran Diazinon.
Kilicel1, F., Sibel Karapinar2, H., & Serin2, I. (2018). Determination of Diazinon and Carbofuran Residue Levels in Apples Kept in Cold Storage Depots in Karaman Province, Turkey. Asian Journal of Chemistry, 30(8), 1701–1705. https://doi.org/10.14233/ajchem.2018.21237
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