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Vol. 30 No. 11 (2018): Vol 30 Issue 11

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Synthesis and Characterization of [(PbX2)2.L1] and [(PbX2)2.(MCl2).L1] Compounds with Macrocyclic Ligand

https://doi.org/10.14233/ajchem.2018.21404
Abhishek Kumar
Department of Chemistry, University of Allahabad, Allahabad-211 002, India
Shishir Malviya
Department of Chemistry, University of Allahabad, Allahabad-211 002, India
Rajeev Lohia
Department of Chemistry, University of Allahabad, Allahabad-211 002, India
Toyaj Shukla
Department of Chemistry, University of Allahabad, Allahabad-211 002, India
Shekhar Srivastava
Department of Chemistry, University of Allahabad, Allahabad-211 002, India

Corresponding Author(s) : Abhishek Kumar

abhishekrajpoot02@gmail.com

Asian Journal of Chemistry, Vol. 30 No. 11 (2018): Vol 30 Issue 11

Abstract

We have synthesized different types of macrocyclic compounds [(PbX2)2.L1] and [(PbX2)2.(MCl2).L1] with macrocyclic ligand (L1) i.e. 36,9,12,20,23,26,29,35,36- decaazatricyclo 29.3.1.114-18] hexatriaconta-1(34), 14,16,18(36) 31(35), 32-haxaene-2,13,19,30-tetraone ligand, where MCl2 = CuCl2 or CoCl2 or MnCl2 or NiCl2 or ZnCl2. The all synthesized complexes were characterized by elemental analysis, molar conductance, IR and X-ray photoelectron spectra (XPS) data.

Keywords

Binuclear and Macrocyclic complexes X-ray photoelectron spectroscopy Heavy metals
Kumar, A., Malviya, S., Lohia, R., Shukla, T., & Srivastava, S. (2018). Synthesis and Characterization of [(PbX2)2.L1] and [(PbX2)2.(MCl2).L1] Compounds with Macrocyclic Ligand. Asian Journal of Chemistry, 30(11), 2415–2420. https://doi.org/10.14233/ajchem.2018.21404
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