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Copyright (c) 2014 Mecit Aksu1
This work is licensed under a Creative Commons Attribution 4.0 International License.
Growth of Nano (Na)V2O5 from NaBH4 and V2O5 at Room Temperature
Corresponding Author(s) : Mecit Aksu1
Asian Journal of Chemistry,
Vol. 26 No. 23 (2014)
Abstract
In this work V2O5 was reduced to sodium intercalated NaV2O5 with NaBH4 in pyridine-water solvent. Techniques to investigate the composition, crystallinity and morphology of products as prepared include field emission scanning electron microscopy, energy dispersive X-ray spectroscopy and X-ray powder diffraction inductively coupled plasma-atomic emission spectroscopy. Unit cell parameters are a = 11.28, b = 3.583, c = 4.76 Å and a = b = g = 90°. Mean crystallite size was calculated to be 4.8 nm.
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- W. Cha, S. Chin, E. Park, S.T. Yun and J. Jurng, Powder Technol., 258, 352 (2014).
- L. Soltane and F. Sediri, Mater. Res. Bull., 53, 79 (2014).
- D. Chen, R. Yi, S. Chen, T. Xu, M.L. Gordin, D. Lv and D. Wang, Mater. Sci. Eng. B, 185, 7 (2014).
- D. Vernardou, M. Apostolopoulou, D. Louloudakis, N. Katsarakis and E. Koudoumas, J. Colloid Interf. Sci., 424, 1 (2014).
- I. Mjejri, N. Etteyeb and F. Sediri, Ceram. Int., 40, 5379 (2014).
- M. Guignard, C. Didier, J. Darriet, P. Bordet, E. Elkaïm and C. Delmas, Nat. Mater., 12, 74 (2012).
- C. Didier, M. Guignard, J. Darriet and C. Delmas, Inorg. Chem., 51, 11007 (2012).
- J.S. Ke, M.C. Wu, S.F. Weng and C.S. Lee, J. Nanopart. Res., 14, 1167 (2012).
- R.S. Devan, R.A. Patil, J.H. Lin and Y.R. Ma, Adv. Funct. Mater., 22, 3326 (2012).
- S. Tepavcevic, H. Xiong, V.R. Stamenkovic, X. Zuo, M. Balasubrama-nian, V.B. Prakapenka, C.S. Johnson, T. Rajh, ACS Nano, 6, 530 (2012).
- S. Yagoubi, L. El Ammari, A. Assani and M. Saadi, Acta Crystallogr., 67E, i60 (2011).
- W. Jiang, J. Ni, K. Yu and Z. Zhu, Appl. Surf. Sci., 257, 3253 (2011).
- H. Fang, W. Ying-jin, J. Tao, M. Xing, C. Gang and W. Chun-zhong, Chem. Res. Chin. Univ., 26, 291 (2010).
- Y.A. Bakhteeva, N.V. Podvalnaya and V.L. Volkov, Inorg. Mater., 46, 1112 (2010).
- F. Hu, X. Ming, G. Chen, C. Wang, A. Li, J. Li and Y. Wei, J. Alloys Comp., 479, 888 (2009).
References
W. Cha, S. Chin, E. Park, S.T. Yun and J. Jurng, Powder Technol., 258, 352 (2014).
L. Soltane and F. Sediri, Mater. Res. Bull., 53, 79 (2014).
D. Chen, R. Yi, S. Chen, T. Xu, M.L. Gordin, D. Lv and D. Wang, Mater. Sci. Eng. B, 185, 7 (2014).
D. Vernardou, M. Apostolopoulou, D. Louloudakis, N. Katsarakis and E. Koudoumas, J. Colloid Interf. Sci., 424, 1 (2014).
I. Mjejri, N. Etteyeb and F. Sediri, Ceram. Int., 40, 5379 (2014).
M. Guignard, C. Didier, J. Darriet, P. Bordet, E. Elkaïm and C. Delmas, Nat. Mater., 12, 74 (2012).
C. Didier, M. Guignard, J. Darriet and C. Delmas, Inorg. Chem., 51, 11007 (2012).
J.S. Ke, M.C. Wu, S.F. Weng and C.S. Lee, J. Nanopart. Res., 14, 1167 (2012).
R.S. Devan, R.A. Patil, J.H. Lin and Y.R. Ma, Adv. Funct. Mater., 22, 3326 (2012).
S. Tepavcevic, H. Xiong, V.R. Stamenkovic, X. Zuo, M. Balasubrama-nian, V.B. Prakapenka, C.S. Johnson, T. Rajh, ACS Nano, 6, 530 (2012).
S. Yagoubi, L. El Ammari, A. Assani and M. Saadi, Acta Crystallogr., 67E, i60 (2011).
W. Jiang, J. Ni, K. Yu and Z. Zhu, Appl. Surf. Sci., 257, 3253 (2011).
H. Fang, W. Ying-jin, J. Tao, M. Xing, C. Gang and W. Chun-zhong, Chem. Res. Chin. Univ., 26, 291 (2010).
Y.A. Bakhteeva, N.V. Podvalnaya and V.L. Volkov, Inorg. Mater., 46, 1112 (2010).
F. Hu, X. Ming, G. Chen, C. Wang, A. Li, J. Li and Y. Wei, J. Alloys Comp., 479, 888 (2009).