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Copyright (c) 2014 Lan-Qin Chai*, Jiao-Jiao Huang, Yao-Xin Li, Jian-Yu Zhang
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Synthesis and Crystal Structure of New Nitrogen Heterocyclic Compound
Corresponding Author(s) : Lan-Qin Chai*
Asian Journal of Chemistry,
Vol. 26 No. 20 (2014)
Abstract
An unexpected nitrogen heterocyclic compound has been synthesized originally. Furthermore, the compound was characterized by elemental analysis. The crystal structure of the title compound has been determined by single-crystal X-ray diffraction. It crystallizes in the orthorhombic space group Pmcn with a = 12.056(2) Å, b = 4.6016(8) Å, c = 22.185(6) Å, b = 90.00°, Z = 4. There are two fairly strong intramolecular C3-H3···N1 and C5-H5···N2 hydrogen bonds.
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- M.A. Pantaleo, E. Mishani, C. Nanni, L. Landuzzi, S. Boschi, G. Nicoletti, S. Dissoki, P. Paterini, P.P. Piccaluga, F. Lodi, P.L. Lollini, S. Fanti and G. Biasco, Mol. Imaging Biol., 12, 616 (2010).
- K.R. Grunwald, M. Volpe, P. Cias, G. Gescheidt and N.C. Mösch-Zanetti, Inorg. Chem., 50, 7478 (2011).
- Y.C. Chen and D.Y. Yang, Tetrahedron, 69, 10438 (2013).
- C.M. Martínez-Viturro and D. Domínguez, Heterocycl. Chem., 44, 1035 (2007).
- G. Liu, D.-Y. Hu, L.-H. Jin, B.-A. Song, S. Yang, P.-S. Liu, P.S. Bhadury, Y. Ma, H. Luo and X. Zhou, Bioorg. Med. Chem., 15, 6608 (2007).
- J.C. Liu, J. Cao, W.T. Deng and B.H. Chen, J. Chem. Crystallogr., 41, 806 (2011).
- J. Thurmond, M.E.R. Butchbach, M. Palomo, B. Pease, M. Rao, L. Bedell, M. Keyvan, G. Pai, R. Mishra, M. Haraldsson, T. Andresson, G. Bragason, M. Thosteinsdottir, J.M. Bjornsson, D.D. Coovert, A.H.M. Burghes, M.E. Gurney and J. Singh, J. Med. Chem., 51, 449 (2008).
- S.T. Al-Rashood, I.A. Aboldahab, M.N. Nagi, L.A. Abouzeid, A.A.M. Abdel-Aziz, S.G. Abdel-Hamide, K.M. Youssef, A.M. Al-Obaid and H.I. El-Subbagh, Bioorg. Med. Chem., 14, 8608 (2006).
- L.Q. Chai, Y.L. Zhang, J.F. Tong and G. Liu, Z. Naturforsch. B, 68, 239 (2013).
- S.H. Yang, D.B. Khadka, S.H. Cho, H.-K. Ju, K.Y. Lee, H.J. Han, K.-T. Lee and W.-J. Cho, Bioorg. Med. Chem., 19, 968 (2011).
- R. Alonso, A. Caballero, P.J. Campos, D. Sampedro and M.A. Rodríguez, Tetrahedron, 66, 4469 (2010).
- L.Q. Chai, G. Liu, Y.L. Zhang, J.J. Huang and J.F. Tong, J. Coord. Chem., 66, 3926 (2013).
- Bruker, SAINT and SMART, Bruker AXS Inc., Madison, WI, USA (2001).
- G.M. Sheldrick, SHELXS97, Program for Crystal Structure Determination, University of Göttingen, Germany (1996).
- G.M. Sheldrick, SADABS, University of Göttingen, Göttingen, Germany (2001).
- G.M. Sheldrick, Acta Crystallogr. A, 64, 112 (2008).
References
M.A. Pantaleo, E. Mishani, C. Nanni, L. Landuzzi, S. Boschi, G. Nicoletti, S. Dissoki, P. Paterini, P.P. Piccaluga, F. Lodi, P.L. Lollini, S. Fanti and G. Biasco, Mol. Imaging Biol., 12, 616 (2010).
K.R. Grunwald, M. Volpe, P. Cias, G. Gescheidt and N.C. Mösch-Zanetti, Inorg. Chem., 50, 7478 (2011).
Y.C. Chen and D.Y. Yang, Tetrahedron, 69, 10438 (2013).
C.M. Martínez-Viturro and D. Domínguez, Heterocycl. Chem., 44, 1035 (2007).
G. Liu, D.-Y. Hu, L.-H. Jin, B.-A. Song, S. Yang, P.-S. Liu, P.S. Bhadury, Y. Ma, H. Luo and X. Zhou, Bioorg. Med. Chem., 15, 6608 (2007).
J.C. Liu, J. Cao, W.T. Deng and B.H. Chen, J. Chem. Crystallogr., 41, 806 (2011).
J. Thurmond, M.E.R. Butchbach, M. Palomo, B. Pease, M. Rao, L. Bedell, M. Keyvan, G. Pai, R. Mishra, M. Haraldsson, T. Andresson, G. Bragason, M. Thosteinsdottir, J.M. Bjornsson, D.D. Coovert, A.H.M. Burghes, M.E. Gurney and J. Singh, J. Med. Chem., 51, 449 (2008).
S.T. Al-Rashood, I.A. Aboldahab, M.N. Nagi, L.A. Abouzeid, A.A.M. Abdel-Aziz, S.G. Abdel-Hamide, K.M. Youssef, A.M. Al-Obaid and H.I. El-Subbagh, Bioorg. Med. Chem., 14, 8608 (2006).
L.Q. Chai, Y.L. Zhang, J.F. Tong and G. Liu, Z. Naturforsch. B, 68, 239 (2013).
S.H. Yang, D.B. Khadka, S.H. Cho, H.-K. Ju, K.Y. Lee, H.J. Han, K.-T. Lee and W.-J. Cho, Bioorg. Med. Chem., 19, 968 (2011).
R. Alonso, A. Caballero, P.J. Campos, D. Sampedro and M.A. Rodríguez, Tetrahedron, 66, 4469 (2010).
L.Q. Chai, G. Liu, Y.L. Zhang, J.J. Huang and J.F. Tong, J. Coord. Chem., 66, 3926 (2013).
Bruker, SAINT and SMART, Bruker AXS Inc., Madison, WI, USA (2001).
G.M. Sheldrick, SHELXS97, Program for Crystal Structure Determination, University of Göttingen, Germany (1996).
G.M. Sheldrick, SADABS, University of Göttingen, Göttingen, Germany (2001).
G.M. Sheldrick, Acta Crystallogr. A, 64, 112 (2008).