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Determination of Metoclopramide with Chromium(III) Thiocyanate Complexes
Corresponding Author(s) : George Bratulescu
Asian Journal of Chemistry,
Vol. 28 No. 1 (2016): Vol 28 Issue 1
Abstract
The determination of metoclopramide (4-amino-5-chloro-N-[(2-diethylamino)ethyl]-2-methoxybenzamide) has been achieved by means of gravimetric, oxidimetric and spectrometric methods. The experimental data proves that the methods are accurate enough and not affected by systematic errors.
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- V. Zotta, Pharmaceutical Chemistry, Medicala Publishing House, Bucharest, p. 688 (1985) (in Romanian).
- M.S. Attia and M.M. Aboaly, Talanta, 82, 78 (2010); doi:10.1016/j.talanta.2010.03.062.
- J. Shah, M.R. Jan, M.A. Khan and S. Amin, J. Anal. Chem., 60, 633 (2005); doi:10.1007/s10809-005-0151-5.
- I. de Souza Silva, M.L.M.F.S. Saraiva, J.L.M. Santos and J.L.F.C. Lima, Spectrosc. Lett., 40, 51 (2007); doi:10.1080/00387010601093778.
- S.J. Wadher, P.R. Pathankar, M. Puranik, R.O. Ganjiwale and P.G. Yeole, Indian J. Pharm. Sci., 70, 393 (2008); doi:10.4103/0250-474X.43014.
- F.F. Belal, M.K. Sharaf El-Din, M.M. Tolba and H. Elmansi, J. Chromatogr. Sci., 52, 1224 (2014); doi:10.1093/chromsci/bmt202.
- S.T. Ulu, Chin. J. Chem., 30, 634 (2012); doi:10.1002/cjoc.201280001.
- M. Yan, H.D. Li, B.M. Chen, X.L. Liu and Y.G. Zhu, J. Chromatogr. B Analyt. Technol. Biomed. Life Sci., 878, 883 (2010); doi:10.1016/j.jchromb.2010.02.006.
- H. Dejmkova, C. Dag, J. Barek and J. Zima, Cent. Eur. J. Chem., 10, 1310 (2012); doi:10.2478/s11532-012-0056-8.
- M.A. Sultan, H.M. Maher, N.Z. Alzoman, M.M. Alshehri, M.S. Rizk, M.S. Elshahed and I.V. Olah, J. Chromatogr. Sci., 51, 502 (2013); doi:10.1093/chromsci/bms175.
- K.W. Zhou, X.M. Gu, X.C. Cui and X.C. Chen, Acta Chim. Sin., 69, 221 (2011).
- I. Soykan, B. Sivri, I. Sarosiek, B. Kiernan and R.W. McCallum, Dig. Dis. Sci., 43, 2398 (1998); doi:10.1023/A:1026665728213.
- A.G. Stosik, H.E. Junginger, S. Kopp, K.K. Midha, V.P. Shah, S. Stavchansky, J.B. Dressman and D.M. Barends, Pharm. Sci., 97, 3700 (2008); doi:10.1002/jps.21276.
- I. Ganescu, Studia Univ. Babes-Bolyai Chem., 13, 25 (1967).
- J. Roesler, Liebigs Ann. Chem., 141, 189 (1967).
- I. Ganescu, C. Várhelyi and G. Brînzan, Archiv. Pharm., 318, 30 (1985); doi:10.1002/ardp.19853180108.
- I. Ganescu, I. Papa, A. Ganescu, G. Bratulescu and D. Cirtina, Acta Chim. Slov., 49, 181 (2002).
- I. Ganescu, A. Popescu, L. Chirigiu and I. Papa, Anal. Univ. Bucuresti, 7, 33 (1988).
- C. Varhely, I. Zsakó and I. Ganescu, Magy. Kem. Foly., 106, 1 (2000).
- I. Ganescu, V. Aldea, A. Ganescu, I. Papa and A. Barbu, Farmacia, 1, 47 (2003).
- G.S. Desmukh and M. Joshi, Z. Anal. Chem., 142, 275 (1954).
- L.M. Batuner and M.E. Pozin, Mathematical Methods in Chemical Technique, Tehnica Publishing House, Bucharest, Romania, p. 486 (1956) (in Romanian).
References
V. Zotta, Pharmaceutical Chemistry, Medicala Publishing House, Bucharest, p. 688 (1985) (in Romanian).
M.S. Attia and M.M. Aboaly, Talanta, 82, 78 (2010); doi:10.1016/j.talanta.2010.03.062.
J. Shah, M.R. Jan, M.A. Khan and S. Amin, J. Anal. Chem., 60, 633 (2005); doi:10.1007/s10809-005-0151-5.
I. de Souza Silva, M.L.M.F.S. Saraiva, J.L.M. Santos and J.L.F.C. Lima, Spectrosc. Lett., 40, 51 (2007); doi:10.1080/00387010601093778.
S.J. Wadher, P.R. Pathankar, M. Puranik, R.O. Ganjiwale and P.G. Yeole, Indian J. Pharm. Sci., 70, 393 (2008); doi:10.4103/0250-474X.43014.
F.F. Belal, M.K. Sharaf El-Din, M.M. Tolba and H. Elmansi, J. Chromatogr. Sci., 52, 1224 (2014); doi:10.1093/chromsci/bmt202.
S.T. Ulu, Chin. J. Chem., 30, 634 (2012); doi:10.1002/cjoc.201280001.
M. Yan, H.D. Li, B.M. Chen, X.L. Liu and Y.G. Zhu, J. Chromatogr. B Analyt. Technol. Biomed. Life Sci., 878, 883 (2010); doi:10.1016/j.jchromb.2010.02.006.
H. Dejmkova, C. Dag, J. Barek and J. Zima, Cent. Eur. J. Chem., 10, 1310 (2012); doi:10.2478/s11532-012-0056-8.
M.A. Sultan, H.M. Maher, N.Z. Alzoman, M.M. Alshehri, M.S. Rizk, M.S. Elshahed and I.V. Olah, J. Chromatogr. Sci., 51, 502 (2013); doi:10.1093/chromsci/bms175.
K.W. Zhou, X.M. Gu, X.C. Cui and X.C. Chen, Acta Chim. Sin., 69, 221 (2011).
I. Soykan, B. Sivri, I. Sarosiek, B. Kiernan and R.W. McCallum, Dig. Dis. Sci., 43, 2398 (1998); doi:10.1023/A:1026665728213.
A.G. Stosik, H.E. Junginger, S. Kopp, K.K. Midha, V.P. Shah, S. Stavchansky, J.B. Dressman and D.M. Barends, Pharm. Sci., 97, 3700 (2008); doi:10.1002/jps.21276.
I. Ganescu, Studia Univ. Babes-Bolyai Chem., 13, 25 (1967).
J. Roesler, Liebigs Ann. Chem., 141, 189 (1967).
I. Ganescu, C. Várhelyi and G. Brînzan, Archiv. Pharm., 318, 30 (1985); doi:10.1002/ardp.19853180108.
I. Ganescu, I. Papa, A. Ganescu, G. Bratulescu and D. Cirtina, Acta Chim. Slov., 49, 181 (2002).
I. Ganescu, A. Popescu, L. Chirigiu and I. Papa, Anal. Univ. Bucuresti, 7, 33 (1988).
C. Varhely, I. Zsakó and I. Ganescu, Magy. Kem. Foly., 106, 1 (2000).
I. Ganescu, V. Aldea, A. Ganescu, I. Papa and A. Barbu, Farmacia, 1, 47 (2003).
G.S. Desmukh and M. Joshi, Z. Anal. Chem., 142, 275 (1954).
L.M. Batuner and M.E. Pozin, Mathematical Methods in Chemical Technique, Tehnica Publishing House, Bucharest, Romania, p. 486 (1956) (in Romanian).