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Vol. 28 No. 10 (2016): Vol 28 Issue 10

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Microwave Assisted Preparation and Physico-Chemical Properties of Mixed Oxides Silica-Zirconia Montmorillonite K10 Nanocomposite

https://doi.org/10.14233/ajchem.2016.19982
Serly Jol
1Department of Chemistry, Faculty of Mathematics and Natural Sciences, Pattimura University, Ambon, Indonesia 2Department of Chemistry, Faculty of Mathematics and Natural Sciences, Gadjah Mada University, Yogyakarta, Indonesia 3Department of Chemical Engineering, Faculty of Engineering, Gadjah Mada University, Yogyakarta, Indonesia *Corresponding author: Tel: +62 85243640076; E-mail: sjsekewael@yahoo.com
a Sekewael1
1Department of Chemistry, Faculty of Mathematics and Natural Sciences, Pattimura University, Ambon, Indonesia 2Department of Chemistry, Faculty of Mathematics and Natural Sciences, Gadjah Mada University, Yogyakarta, Indonesia 3Department of Chemical Engineering, Faculty of Engineering, Gadjah Mada University, Yogyakarta, Indonesia *Corresponding author: Tel: +62 85243640076; E-mail: sjsekewael@yahoo.com
Karna Wijaya2
1Department of Chemistry, Faculty of Mathematics and Natural Sciences, Pattimura University, Ambon, Indonesia 2Department of Chemistry, Faculty of Mathematics and Natural Sciences, Gadjah Mada University, Yogyakarta, Indonesia 3Department of Chemical Engineering, Faculty of Engineering, Gadjah Mada University, Yogyakarta, Indonesia *Corresponding author: Tel: +62 85243640076; E-mail: sjsekewael@yahoo.com
Arief Budiman3
1Department of Chemistry, Faculty of Mathematics and Natural Sciences, Pattimura University, Ambon, Indonesia 2Department of Chemistry, Faculty of Mathematics and Natural Sciences, Gadjah Mada University, Yogyakarta, Indonesia 3Department of Chemical Engineering, Faculty of Engineering, Gadjah Mada University, Yogyakarta, Indonesia *Corresponding author: Tel: +62 85243640076; E-mail: sjsekewael@yahoo.com

Asian Journal of Chemistry, Vol. 28 No. 10 (2016): Vol 28 Issue 10

Abstract

A new solid material, silica-zirconia mixed oxides montmorillonite K10 nanocomposite was prepared through calcination process at various microwave radiation energy output and conventional method along with their characterization.The results show that microwave irradiation at 700 W enhanced the physico-chemical properties of montmorillonite K10. The increase of total surface acidity, specific surface area as well as the total pore volume, respectively. The slightly increased of basal spacing (d001) caused the layers structure of mixed oxide silica-zirconia montmorillonite becoming more regular than untreated montmorillonite as investigated by TEM analyses.

Keywords

Montmorillonite K10 Mixed oxide silica-zirconia Microwave radiation.
Jol, S., Sekewael1, a, Wijaya2, K., & Budiman3, A. (2016). Microwave Assisted Preparation and Physico-Chemical Properties of Mixed Oxides Silica-Zirconia Montmorillonite K10 Nanocomposite. Asian Journal of Chemistry, 28(10), 2325–2330. https://doi.org/10.14233/ajchem.2016.19982
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