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Vol. 27 No. 9 (2015): Vol 27 Issue 9

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Determination of 5 Photoinitiators, 6 Plasticizers and 9 Primary Aromatic Amines in Plastic and Canned Food Contact Materials by Gas Chromatography-Mass Spectrometry

https://doi.org/10.14233/ajchem.2015.18360
Qin-Bao Lin
Key Laboratory of Product Packaging and Logistics, Packaging Engineering Institute, Jinan University, Zhuhai 519070, P.R. China; College of Life Science, Shanxi University, Taiyuan 030006, P.R. China
He Li
College of Life Science, Shanxi University, Taiyuan 030006, P.R. China
Ya-Kun Chen
College of Life Science, Shanxi University, Taiyuan 030006, P.R. China
Yu-Mei Wu
Key Laboratory of Product Packaging and Logistics, Packaging Engineering Institute, Jinan University, Zhuhai 519070, P.R. China
Shao-Jing Wu
Shenzhen Entry-Exit Inspection and Quarantine Bureau, Shenzhen 518010, P.R. China
Zhi-Nan Chen
Shenzhen Entry-Exit Inspection and Quarantine Bureau, Shenzhen 518010, P.R. China
Zhi-Wei Wang
Key Laboratory of Product Packaging and Logistics, Packaging Engineering Institute, Jinan University, Zhuhai 519070, P.R. China

Corresponding Author(s) : Qin-Bao Lin

tlinqb@jnu.edu.cn

Asian Journal of Chemistry, Vol. 27 No. 9 (2015): Vol 27 Issue 9

Abstract

A practical and simple method was developed for determination of five photoinitiators, six adipate-based plasticizers and nine primary aromatic amines in three ink-printed plastic composite bags, one polyvinyl chloride film and two metal cans using ultrasonic extraction coupled with gas chromatography-mass spectrometry. The correlation coefficient (R2) of standard curve was ³ 0.9973 and limits of detection of the method ranged from 0.80 to 10 μg kg-1. The recoveries and precision was satisfactory. The results indicated that the di(2-ethylhexyl) adipate was prevalent exist in studied food contact materials and the content ranged from 0.19 to 1.01 × 105 mg kg-1. Benzophenone concentration ranged 0.020 to 0.065 mg kg-1. Aniline concentration ranged 0.020 to 0.27 mg kg-1.

Keywords

Food contact materials Photoinitiators Adipate-based plasticizers Primary aromatic amines
Lin, Q.-B., Li, H., Chen, Y.-K., Wu, Y.-M., Wu, S.-J., Chen, Z.-N., & Wang, Z.-W. (2015). Determination of 5 Photoinitiators, 6 Plasticizers and 9 Primary Aromatic Amines in Plastic and Canned Food Contact Materials by Gas Chromatography-Mass Spectrometry. Asian Journal of Chemistry, 27(9), 3173–3179. https://doi.org/10.14233/ajchem.2015.18360
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