Microwave Solid Phase Synthesis, Characterization and Antimicrobial Activities of 2,2'-[(1E,1'E)- {ethane-1,2-diylbis(azanylylidene)}bis(methanylylidene)]bis(4-chlorophenol)manganese(II)

Suo-Ping Xu; Dan-Dan Wei

doi:10.14233/ajchem.2015.18876

Issue

Vol. 27 No. 9 (2015): Vol 27 Issue 9

Issue Published : May 26, 2015

This work is licensed under a Creative Commons Attribution 4.0 International License.

Microwave Solid Phase Synthesis, Characterization and Antimicrobial Activities of 2,2'-[(1E,1'E)- {ethane-1,2-diylbis(azanylylidene)}bis(methanylylidene)]bis(4-chlorophenol)manganese(II)

https://doi.org/10.14233/ajchem.2015.18876

Suo-Ping Xu

Jiangsu Key Laboratory of Green Synthetic Chemistry for Functional Materials, Jiangsu Normal University, Xuzhou 221116, P.R. China

Dan-Dan Wei

Jiangsu Key Laboratory of Green Synthetic Chemistry for Functional Materials, Jiangsu Normal University, Xuzhou 221116, P.R. China

Corresponding Author(s) : Suo-Ping Xu

xsp62@jsnu.edu.cn

Asian Journal of Chemistry, Vol. 27 No. 9 (2015): Vol 27 Issue 9
Article Published : May 26, 2015

Abstract

One mononuclear complex (1) has been designed and synthesized by 2,2'-[(1E,1'E)-{ethane-1,2- diylbis(azanylylidene)}bis(methanylylidene)]bis(4-chlorophenol) (L) with MnCl₂·4H₂O in microwave radiation assistance. The complex was characterized by X-ray crystallo-graphy, confirming that the central mangances(II) was coordinated by two oxygen atoms, two nitrogen atoms from L and two oxygen atoms from H₂O. The complex was assayed for in vitro antibacterial (B. subtilis, S. aureus, S. faecalis, P. aeruginosa, E. coli and E. cloacae) activities and showed better antimicrobial activity against Gram positive strains than Gram negative strains.

Keywords

Salicylaldehyde type's schiff base Mononuclear mangancse(II) complex Antibacterial activity

Xu, S.-P., & Wei, D.-D. (2015). Microwave Solid Phase Synthesis, Characterization and Antimicrobial Activities of 2,2’-[(1E,1’E)- {ethane-1,2-diylbis(azanylylidene)}bis(methanylylidene)]bis(4-chlorophenol)manganese(II). Asian Journal of Chemistry, 27(9), 3404–3406. https://doi.org/10.14233/ajchem.2015.18876

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References

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M. Nath, S. Pokharia, X. Song, G. Eng, M. Gielen, M. Kemmer, M. Biesemans, R. Willem and D. De Vos, Appl. Organomet. Chem., 17, 305 (2003); doi:10.1002/aoc.451.

References

S.-P. Xu, L. Shi, P.-C. Lv, R.-Q. Fang and H.-L. Zhu, J. Coord. Chem., 62, 2048 (2009); doi:10.1080/00958970902741251.

L. Shi, H.-M. Ge, S.-H. Tan, H.-Q. Li, Y.-C. Song, H.-L. Zhu and R.-X. Tan, Eur. J. Med. Chem., 42, 558 (2007); doi:10.1016/j.ejmech.2006.11.010.

A. Roth, E.T. Spielberg and W. Plass, Inorg. Chem., 46, 4362 (2007); doi:10.1021/ic070088i.

J.D. Ranford, J.J. Vittal and Y.M. Wang, Inorg. Chem., 37, 1226 (1998); doi:10.1021/ic970805g.

S.-P. Xu, Y. Pei, G. Xu, W.-X. Su and J.-X. Shu, J. Xuzhou Norm. Univ. Nat. Sci. Ed., 28, 57 (2010).

L.-M. Wu, H.-B. Teng, X.-C. Feng, X.-B. Ke, Q.-F. Zhu, J.-T. Su, W.-J. Xu and X.-M. Hu, Cryst. Growth Des., 7, 1337 (2007); doi:10.1021/cg070196f.

S.-P. Xu, P.-C. Lv, L. Shi and H.-L. Zhu, Arch. Pharm. Chem. Life Sci., 343, 282 (2010).

S.-P. Xu, Y. Pei, G. Xu, W.-X. Su and J.-X. Shu, J. Xuahou Norm. Univ. Nat. Sci. Ed., 28, 57 (2010).

P. Prusis, M. Dambrova, V. Andrianov, E. Rozhkov, V. Semenikhina, I. Piskunova, E. Ongwae, T. Lundstedt, I. Kalvinsh and J.E.S. Wikberg, J. Med. Chem., 47, 3105 (2004); doi:10.1021/jm031127c.

S. Ren, R. Wang, K. Komatsu, P. Bonaz-Krause, Y. Zyrianov, C.E. McKenna, C. Csipke, Z.A. Tokes and E.J. Lien, J. Med. Chem., 45, 410 (2002); doi:10.1021/jm010252q.

P.H. Wang, J.G. Keck, E.J. Lien and M.M.C. Lai, J. Med. Chem., 33, 608 (1990); doi:10.1021/jm00164a023.

S.-P. Xu, B.-F. Ruan, Q.-Y. Pan and R.-T. Hu, J. Coord. Chem., 64, 2489 (2011); doi:10.1080/00958972.2011.601459.

G.M. Sheldrick, SHELXL V5.1 Software Reference Manual, Bruker AXS, Inc., Madison, WI, USA (1997).

J. Meletiadis, J.F. Meis, J.W. Mouton, J.P. Donnelly and P.E. Verweij, J. Clin. Microbiol., 38, 2949 (2000).

K. Nakamato, Infrared Spectra of Inorganic and Coordination Compounds, Wiley, New York (1994).

J.-M. Li, J.-Z. Li, H.-Q. Zhang and L.-Y. Xu, Inorg. Chem. Commun., 13, 573 (2010); doi:10.1016/j.inoche.2010.01.023.

S.-P. Xu, L. Shi, P.-C. Lv, R.-Q. Fang and H.-L. Zhu, J. Coord. Chem., 62, 2048 (2009); doi:10.1080/00958970902741251.

M. Nath, S. Pokharia, X. Song, G. Eng, M. Gielen, M. Kemmer, M. Biesemans, R. Willem and D. De Vos, Appl. Organomet. Chem., 17, 305 (2003); doi:10.1002/aoc.451.

Issue

Vol. 27 No. 9 (2015): Vol 27 Issue 9

Microwave Solid Phase Synthesis, Characterization and Antimicrobial Activities of 2,2'-[(1E,1'E)- {ethane-1,2-diylbis(azanylylidene)}bis(methanylylidene)]bis(4-chlorophenol)manganese(II)

Corresponding Author(s) : Suo-Ping Xu

Abstract

Keywords

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