Copyright (c) 2015 AJC
This work is licensed under a Creative Commons Attribution 4.0 International License.
Study on the Preparation and Properties of Inorganic Silica Single-Layer Film
Corresponding Author(s) : Haihong Li
Asian Journal of Chemistry,
Vol. 27 No. 8 (2015): Vol 27 Issue 8
Abstract
The silica single-layer film catalyzed by hydrochloric acid was prepared on the glass matrix with tetraethyl orthosilicate and absolute alcohol as main raw materials by sol-gel method. The reaction mechanism of sol-gel method included hydrolysis reactions and polymerization reactions. The samples were characterized by visible spectrophotometer, X-ray diffraction and thermal analysis (TG and DTA). Results showed that the light transmittance of the silica single-layer film was enhanced remarkably. X-ray diffraction results indicated that the single-layer film possessed amorphous characteristic. Adhesion tests showed that the adhesion force between the silica single-layer film and the glass matrix was very strong. Thermal analytical results demonstrated that silica would absorb heat when it transformed from amorphous structure to crystal structure.
Keywords
Download Citation
Endnote/Zotero/Mendeley (RIS)BibTeX
- H. Zhang, J.-H. Zhou, Q.-L. Zhang and H. Yang, J. Inorg. Mater., 28, 785 (2013); doi:10.3724/SP.J.1077.2013.13014.
- H. Zhang, D. Fan, T. Yu and C. Wang, J. Sol-Gel Sci. Technol., 66, 274 (2013); doi:10.1007/s10971-013-3004-y.
- J. Ma, J. Hu, Z. Yang and L. Liu, J. Sol-Gel Sci. Technol., 41, 209 (2007); doi:10.1007/s10971-006-1506-6.
- A. Nakajima, K. Abe, K. Hashimoto and T. Watanabe, Thin Solid Films, 376, 140 (2000); doi:10.1016/S0040-6090(00)01417-6.
- A. Martucci, N. Bassiri, M. Guglielmi, L. Armelao, S. Gross and J.C. Pivin, J. Sol-Gel Sci. Technol., 26, 993 (2003); doi:10.1023/A:1020717614995.
- D. Jiao, S.H. Zheng, H.Y. Xu and B.Q. Cao, Asian J. Chem., 23, 3912 (2011).
- C.F. Xin, C. Peng, Y.D. Xu and J.Q. Wu, Solar Energy, 93, 121(2013); doi:10.1016/j.solener.2013.04.006.
- R. Prado, G. Beobide, A. Marcaide, J. Goikoetxea and A. Aranzabe, Sol. Energy Mater. Sol. Cells, 94, 1081 (2010); doi:10.1016/j.solmat.2010.02.031.
- W.J. Zhang, X.B. Pei, J.W. Bai and H.B. He, J. Mater. Eng. Perform., 23, 1049 (2014); doi:10.1007/s11665-013-0833-3.
- H.-S. Chen, S.-H. Huang and T.-P. Perng, Surf. Coat. Technol., 233, 140 (2013); doi:10.1016/j.surfcoat.2013.04.023.
References
H. Zhang, J.-H. Zhou, Q.-L. Zhang and H. Yang, J. Inorg. Mater., 28, 785 (2013); doi:10.3724/SP.J.1077.2013.13014.
H. Zhang, D. Fan, T. Yu and C. Wang, J. Sol-Gel Sci. Technol., 66, 274 (2013); doi:10.1007/s10971-013-3004-y.
J. Ma, J. Hu, Z. Yang and L. Liu, J. Sol-Gel Sci. Technol., 41, 209 (2007); doi:10.1007/s10971-006-1506-6.
A. Nakajima, K. Abe, K. Hashimoto and T. Watanabe, Thin Solid Films, 376, 140 (2000); doi:10.1016/S0040-6090(00)01417-6.
A. Martucci, N. Bassiri, M. Guglielmi, L. Armelao, S. Gross and J.C. Pivin, J. Sol-Gel Sci. Technol., 26, 993 (2003); doi:10.1023/A:1020717614995.
D. Jiao, S.H. Zheng, H.Y. Xu and B.Q. Cao, Asian J. Chem., 23, 3912 (2011).
C.F. Xin, C. Peng, Y.D. Xu and J.Q. Wu, Solar Energy, 93, 121(2013); doi:10.1016/j.solener.2013.04.006.
R. Prado, G. Beobide, A. Marcaide, J. Goikoetxea and A. Aranzabe, Sol. Energy Mater. Sol. Cells, 94, 1081 (2010); doi:10.1016/j.solmat.2010.02.031.
W.J. Zhang, X.B. Pei, J.W. Bai and H.B. He, J. Mater. Eng. Perform., 23, 1049 (2014); doi:10.1007/s11665-013-0833-3.
H.-S. Chen, S.-H. Huang and T.-P. Perng, Surf. Coat. Technol., 233, 140 (2013); doi:10.1016/j.surfcoat.2013.04.023.