Copyright (c) 2015 AJC
This work is licensed under a Creative Commons Attribution 4.0 International License.
Preparation of C60 Nanowhiskers-ZnS Nanocomposites and Photocatalytic Degradation of Methylene Blue
Corresponding Author(s) : Weon Bae Ko
Asian Journal of Chemistry,
Vol. 27 No. 6 (2015): Vol 27 Issue 6
Abstract
Liquid-liquid interfacial precipitation (LLIP) method was used to prepare C60 nanowhiskers. Zinc sulfide nanoparticles were synthesized by zinc nitrate hexahydrate and thiourea under microwave irradiation. C60 nanowhiskers-ZnS nanocomposites were prepared by a reaction of C60 nanowhiskers and ZnS nanoparticles in an electric furnace. The C60 nanowhiskers-ZnS nanocomposites were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and UV-visible spectrophotometry. The C60 nanowhiskers-ZnS nanocomposites were evaluated as a photocatalyst in the photocatalytic degradation of methylene by UV-visible spectrophotometry under ultraviolet light at 254 nm.
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References
H.W. Kroto, J.R. Heath, S.C. O’Brien, R.F. Curl and R.E. Smalley, Nature, 318, 162 (1985); doi:10.1038/318162a0.
W. Kratshmer, L.D. Lamb, K. Fostiropoulos and D.R. Huffman, Nature, 347, 354 (1990); doi:10.1038/347354a0.
E.Y. Zhang and C.R. Wang, Curr. Opin.Colloid Interface Sci., 14, 148 (2009); doi:10.1016/j.cocis.2007.10.002.
K. Asaka, T. Nakayama, K. Miyazawa and Y. Saito, Carbon, 50, 1209 (2012); doi:10.1016/j.carbon.2011.10.035.
K. Miyazawa, A. Obayashi and M. Kuwabara, J. Am. Ceram. Soc., 84, 3037 (2001); doi:10.1111/j.1151-2916.2001.tb01133.x.
K. Miyazawa, Y. Kuwasaki, A. Obayashi and M. Kuwabara, J. Mater. Res., 17, 83 (2002); doi:10.1557/JMR.2002.0014.
K. Miyazawa, Y. Kuwasaki, K. Hamamoto, S. Nagata, A. Obayashi and M. Kuwabara, Surf. Interface Anal., 35, 117 (2003); doi:10.1002/sia.1506.
K. Miyazawa, K. Hamamoto, S. Nagata and T. Suga, J. Mater. Res., 18, 1096 (2003); doi:10.1557/JMR.2003.0151.
J. Miyamoto, H. Kanoh and K. Kaneko, Carbon, 43, 855 (2005); doi:10.1016/j.carbon.2004.10.049.
K. Miyazawa and K. Hotta, J. Cryst. Growth, 312, 2764 (2010); doi:10.1016/j.jcrysgro.2010.06.020.
C.S. Pathak, D.D. Mishra, V. Agarwala and M.K. Mandal, Ceram. Int., 38, 5497 (2012); doi:10.1016/j.ceramint.2012.03.063.
N. Karar, F. Singh and B.R. Mehta, J. Appl. Phys., 95, 656 (2004); doi:10.1063/1.1633347.
S. Yanagida, H. Kawakami, Y. Midori, H. Kizumoto, C. Pac and Y. Wada, Bull. Chem. Soc. Jpn., 68, 1811 (1995); doi:10.1246/bcsj.68.1811.
S.R. Chalana, R. Vinodkumar, I. Navas, V. Ganesan and V.P. Mahadevan Pillai, J. Lumin., 132, 944 (2012); doi:10.1016/j.jlumin.2011.10.017.
E.K. Goharshadi, S. Sajjadi, R. Mehrkhah and P. Nancarrow, Chem. Eng. J., 209, 113 (2012); doi:10.1016/j.cej.2012.07.131.
V. Stanić, T.H. Etsell, A.C. Pierre and R.J. Mikula, Mater. Lett., 31, 35 (1997); doi:10.1016/S0167-577X(96)00237-6.
Q. Zhao, L. Hou and R. Huang, Inorg. Chem. Commun., 6, 971 (2003); doi:10.1016/S1387-7003(03)00146-1.
D. Zhang, L. Qi, H. Cheng and J. Ma, J. Colloid Interf. Sci., 246, 413 (2002); doi:10.1006/jcis.2001.8081.
A.K. Verma, T.B. Rauchfuss and S.R. Wilson, Inorg. Chem., 34, 3072 (1995); doi:10.1021/ic00115a038.
F. Huang and J.F. Banfield, J. Am. Chem. Soc., 127, 4523 (2005); doi:10.1021/ja048121c.
W.T. Yao, S.H. Yu, L. Pan, J. Li, Q.S. Wu, L. Zhang and J. Jiang, Small, 1, 320 (2005); doi:10.1002/smll.200400079.
D. Synnott, M. Seery, S. Hinder, J. Colreavy and S. Pillai, Nanotechnology, 24, 045704 (2013); doi:10.1088/0957-4484/24/4/045704.
A.M. Peiró, J.A. Ayllón, J. Peral, X. Domènech and C. Domingo, J. Cryst. Growth, 285, 6 (2005); doi:10.1016/j.jcrysgro.2005.07.028.
S.C. Padmanabhan, D. Ledwith, S.C. Pillai, D.E. McCormack and J.M. Kelly, J. Mater. Chem., 19, 9250 (2009); doi:10.1039/b912537j.
S. Liang, L. Zhu, G. Gai, Y. Yao, J. Huang, X. Ji, X. Zhou, D. Zhang and P. Zhang, Ultrason. Sonochem., 21, 1335 (2014); doi:10.1016/j.ultsonch.2014.02.007.
U.G. Akpan and B.H. Hameed, J. Hazard. Mater., 170, 520 (2009); doi:10.1016/j.jhazmat.2009.05.039.
I. Fatimah, S. Wang and D. Wulandari, Appl. Clay Sci., 53, 553 (2011); doi:10.1016/j.clay.2011.05.001.
C. Liu, Y. Yang, Q. Wang, M. Kim, Q. Zhu, D. Li and Z. Zhang, Bioresour. Technol., 125, 30 (2012); doi:10.1016/j.biortech.2012.08.139.
N. Miranda-García, S. Suárez, B. Sánchez, J.M. Coronado, S. Malato and M.I. Maldonado, Appl. Catal. B, 103, 294 (2011); doi:10.1016/j.apcatb.2011.01.030.
S.K. Hong, J.H. Lee and W.B. Ko, J. Nanosci. Nanotechnol., 11, 6049 (2011); doi:10.1166/jnn.2011.4374.
K. Ullah, S. Ye, S. Sarkar, L. Zhu, Z.D. Meng and W.C. Oh, Asian J. Chem., 26, 145 (2014); doi:10.14233/ajchem.2014.15351.
W.B. Ko, Elast. Compos., 49, 155 (2014).