Microwave Solid Phase Synthesis, Characterization and Antimicrobial Activities of Manganese(II) Complex with 2-((Furan-3-ylmethylimino)methyl)phenol

Suo-Ping Xu; Ting-Ting Cao; Si-Jia Wang; Wei-Qing Miao; Shu-Jie Wu; Ya-Nan Zhu

doi:10.14233/ajchem.2015.17584

Issue

Vol. 27 No. 5 (2015): Vol 27 Issue 5

Issue Published : February 20, 2015

This work is licensed under a Creative Commons Attribution 4.0 International License.

Microwave Solid Phase Synthesis, Characterization and Antimicrobial Activities of Manganese(II) Complex with 2-((Furan-3-ylmethylimino)methyl)phenol

https://doi.org/10.14233/ajchem.2015.17584

Suo-Ping Xu

Jiangsu Key Laboratory of Green Synthetic Chemistry for Functional Materials, Jiangsu Normal University, Xuzhou 221116, P.R. China

Ting-Ting Cao

Jiangsu Key Laboratory of Green Synthetic Chemistry for Functional Materials, Jiangsu Normal University, Xuzhou 221116, P.R. China

Si-Jia Wang

Jiangsu Key Laboratory of Green Synthetic Chemistry for Functional Materials, Jiangsu Normal University, Xuzhou 221116, P.R. China

Wei-Qing Miao

Jiangsu Key Laboratory of Green Synthetic Chemistry for Functional Materials, Jiangsu Normal University, Xuzhou 221116, P.R. China

Shu-Jie Wu

Jiangsu Key Laboratory of Green Synthetic Chemistry for Functional Materials, Jiangsu Normal University, Xuzhou 221116, P.R. China

Ya-Nan Zhu

Jiangsu Key Laboratory of Green Synthetic Chemistry for Functional Materials, Jiangsu Normal University, Xuzhou 221116, P.R. China

Corresponding Author(s) : Suo-Ping Xu

xsp62@jsnu.edu.cn

Asian Journal of Chemistry, Vol. 27 No. 5 (2015): Vol 27 Issue 5
Article Published : February 20, 2015

Abstract

Mononuclear complex of manganese (1) has been designed and synthesized by 2-((furan-3-ylmethylimino)methyl)phenol (L) with MnCl₂·4H₂O in microwave radiation. The complex was characterized by X-ray crystallography, confirming that the central mangances(II) was coordinated by two oxygen atoms and two nitrogen atoms from two L. The complex was assayed for in vitro antibacterial (B. subtilis, S. aureus, S. faecalis, P. aeruginosa, E. coli and E. cloacae ) activities and showed better antimicrobial activity against Gram positive strains than Gram negative strains.

Keywords

Microwave solid phase synthesis 2-((Furan-3-ylmethylimino)methyl)phenol ligand Mononuclear mangancse(II) complex

Xu, S.-P., Cao, T.-T., Wang, S.-J., Miao, W.-Q., Wu, S.-J., & Zhu, Y.-N. (2015). Microwave Solid Phase Synthesis, Characterization and Antimicrobial Activities of Manganese(II) Complex with 2-((Furan-3-ylmethylimino)methyl)phenol. Asian Journal of Chemistry, 27(5), 1735–1738. https://doi.org/10.14233/ajchem.2015.17584

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References

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References

S.-P. Xu, L. Shi, P.-C. Lv, R.-Q. Fang and H.-L. Zhu, J. Coord. Chem., 62, 2048 (2009); doi:10.1080/00958970902741251.

L. Shi, H.-M. Ge, S.-H. Tan, H.-Q. Li, Y.-C. Song, H.-L. Zhu and R.-X. Tan, Eur. J. Med. Chem., 42, 558 (2007); doi:10.1016/j.ejmech.2006.11.010.

A. Roth, E.T. Spielberg and W. Plass, Inorg. Chem., 46, 4362 (2007); doi:10.1021/ic070088i.

J.D. Ranford, J.J. Vittal and Y.M. Wang, Inorg. Chem., 37, 1226 (1998); doi:10.1021/ic970805g.

S. Toroglu, E. Ispir and C. Çelik, Asian J. Chem., 19, 5497 (2009).

L.-M. Wu, H.-B. Teng, X.-C. Feng, X.-B. Ke, Q.-F. Zhu, J.-T. Su, W.-J. Xu and X.-M. Hu, Cryst. Growth Des., 7, 1337 (2007); doi:10.1021/cg070196f.

S.-P. Xu, P.-C. Lv, L. Shi and H.-L. Zhu, Arch. Pharm. Chem. Life Sci., 343, 282 (2010).

S.-P. Xu, Y. Pei, G. Xu, W.-X. Su and J.-X. Shu, J. Xuahou Norm. Univ.: Nat. Sci. Ed., 28, 57 (2010).

P. Prusis, M. Dambrova, V. Andrianov, E. Rozhkov, V. Semenikhina, I. Piskunova, E. Ongwae, T. Lundstedt, I. Kalvinsh and J.E.S. Wikberg, J. Med. Chem., 47, 3105 (2004); doi:10.1021/jm031127c.

S. Ren, R. Wang, K. Komatsu, P. Bonaz-Krause, Y. Zyrianov, C.E. McKenna, C. Csipke, Z.A. Tokes and E.J. Lien, J. Med. Chem., 45, 410 (2002); doi:10.1021/jm010252q.

P.H. Wang, J.G. Keck, E.J. Lien and M.M.C. Lai, J. Med. Chem., 33, 608 (1990); doi:10.1021/jm00164a023.

S.-P. Xu, B.-F. Ruan, Q.-Y. Pan and R.-T. Hu, J. Coord. Chem., 64, 2489 (2011); doi:10.1080/00958972.2011.601459.

G.M. Sheldrick, SHELXL V5.1 Software Reference Manual, Bruker AXS, Inc., Madison, WI, USA (1997).

J. Meletiadis, J.F. Meis, J.W. Mouton, J.P. Donnelly and P.E. Verweij, J. Clin. Microbiol., 38, 2949 (2000).

K. Nakamato, Infrared Spectra of Inorganic and Coordination Compounds, Wiley, New York (1994).

J.-M. Li, J.-Z. Li, H.-Q. Zhang and L.-Y. Xu, Inorg. Chem. Commun., 13, 573 (2010); doi:10.1016/j.inoche.2010.01.023.

S.-P. Xu, L. Shi, P.-C. Lv, R.-Q. Fang and H.-L. Zhu, J. Coord. Chem., 62, 2048 (2009); doi:10.1080/00958970902741251.

R.V. Singh, P. Chaudhary, S. Chauhan and M. Swami, Spectrochim. Acta A, 72, 260 (2009); doi:10.1016/j.saa.2008.09.017.

M. Nath, S. Pokharia, X. Song, G. Eng, M. Gielen, M. Kemmer, M. Biesemans, R. Willem and D. De Vos, Appl. Organomet. Chem., 17, 305 (2003); doi:10.1002/aoc.451.

Issue

Vol. 27 No. 5 (2015): Vol 27 Issue 5

Microwave Solid Phase Synthesis, Characterization and Antimicrobial Activities of Manganese(II) Complex with 2-((Furan-3-ylmethylimino)methyl)phenol

Corresponding Author(s) : Suo-Ping Xu

Abstract

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