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Solvent Evaporation Method and Crystal Structure of 1,3-Dimethyl-3-(2,2,2-trifluoro-ethyl)-1H,3H-1-aza-phenalen-2-one
Corresponding Author(s) : Y. Zhao
Asian Journal of Chemistry,
Vol. 27 No. 2 (2015): Vol 27 Issue 2
Abstract
One new compound [N-arylacrylamides (0.30 mmol), PhI(OAc) (0.6 mmol), NaOAc (0.6 mmol) in NMP (1 mL) was added TMSCF3 (1.8 mmol)] has been successfully synthesized. Compound shows a one-dimensional framework. The 1D supramolecular structure is formed via hydrogen bonding connection.
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- Chemistry, Wiley-VCH, Weinheim, Germany (2004).
- A. Studer, Angew. Chem. Int. Ed., 51, 8950 (2012); doi:10.1002/anie.201202624.
- A. Zanardi, M.A. Novikov, E. Martin, J. Benet-Buchholz and V.V. Grushin, J. Am. Chem. Soc., 133, 20901 (2011); doi:10.1021/ja2081026.
- T.D. Senecal, A.T. Parsons and S.L. Buchwald, J. Org. Chem., 76, 1174 (2011); doi:10.1021/jo1023377.
- X. Wang, L. Truesdale and J.-Q. Yu, J. Am. Chem. Soc., 132, 3648 (2010); doi:10.1021/ja909522s.
- Z. Weng, H. Li, W. He, L.-F. Yao, J. Tan, J. Chen, Y. Yuan and K.-W. Huang, Tetrahedron, 68, 2527 (2012); doi:10.1016/j.tet.2011.12.085.
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- G.M. Sheldrick, SHELXTL97, Program for the Refinement of Crystal Structure, University of Gottingen, Germany (1997).
References
Chemistry, Wiley-VCH, Weinheim, Germany (2004).
A. Studer, Angew. Chem. Int. Ed., 51, 8950 (2012); doi:10.1002/anie.201202624.
A. Zanardi, M.A. Novikov, E. Martin, J. Benet-Buchholz and V.V. Grushin, J. Am. Chem. Soc., 133, 20901 (2011); doi:10.1021/ja2081026.
T.D. Senecal, A.T. Parsons and S.L. Buchwald, J. Org. Chem., 76, 1174 (2011); doi:10.1021/jo1023377.
X. Wang, L. Truesdale and J.-Q. Yu, J. Am. Chem. Soc., 132, 3648 (2010); doi:10.1021/ja909522s.
Z. Weng, H. Li, W. He, L.-F. Yao, J. Tan, J. Chen, Y. Yuan and K.-W. Huang, Tetrahedron, 68, 2527 (2012); doi:10.1016/j.tet.2011.12.085.
Y. Miyake, S.-I. Ota and Y. Nishibayashi, Chem. Eur. J., 18, 13255 (2012); doi:10.1002/chem.201202853.
G.M. Sheldrick, SHELXTL97, Program for the Refinement of Crystal Structure, University of Gottingen, Germany (1997).