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Vol. 27 No. 2 (2015): Vol 27 Issue 2

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Solvothermal Synthesis of Nickel Oxide Nanoparticles Decorated Graphene Sheets for Electrochemical Detection of Glucose

https://doi.org/10.14233/ajchem.2015.17947
Jianping Xu
Fundamental Science on Radioactive Geology and Exploration Technology Laboratory, Department of Materials Science and Engineering, East China Institute of Technology, Nanchang 330013, Jiangxi Province, P.R. China
Fucheng Ye
Fundamental Science on Radioactive Geology and Exploration Technology Laboratory, Department of Materials Science and Engineering, East China Institute of Technology, Nanchang 330013, Jiangxi Province, P.R. China
Chunyan Wang
Fundamental Science on Radioactive Geology and Exploration Technology Laboratory, Department of Materials Science and Engineering, East China Institute of Technology, Nanchang 330013, Jiangxi Province, P.R. China

Corresponding Author(s) : Chunyan Wang

chunyanwang@ecit.cn

Asian Journal of Chemistry, Vol. 27 No. 2 (2015): Vol 27 Issue 2

Abstract

In this study, we proposed a facial solvothermal approach to the in situ decoration of nickel oxide nanoparticles on the surface of solvothermal reduced graphene (NiO@SRG). The high dispersion of NiO nanoparticles with the uniform size distribution could be easily obtained via using simple solvothermal process. Moreover, the as-prepared NiO@SRG modified glassy carbon electrode (GCE) exhibited better non-enzymatic electrocatalytic responses towards glucose detection and the limit of detection is 1.15 μM (S/N = 3) in alkaline media. In addition, this electrode material possessed some important advantages such as low cost, easy preparation, good stability and high reproducibility. The influence of some interfering species was investigated and the result indicated that these foreign substances did not interfere significantly on the detection of glucose. This new findings demonstrate that NiO@SRG is a promising candidate of advanced electrode material in electrochemical sensing and other electrocatalytic applications.

Keywords

Synthesis NiO nanoparticles Solvothermal reduced graphene Enzyme-free glucose detection
Xu, J., Ye, F., & Wang, C. (2015). Solvothermal Synthesis of Nickel Oxide Nanoparticles Decorated Graphene Sheets for Electrochemical Detection of Glucose. Asian Journal of Chemistry, 27(2), 729–733. https://doi.org/10.14233/ajchem.2015.17947
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